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CN1362180A - Nano spleen and stomach invigorating and vital energy benefiting medicine and its preparation - Google Patents

Nano spleen and stomach invigorating and vital energy benefiting medicine and its preparation Download PDF

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Publication number
CN1362180A
CN1362180A CN 01100335 CN01100335A CN1362180A CN 1362180 A CN1362180 A CN 1362180A CN 01100335 CN01100335 CN 01100335 CN 01100335 A CN01100335 A CN 01100335A CN 1362180 A CN1362180 A CN 1362180A
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nanometer
nano
parts
chinese
spleen
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CN 01100335
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Chinese (zh)
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杨孟君
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Individual
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Individual
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Abstract

The present invention discloses a nano Buzhong-Yiqi preparation medicine. It is made up by uisng 10 Chinese medicinal materials of nano astragalus, nano codonopsis, nano licorice, nano tangkui, nano ovate atractylodes and others as raw material through the processes of microwave extraction, reduced pressure concentration and supersonic jet spray drying. Its grain fineness is up to 1200-1500 meshes, grain size is 0.1-200 nm, in whic hmost of grain size is less than 100 nm. Said medicine is high in biological utilization rate and obvious in therapeutic effect.

Description

A kind of nanometer invigorating the spleen and replenishing QI preparation medicine and preparation method thereof
The present invention relates to a kind of invigorating the spleen and replenishing QI, yang invigorating master and fall into, cure mainly the insufficiency of the spleen nanometer invigorating the spleen and replenishing QI preparation medicine that waits disease, the invention still further relates to the method for this medication preparation.
BUZHONG YIQI WAN is a kind of classical Chinese patent medicine, mainly contains the adjusting gastrointestinal motility, anti-gastric-ulcer and anti-gastric mucosa injury, excited uterus, regulate immunologic function, promote effects such as metabolism, be used for weakness of the spleen and stomach, sinking of QI of middle-JIAO and cause fatigue and asthenia, lack of appetite abdominal distention, chronic diarrhea, diseases such as dehydration.But traditional BUZHONG YIQI WAN disintegrate is slower, absorbs not exclusively, and bioavailability is not high, slow curative effect.
The object of the present invention is to provide a kind of bioavailability height, solid dispersion is good, absorbs fully the nanometer invigorating the spleen and replenishing QI preparation medicine of increase evident in efficacy.
Another object of the present invention provides the preparation method of this nanometer invigorating the spleen and replenishing QI preparation medicine.
To achieve these goals, the present invention takes following technical scheme:
Medicine of the present invention is to make (consumption is a weight portion) by following component:
Nano astragalus 150-250 part nanometer Radix Codonopsis 40-80 part nanometer Radix Glycyrrhizae 60-140 part
Nano Chinese angelica 40-80 part nanometer Rhizoma Atractylodis Macrocephalae 40-80 part nanometer Rhizoma Cimicifugae 40-80 part
Nano bupleurum 40-80 part nanometer Pericarpium Citri Reticulatae 40-80 part nanometer Rhizoma Zingiberis Recens 10-30 part
Nanometer Fructus Jujubae 20-60 part
The formula optimization weight proportion scope of medicine of the present invention is:
Nano astragalus 160-240 part nanometer Radix Codonopsis 50-70 part nanometer Radix Glycyrrhizae 80-120 part
Nano Chinese angelica 50-70 part nanometer Rhizoma Atractylodis Macrocephalae 50-70 part nanometer Rhizoma Cimicifugae 50-70 part
Nano bupleurum 50-70 part nanometer Pericarpium Citri Reticulatae 50-70 part nanometer Rhizoma Zingiberis Recens 15-25 part
Nanometer Fructus Jujubae 30-50 part
The optimum weight proportioning of medicine of the present invention is:
100 parts in 60 parts of nanometer Radix Glycyrrhizaes of 200 parts of nanometer Radix Codonopsis of nano astragalus
60 parts of 60 parts of nanometer Rhizoma Cimicifugaes of 60 parts of nanometer Rhizoma Atractylodis Macrocephalaes of nano Chinese angelica
20 parts in 60 portions of nanometer Rhizoma Zingiberis Recenss of 60 parts of nanometer Pericarpium Citri Reticulataes of nano bupleurum
40 parts in nanometer Fructus Jujubae
Technical scheme of the present invention is based on the modern material technology.One of modern material Developing Trend in Technology is to develop to the more and more littler direction of yardstick.The granule of the past composition material, its size all are at micron or more than the millimeter magnitude, and have occurred the material to the nanoscale development now.Because extremely refinement of granule, the shared percentage by volume of crystal boundary increases, and makes some performance of material that outstanding variation take place.
The property of nano material is because the special construction of nano material---the particle size of material is less than the ultra-micro powder of 100nm, its body surface area is very big, the atom number ratio at crystal boundary place makes it to produce four big effects up to 15%-50%: i.e. small-size effect, quantum effect (containing macro quanta tunnel effect), skin effect and interfacial effect.Thereby has the not available physical and chemical performance of traditional material.Nanotechnology will bring a technological revolution of the field of Chinese medicines.
One of method of above-mentioned each component being made medicine of the present invention is:
1. divide and get the Chinese crude drug of respectively distinguishing the flavor of, add to concoct according to Chinese Pharmacopoeia one one of version in 2000 and be processed into the common Chinese decoction pieces
2. divide and get the common Chinese decoction pieces of respectively distinguishing the flavor of, be processed into the nanometer prepared slices of Chinese crude drugs, its method comprises the following steps:
1. the common Chinese decoction pieces is placed extraction pot, solubilizer also imports microwave extracting, makes its speed with 20-30 hundred million times/second do the change in polarity motion, and the temperature of its microwave extracting is 30 ℃-60 ℃, time 1-10 hour;
2. above-mentioned extract is carried out concentrating under reduced pressure, temperature is 30 ℃-60 ℃, and the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition;
3. decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 330 meters-990 meter per seconds of effluxvelocity, 30 ℃ of-60 ℃ of temperature, under 0 to 0.05MPa the pressure,, promptly make the nanometer prepared slices of Chinese crude drugs with the instantaneous drying of hypersonic velocity.
3. the nanometer prepared slices of Chinese crude drugs (powder) are prepared mixing in described ratio, according to Chinese Pharmacopoeia version two-shift system in 2000 agent standard, make pill, powder, tablet, suppository, granule, membrane, capsule, microcapsule, drop pill, aerosol, injection, unguentum, medicated wine, syrup, oral solution.
Two of medicine method for making of the present invention is:
1. be equipped with whole common Chinese decoction pieces in the proportioning ratio, place extraction pot, solubilizer also imports microwave extracting, makes its speed with 20-30 hundred million times/second do the change in polarity motion, and the temperature of its microwave extracting is 30 ℃-60 ℃, time 1-10 hour;
2. above-mentioned extract is carried out concentrating under reduced pressure, temperature is 30 ℃-60 ℃, and the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition;
3. decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 330 meters-990 meter per seconds of effluxvelocity, 30 ℃ of-60 ℃ of temperature, under 0 to 0.05MPa the pressure,, get invigorating the spleen and replenishing QI preparation nano powder with the instantaneous drying of hypersonic velocity jet;
4. its nano powder is made aforementioned various preparation according to Chinese Pharmacopoeia version standard preparation in 2000.
The pharmacological effect that above-mentioned two kinds of methods are made nanometer invigorating the spleen and replenishing QI preparation medicine is identical.
A kind of important feature of the present invention is: the made drug material of the present invention has reached nanoscale, common BUZHONG YIQI WAN preparation material is micron or the above particle diameter of millimeter, can only cross the 80-120 mesh sieve, the drug material that the present invention is made, particle diameter is at 0.1-200nm, the overwhelming majority can be crossed the 1200-1500 mesh sieve less than 100nm.
Another important feature of the present invention is: solid preparation of the present invention disintegrate rapidly, and solid dispersion is good in water, absorbs fully, and the pharmacological action effect that mainly contains effective constituent is significantly higher than conventional formulation.
The pharmaceutical preparation that the present invention is made does not need to add any adjuvant, and is more favourable to human body.
The present invention has also created the new drug formulation that powder, suppository, granule, membrane, microcapsule, drop pill, aerosol, injection, unguentum, medicated wine, syrup of nanometer invigorating the spleen and replenishing QI preparation medicine etc. is had no precedent in the past.
Pharmaceutical preparation of the present invention can be used for spleen deficiency, gastroptosis, and uterine prolapse, proctoptosis, treatment of conditions such as metrorrhagia, clinical efficacy significantly is better than traditional BUZHONG YIQI WAN.
The present invention's added solvent in microwave extracting is water or ethanol.
The present invention carries out in the concentrating under reduced pressure step at extract, and its concentrating under reduced pressure is conventional scheme.
Embodiment 1:
Prepare nano raw material by preceding method:
100 parts in 60 parts of nanometer Radix Glycyrrhizaes of 200 parts of nanometer Radix Codonopsis of nano astragalus
60 parts of 60 parts of nanometer Rhizoma Cimicifugaes of 60 parts of nanometer Rhizoma Atractylodis Macrocephalaes of nano Chinese angelica
20 parts in 60 portions of nanometer Rhizoma Zingiberis Recenss of 60 parts of nanometer Pericarpium Citri Reticulataes of nano bupleurum
40 parts in nanometer Fructus Jujubae
Production method is as follows:
In the GMP cleaning shop, after the above-mentioned nanometer prepared slices of Chinese crude drugs or powder prepared mixing in described ratio, according to Chinese Pharmacopoeia version two-shift system in 2000 agent capsules agent standard, do not add adjuvant, do not granulate, directly divide encapsulated with the fully-automatic capsule racking machine, make capsule, every capsules content of dispersion is the 0.1-0.6 gram, and the patient takes the 1-5 grain at every turn, and is every with 1-4 time.
Embodiment 2:
Prepare nano raw material by preceding method:
100 parts in 60 parts of nanometer Radix Glycyrrhizaes of 200 parts of nanometer Radix Codonopsis of nano astragalus
60 parts of 60 parts of nanometer Rhizoma Cimicifugaes of 60 parts of nanometer Rhizoma Atractylodis Macrocephalaes of nano Chinese angelica
20 parts in 60 portions of nanometer Rhizoma Zingiberis Recenss of 60 parts of nanometer Pericarpium Citri Reticulataes of nano bupleurum
40 parts in nanometer Fructus Jujubae
Production method is as follows:
In the GMP cleaning shop, after the above-mentioned nanometer prepared slices of Chinese crude drugs or powder prepared mixing in described ratio, according to Chinese Pharmacopoeia version two-shift system in 2000 agent capsules agent standard, do not add adjuvant, make nanometer invigorating the spleen and replenishing QI powder needle injection, every injection content 5-20 milligram, each consumption is that 1-2 props up, use 1-3 every day.
Embodiment 3:
Prepare nano raw material by preceding method:
100 parts in 60 parts of nanometer Radix Glycyrrhizaes of 200 parts of nanometer Radix Codonopsis of nano astragalus
60 parts of 60 parts of nanometer Rhizoma Cimicifugaes of 60 parts of nanometer Rhizoma Atractylodis Macrocephalaes of nano Chinese angelica
20 parts in 60 portions of nanometer Rhizoma Zingiberis Recenss of 60 parts of nanometer Pericarpium Citri Reticulataes of nano bupleurum
40 parts in nanometer Fructus Jujubae
Production method is as follows:
In the GMP cleaning shop, after the above-mentioned nanometer prepared slices of Chinese crude drugs or powder prepared mixing in described ratio, according to Chinese Pharmacopoeia version two-shift system in 2000 agent capsules agent standard, filmogen adopts polyvinyl alcohol, make nanometer invigorating the spleen and replenishing QI membrane, every membrane area size 2-100 square centimeter, content of dispersion is the 1-50 gram, every medicine film pasted 1-7 days, pasted the medicine position: abdominal part, back, chest.

Claims (6)

1, a kind of nanometer invigorating the spleen and replenishing QI preparation medicine is characterized in that it is the medicament that the nano raw material of following weight proportioning is made:
Nano astragalus 150-250 part nanometer Radix Codonopsis 40-80 part nanometer Radix Glycyrrhizae 60-140 part
Nano Chinese angelica 40-80 part nanometer Rhizoma Atractylodis Macrocephalae 40-80 part nanometer Rhizoma Cimicifugae 40-80 part
Nano bupleurum 40-80 part nanometer Pericarpium Citri Reticulatae 40-80 part nanometer Rhizoma Zingiberis Recens 10-30 part
Nanometer Fructus Jujubae 20-60 part
And adopt following method to make: to select the formula Chinese drug material to concoct and be processed into the prepared slices of Chinese crude drugs; Place extraction pot, solubilizer also imports microwave extracting, makes it do the change in polarity motion with hundred million times/second speed of 20--30, and the temperature of its microwave extracting is 30--60 ℃, time 1--10 hour; Above-mentioned extract is carried out concentrating under reduced pressure, and temperature is 30--60 ℃, and the time is 3--72 hour, collects volatile material in the Chinese medicine simultaneously in addition; Decompressed concentrate and volatile material merging are placed spray drying tower, use the Supersonic fluidics, 30--60 ℃ of temperature, under 0 to 0.05MPa the pressure, with hypersonic velocity instantaneous jet drying, wherein supersonic jet speed is 330 meters-990 meter per seconds, promptly makes the nanometer prepared slices of Chinese crude drugs.
2, nanometer invigorating the spleen and replenishing QI preparation medicine according to claim 1, wherein the weight proportion of each nano raw material is:
Nano astragalus 160-240 part nanometer Radix Codonopsis 50-70 part nanometer Radix Glycyrrhizae 80-120 part
Nano Chinese angelica 50-70 part nanometer Rhizoma Atractylodis Macrocephalae 50-70 part nanometer Rhizoma Cimicifugae 50-70 part
Nano bupleurum 50-70 part nanometer Pericarpium Citri Reticulatae 50-70 part nanometer Rhizoma Zingiberis Recens 15-25 part
Nanometer Fructus Jujubae 30-50 part
3, nanometer invigorating the spleen and replenishing QI preparation medicine according to claim 1, wherein the weight proportion of each nano raw material is:
100 parts in 60 parts of nanometer Radix Glycyrrhizaes of 200 parts of nanometer Radix Codonopsis of nano astragalus
60 parts of 60 parts of nanometer Rhizoma Cimicifugaes of 60 parts of nanometer Rhizoma Atractylodis Macrocephalaes of nano Chinese angelica
20 parts in 60 portions of nanometer Rhizoma Zingiberis Recenss of 60 parts of nanometer Pericarpium Citri Reticulataes of nano bupleurum
40 parts in nanometer Fructus Jujubae
4, according to claim 1 or 2 or 3 described nanometer invigorating the spleen and replenishing QI preparation medicines, it is characterized in that said medicine is pill, powder, tablet, suppository, granule, membrane, capsule, microcapsule, drop pill, aerosol, injection, unguentum, medicated wine, syrup, oral solution.
5,, it is characterized in that this method comprises the steps: to select the formula Chinese drug material to concoct and is processed into the prepared slices of Chinese crude drugs according to the pharmaceutical methods of claim 1 or 2 or 3 described nanometer invigorating the spleen and replenishing QI preparation medicines; Place extraction pot, solubilizer also imports microwave extracting, makes it do the change in polarity motion with hundred million times/second speed of 20--30, and the temperature of its microwave extracting is 30--60 ℃, time 1--10 hour; Above-mentioned extract is carried out concentrating under reduced pressure, and temperature is 30--60 ℃, and the time is 3--72 hour, collects volatile material in the Chinese medicine simultaneously in addition; Decompressed concentrate and volatile material merging are placed spray drying tower, use the Supersonic fluidics, 30--60 ℃ of temperature, under 0 to 0.05MPa the pressure, with hypersonic velocity instantaneous jet drying, wherein supersonic jet speed is 330 meters-990 meter per seconds, promptly makes the nanometer prepared slices of Chinese crude drugs.
6, wherein respectively distinguish the flavor of Chinese medicine in the ratio of prescription or Chinese crude drug concoct be processed into the prepared slices of Chinese crude drugs after mixing, or after making the nanometer prepared slices of Chinese crude drugs mixing.
CN 01100335 2001-01-02 2001-01-02 Nano spleen and stomach invigorating and vital energy benefiting medicine and its preparation Pending CN1362180A (en)

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Application Number Priority Date Filing Date Title
CN 01100335 CN1362180A (en) 2001-01-02 2001-01-02 Nano spleen and stomach invigorating and vital energy benefiting medicine and its preparation

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Application Number Priority Date Filing Date Title
CN 01100335 CN1362180A (en) 2001-01-02 2001-01-02 Nano spleen and stomach invigorating and vital energy benefiting medicine and its preparation

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CN1362180A true CN1362180A (en) 2002-08-07

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103251856A (en) * 2013-05-08 2013-08-21 山西省肿瘤研究所 Traditional Chinese medicine preparation for benefiting Qi and nourishing blood and preparation method of traditional Chinese medicine preparation
CN105193967A (en) * 2015-09-12 2015-12-30 南京正亮医药科技有限公司 Method for extracting plant composition containing cimicifugae foetidae and application

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103251856A (en) * 2013-05-08 2013-08-21 山西省肿瘤研究所 Traditional Chinese medicine preparation for benefiting Qi and nourishing blood and preparation method of traditional Chinese medicine preparation
CN103251856B (en) * 2013-05-08 2015-07-22 山西省肿瘤研究所 Traditional Chinese medicine preparation for benefiting Qi and nourishing blood and preparation method of traditional Chinese medicine preparation
CN105193967A (en) * 2015-09-12 2015-12-30 南京正亮医药科技有限公司 Method for extracting plant composition containing cimicifugae foetidae and application

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