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CN1366937A - Nano quiet heart and supplement kidney preparation medicine and preparation method - Google Patents

Nano quiet heart and supplement kidney preparation medicine and preparation method Download PDF

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Publication number
CN1366937A
CN1366937A CN 01102079 CN01102079A CN1366937A CN 1366937 A CN1366937 A CN 1366937A CN 01102079 CN01102079 CN 01102079 CN 01102079 A CN01102079 A CN 01102079A CN 1366937 A CN1366937 A CN 1366937A
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nanometer
parts
nano
part nanometer
semen
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Chinese (zh)
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杨孟君
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Abstract

The present invention discloses a nano Ningxin Bushen preparation medicine. It is made up by using 20 Chinese medicinal materials of nano codonopsis, nano dipsacus, nano complanate astragalus seed, nano cherokee rose fruit, nano euryale and others as raw material through the processes of microwave extraction, reduced pressure concentration and supersonic jet spray drying. Its grain fineness is up to 1200-1500 meshes, grain size is 0.1-200 nm, in which most of grain size is less than 100 nm.

Description

Nano quiet heart and supplement kidney preparation medicine and preparation method thereof
The present invention relates to a kind of quiet heart and supplement kidney, the smart nano quiet heart and supplement kidney preparation medicine that ends flaccidity of benefit, the invention still further relates to the method for this medication preparation.
The quiet heart and supplement kidney ball is a kind of classical Chinese patent medicine, mainly contains that quiet heart and supplement kidney, benefit are smart to end effect such as flaccidity, is used for that tinnitus due to deficiency of the kidney, dizziness and blurred vision, palpitation with fear are peaceful, the night sweat body is tired, seminal emission, sterile, the soreness of the waist and knees of sexual impotence.But traditional quiet heart and supplement kidney ball disintegrate is slower, absorbs not exclusively, and bioavailability is not high, slow curative effect.
The object of the present invention is to provide a kind of bioavailability height, solid dispersion is good, absorbs fully the nano quiet heart and supplement kidney preparation medicine of increase evident in efficacy.
Another object of the present invention provides the preparation method of this nano quiet heart and supplement kidney preparation medicine.
To achieve these goals, the present invention takes following technical scheme:
Medicine of the present invention is to make (consumption is a weight portion) by following component:
Nanometer Radix Codonopsis 1000-2500 part nanometer Radix Dipsaci 150-400 part nanometer Semen Astragali Complanati 200-400 part
Nanometer Fructus Rosae Laevigatae 150-400 part nanometer Semen Euryales 180-400 part nm acid Semen Ziziphi Spinosae 150-400 part
Nanometer Stamen Nelumbinis 220-400 part nanometer Os Draconis 150-400 part nanometer Radix Polygoni Multiflori 220-400 part
Nanometer Semen Juglandis 150-400 part nanometer Fructus Lycii 250-450 part nano Poria 100-250 part
Nanometer Fructus Psoraleae 300-650 part nanometer Fructus Rubi 100-250 part nanometer Rhizoma Dioscoreae 150-400 part
Nanometer Semen Allii Tuberosi 100-250 part nanometer Semen Cuscutae 150-400 part nanometer Testis Et penis Bovis seu Bubali 60-150 part
Nanometer Semen Nelumbinis 150-400 part nanometer Fructus Amomi 30-65 part
The formula optimization weight proportion scope of medicine of the present invention is:
Nanometer Radix Codonopsis 1200-2000 part nanometer Radix Dipsaci 200-300 part nanometer Semen Astragali Complanati 250-350 part
Nanometer Fructus Rosae Laevigatae 200-300 part nanometer Semen Euryales 250-350 part nm acid Semen Ziziphi Spinosae 200-300 part
Nanometer Stamen Nelumbinis 250-350 part nanometer Os Draconis 200-300 part nanometer Radix Polygoni Multiflori 270-350 part
Nanometer Semen Juglandis 200-300 part nanometer Fructus Lycii 270-350 part nano Poria 120-200 part
Nanometer Fructus Psoraleae 350-550 part nanometer Fructus Rubi 120-200 part nanometer Rhizoma Dioscoreae 200-300 part
Nanometer Semen Allii Tuberosi 120-200 part nanometer Semen Cuscutae 200-300 part nanometer Testis Et penis Bovis seu Bubali 80-120 part
Nanometer Semen Nelumbinis 200-300 part nanometer Fructus Amomi 35-55 part
The optimum weight proportioning of medicine of the present invention is:
320 parts of 241 parts of nanometer Semen Astragali Complanatis of 1600 parts of nanometer Radix Dipsacis of nanometer Radix Codonopsis
241 parts of 320 parts of nm acid Semen Ziziphi Spinosaes of 241 portions of nanometer Semen Euryaless of nanometer Fructus Rosae Laevigatae
320 parts of 241 parts of nanometer Radix Polygoni Multiflori of 320 parts of nanometer Os Draconis of nanometer Stamen Nelumbinis
160 parts of 320 parts of nano Porias of 241 parts of nanometer Fructus Lycii of nanometer Semen Juglandis
241 parts of 160 parts of nanometer Rhizoma Dioscoreaes of 400 parts of nanometer Fructus Rubies of nanometer Fructus Psoraleae
100 parts of 241 portions of nanometer Testis Et penis Bovis seu Bubali of 160 parts of nanometer Semen Cuscutae of nanometer Semen Allii Tuberosi
47.5 parts of 241 parts of nanometer Fructus Amomis of nanometer Semen Nelumbinis
Technical scheme of the present invention is based on the modern material technology.One of modern material Developing Trend in Technology is to develop to the more and more littler direction of yardstick.The granule of the past composition material, its size all are at micron or more than the millimeter magnitude, and have occurred the material to the nanoscale development now.Because extremely refinement of granule, the shared percentage by volume of crystal boundary increases, and makes some performance of material that outstanding variation take place.
The property of nano material be since special construction----the material grains size of nano material less than the ultra-micro powder of 100nm, its body surface area is very big, the atom number ratio at crystal boundary place makes it to produce four big effects up to 15--50%: i.e. small-size effect, quantum effect (containing macro quanta tunnel effect), skin effect and interfacial effect.Thereby has the not available physical and chemical performance of traditional material.Nanotechnology will bring a technological revolution of the field of Chinese medicines.
One of method of above-mentioned each component being made medicine of the present invention is:
1. divide and get the Chinese crude drug of respectively distinguishing the flavor of, be processed into the common Chinese decoction pieces according to process of preparing Chinese medicine of Chinese Pharmacopoeia version in 2000.
2. divide and get the common Chinese decoction pieces of respectively distinguishing the flavor of, be processed into the nanometer prepared slices of Chinese crude drugs, its method comprises the following steps:
1. the common Chinese decoction pieces is placed extraction pot, solubilizer also imports microwave extracting, makes its speed with 20--30 hundred million times/second do the change in polarity motion, and the temperature of its microwave extracting is 30 ℃--and 60 ℃, time 1-10 hour;
2. above-mentioned extract is carried out concentrating under reduced pressure, temperature is 30 ℃--60 ℃, the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition;
3. decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 330 meters of effluxvelocities--990 meter per seconds, at 30 ℃--60 ℃ of temperature, under 0 to the 0.05MPa pressure,, promptly make the nanometer prepared slices of Chinese crude drugs with hypersonic velocity instantaneous jet drying.
3. the nanometer prepared slices of Chinese crude drugs (powder) are prepared mixing in described ratio, according to Chinese Pharmacopoeia version two-shift system in 2000 agent standard, make pill, powder, tablet, suppository, granule, membrane, capsule, microcapsule, drop pill, aerosol, injection, unguentum, medicated wine, syrup, oral solution.
Two of medicine method for making of the present invention is:
1. be equipped with whole common Chinese decoction pieces in the proportioning ratio, place extraction pot, solubilizer also imports microwave extracting, makes its speed with 20--30 hundred million times/second do the change in polarity motion, and the temperature of its microwave extracting is 30 ℃-60 ℃, time 1-10 hour;
2. above-mentioned extract is carried out concentrating under reduced pressure, temperature is 30 ℃--60 ℃, the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition;
3. decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 330 meters of effluxvelocities--990 meter per seconds, at 30 ℃--60 ℃ of temperature, under 0 to the 0.05MPa pressure,, get the quiet heart and supplement kidney preparation nano powder with hypersonic velocity instantaneous jet drying;
4. its nano powder is made aforementioned various preparation according to Chinese Pharmacopoeia version standard preparation in 2000.
The pharmacological effect that above-mentioned two kinds of methods are made nano quiet heart and supplement kidney preparation medicine is identical.
A kind of important feature of the present invention is: the made drug material of the present invention has reached nanoscale, common quiet heart and supplement kidney pill material is micron or the above particle diameter of millimeter, can only cross the 80-120 mesh sieve, the drug material that the present invention is made, particle diameter is at 0.1--200nm, the overwhelming majority can be crossed the 1200--1500 mesh sieve less than 100nm.
Another important feature of the present invention is: solid preparation of the present invention disintegrate rapidly, and solid dispersion is good in water, absorb fully, the bioavailability height, the pharmacological action effect that mainly contains effective constituent is significantly higher than conventional formulation.
The pharmaceutical preparation that the present invention is made does not need to add any adjuvant, and is more favourable to human body.
The present invention has also created the novel form that powder, tablet, suppository, granule, membrane, capsule, microcapsule, drop pill, aerosol, injection, unguentum, medicated wine, syrup, oral solution of nano quiet heart and supplement kidney preparation medicine etc. is had no precedent in the past.
Treatment of conditions such as pharmaceutical preparation of the present invention can be used for that tinnitus due to deficiency of the kidney, dizziness and blurred vision, palpitation with fear are peaceful, the night sweat body is tired, seminal emission, sexual impotence are sterile, soreness of the waist and knees, clinical efficacy significantly is better than traditional quiet heart and supplement kidney ball.
The present invention's added solvent in microwave extracting is water or ethanol.
The present invention carries out in the concentrating under reduced pressure step at extract, and its concentrating under reduced pressure is conventional scheme.
Embodiment 1:
Prepare nano raw material by preceding method:
320 parts of 241 parts of nanometer Semen Astragali Complanatis of 1600 parts of nanometer Radix Dipsacis of nanometer Radix Codonopsis
241 parts of 320 parts of nm acid Semen Ziziphi Spinosaes of 241 portions of nanometer Semen Euryaless of nanometer Fructus Rosae Laevigatae
320 parts of 241 parts of nanometer Radix Polygoni Multiflori of 320 parts of nanometer Os Draconis of nanometer Stamen Nelumbinis
160 parts of 320 parts of nano Porias of 241 parts of nanometer Fructus Lycii of nanometer Semen Juglandis
241 parts of 160 parts of nanometer Rhizoma Dioscoreaes of 400 parts of nanometer Fructus Rubies of nanometer Fructus Psoraleae
100 parts of 241 portions of nanometer Testis Et penis Bovis seu Bubali of 160 parts of nanometer Semen Cuscutae of nanometer Semen Allii Tuberosi
47.5 parts of 241 parts of nanometer Fructus Amomis of nanometer Semen Nelumbinis
Production method is as follows:
In the GMP cleaning shop, after the above-mentioned nanometer prepared slices of Chinese crude drugs or powder prepared mixing in described ratio, according to Chinese Pharmacopoeia version two-shift system in 2000 agent capsules agent standard, do not add adjuvant, do not granulate, directly divide encapsulated with the fully-automatic capsule racking machine, make capsule, every capsules content of dispersion is the 0.1--0.6 gram, and the patient takes the 1-5 grain at every turn, and take 1-4 every day.
Embodiment 2:
Prepare nano raw material by preceding method:
320 parts of 241 parts of nanometer Semen Astragali Complanatis of 1600 parts of nanometer Radix Dipsacis of nanometer Radix Codonopsis
241 parts of 320 parts of nm acid Semen Ziziphi Spinosaes of 241 portions of nanometer Semen Euryaless of nanometer Fructus Rosae Laevigatae
320 parts of 241 parts of nanometer Radix Polygoni Multiflori of 320 parts of nanometer Os Draconis of nanometer Stamen Nelumbinis
160 parts of 320 parts of nano Porias of 241 parts of nanometer Fructus Lycii of nanometer Semen Juglandis
241 parts of 160 parts of nanometer Rhizoma Dioscoreaes of 400 parts of nanometer Fructus Rubies of nanometer Fructus Psoraleae
100 parts of 241 portions of nanometer Testis Et penis Bovis seu Bubali of 160 parts of nanometer Semen Cuscutae of nanometer Semen Allii Tuberosi
47.5 parts of 241 parts of nanometer Fructus Amomis of nanometer Semen Nelumbinis
Production method is as follows:
In the GMP cleaning shop, with the above-mentioned nanometer prepared slices of Chinese crude drugs or the described mixed of powder good after, according to 2000 editions two-shift system agent of Chinese Pharmacopoeia powder needle injection standard, do not add any adjuvant, make the nano quiet heart and supplement kidney powder needle injection, every injection content is the 5-20 milligram, each consumption is that 1-2 props up, and use 1-3 every day.
Embodiment 3:
Prepare nano raw material by preceding method:
320 parts of 241 parts of nanometer Semen Astragali Complanatis of 1600 parts of nanometer Radix Dipsacis of nanometer Radix Codonopsis
241 parts of 320 parts of nm acid Semen Ziziphi Spinosaes of 241 portions of nanometer Semen Euryaless of nanometer Fructus Rosae Laevigatae
320 parts of 241 parts of nanometer Radix Polygoni Multiflori of 320 parts of nanometer Os Draconis of nanometer Stamen Nelumbinis
160 parts of 320 parts of nano Porias of 241 parts of nanometer Fructus Lycii of nanometer Semen Juglandis
241 parts of 160 parts of nanometer Rhizoma Dioscoreaes of 400 parts of nanometer Fructus Rubies of nanometer Fructus Psoraleae
100 parts of 241 portions of nanometer Testis Et penis Bovis seu Bubali of 160 parts of nanometer Semen Cuscutae of nanometer Semen Allii Tuberosi
47.5 parts of 241 parts of nanometer Fructus Amomis of nanometer Semen Nelumbinis
Production method is as follows:
In the GMP cleaning shop, with the above-mentioned nanometer prepared slices of Chinese crude drugs or powder by described mixed good after, according to 2000 editions two-shift system agent of Chinese Pharmacopoeia membrane standard, filmogen adopts polyvinyl alcohol, make the nano quiet heart and supplement kidney membrane, every membrane area size is the 2-100 square centimeter, and content of dispersion is the 1-50 gram, every medicine film pasted 1-7 days, pasted the medicine position: abdominal part, back, chest.

Claims (6)

1, a kind of nano quiet heart and supplement kidney preparation medicine is characterized in that it is the medicament that the nano raw material of following weight proportioning is made:
Nanometer Radix Codonopsis 1000-2500 part nanometer Radix Dipsaci 150-400 part nanometer Semen Astragali Complanati 200-400 part
Nanometer Fructus Rosae Laevigatae 150-400 part nanometer Semen Euryales 180-400 part nm acid Semen Ziziphi Spinosae 150-400 part
Nanometer Stamen Nelumbinis 220-400 part nanometer Os Draconis 150-400 part nanometer Radix Polygoni Multiflori 220-400 part
Nanometer Semen Juglandis 150-400 part nanometer Fructus Lycii 250-450 powder nano Poria 100-250 part
Nanometer Fructus Psoraleae 300-650 part nanometer Fructus Rubi 100-250 part nanometer Rhizoma Dioscoreae 150-400 part
Nanometer Semen Allii Tuberosi 100-250 part nanometer Semen Cuscutae 150-400 part nanometer Testis Et penis Bovis seu Bubali 60-150 part
Nanometer Semen Nelumbinis 150-400 part nanometer Fructus Amomi 30-65 part
And adopt following method to make: to select the formula Chinese drug material to concoct and be processed into the prepared slices of Chinese crude drugs; Place extraction pot, solubilizer also imports microwave extracting, makes it do the change in polarity motion with hundred million times/second speed of 20--30, and the temperature of its microwave extracting is 30--60 ℃, time 1-10 hour; Above-mentioned extract is carried out concentrating under reduced pressure, and temperature is 30--60 ℃, and the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition; Decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 30--60 ℃ of temperature, under 0 to the 0.05MPa pressure, with hypersonic velocity instantaneous jet drying, wherein supersonic jet speed is 330 meters-990 meter per seconds, promptly makes the nanometer prepared slices of Chinese crude drugs.
2, nano quiet heart and supplement kidney preparation medicine according to claim 1, wherein the weight proportion of each nano raw material is:
Nanometer Radix Codonopsis 1200-2000 part nanometer Radix Dipsaci 200-300 part nanometer Semen Astragali Complanati 250-350 part
Nanometer Fructus Rosae Laevigatae 200-300 part nanometer Semen Euryales 250-350 part nm acid Semen Ziziphi Spinosae 200-300 part
Nanometer Stamen Nelumbinis 250-350 part nanometer Os Draconis 200-300 part nanometer Radix Polygoni Multiflori 270-350 part
Nanometer Semen Juglandis 200-300 part nanometer Fructus Lycii 270-350 part nano Poria 120-200 part
Nanometer Fructus Psoraleae 350-550 part nanometer Fructus Rubi 120-200 part nanometer Rhizoma Dioscoreae 200-300 part
Nanometer Semen Allii Tuberosi 120-200 part nanometer Semen Cuscutae 200-300 part nanometer Testis Et penis Bovis seu Bubali 80-120 part
Nanometer Semen Nelumbinis 200-300 part nanometer Fructus Amomi 35-55 part
3, nano quiet heart and supplement kidney preparation medicine according to claim 1, wherein the weight proportion of each nano raw material is:
320 parts of 241 parts of nanometer Semen Astragali Complanatis of 1600 parts of nanometer Radix Dipsacis of nanometer Radix Codonopsis
241 parts of 320 parts of nm acid Semen Ziziphi Spinosaes of 241 portions of nanometer Semen Euryaless of nanometer Fructus Rosae Laevigatae
320 parts of 241 parts of nanometer Radix Polygoni Multiflori of 320 parts of nanometer Os Draconis of nanometer Stamen Nelumbinis
160 parts of 320 parts of nano Porias of 241 parts of nanometer Fructus Lycii of nanometer Semen Juglandis
241 parts of 160 parts of nanometer Rhizoma Dioscoreaes of 400 parts of nanometer Fructus Rubies of nanometer Fructus Psoraleae
100 parts of 241 portions of nanometer Testis Et penis Bovis seu Bubali of 160 parts of nanometer Semen Cuscutae of nanometer Semen Allii Tuberosi
47.5 parts of 241 parts of nanometer Fructus Amomis of nanometer Semen Nelumbinis
4,, it is characterized in that said medicine is pill, powder, tablet, suppository, granule, membrane, capsule, microcapsule, drop pill, aerosol, injection, unguentum, medicated wine, syrup, oral solution according to claim 1 or 2 or 3 described nano quiet heart and supplement kidney preparation medicines.
5,, it is characterized in that this method comprises the steps: to select the formula Chinese drug material to concoct and is processed into the prepared slices of Chinese crude drugs according to the pharmaceutical methods of claim 1 or 2 or 3 described nano quiet heart and supplement kidney preparation medicines; Place extraction pot, solubilizer also imports microwave extracting, makes it do the change in polarity motion with hundred million times/second speed of 20--30, and the temperature of its microwave extracting is 30--60 ℃, time 1-10 hour; Above-mentioned extract is carried out concentrating under reduced pressure, and temperature is 30--60 ℃, and the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition; Decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 30--60 ℃ of temperature, under 0 to the 0.05MPa pressure, with hypersonic velocity instantaneous jet drying, wherein supersonic jet speed is 330 meters-990 meter per seconds, promptly makes the nanometer prepared slices of Chinese crude drugs.
6, wherein respectively distinguish the flavor of Chinese medicine in the ratio of prescription or Chinese crude drug concoct be processed into the prepared slices of Chinese crude drugs after mixing, or after making the nanometer prepared slices of Chinese crude drugs mixing.
CN 01102079 2001-01-22 2001-01-22 Nano quiet heart and supplement kidney preparation medicine and preparation method Pending CN1366937A (en)

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Application Number Priority Date Filing Date Title
CN 01102079 CN1366937A (en) 2001-01-22 2001-01-22 Nano quiet heart and supplement kidney preparation medicine and preparation method

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CN1366937A true CN1366937A (en) 2002-09-04

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104116887A (en) * 2014-08-15 2014-10-29 徐美春 Pharmaceutical composition for treating arrhythmia and preparation method of pharmaceutical composition
CN104839551A (en) * 2015-05-22 2015-08-19 遵义市杨老大米粉厂 Nutritious rice flour and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104116887A (en) * 2014-08-15 2014-10-29 徐美春 Pharmaceutical composition for treating arrhythmia and preparation method of pharmaceutical composition
CN104839551A (en) * 2015-05-22 2015-08-19 遵义市杨老大米粉厂 Nutritious rice flour and preparation method thereof

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