[go: up one dir, main page]

RU2008108332A - METHOD FOR PRODUCING 2 - [(2-DIMETHYLAMINO) METHYL] PHENOL - Google Patents

METHOD FOR PRODUCING 2 - [(2-DIMETHYLAMINO) METHYL] PHENOL Download PDF

Info

Publication number
RU2008108332A
RU2008108332A RU2008108332/04A RU2008108332A RU2008108332A RU 2008108332 A RU2008108332 A RU 2008108332A RU 2008108332/04 A RU2008108332/04 A RU 2008108332/04A RU 2008108332 A RU2008108332 A RU 2008108332A RU 2008108332 A RU2008108332 A RU 2008108332A
Authority
RU
Russia
Prior art keywords
phenol
dimethylamino
methyl
bisamine
producing
Prior art date
Application number
RU2008108332/04A
Other languages
Russian (ru)
Other versions
RU2384567C2 (en
Inventor
Мария Геннадьевна Шайбакова (RU)
Мария Геннадьевна Шайбакова
Ирина Геннадьевна Титова (RU)
Ирина Геннадьевна Титова
Гилемдар Адыхамович Махмудияров (RU)
Гилемдар Адыхамович Махмудияров
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Original Assignee
ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА Российской академии наук (RU)
ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА Российской Академии Наук
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА Российской академии наук (RU), ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА Российской Академии Наук filed Critical ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА Российской академии наук (RU)
Priority to RU2008108332/04A priority Critical patent/RU2384567C2/en
Publication of RU2008108332A publication Critical patent/RU2008108332A/en
Application granted granted Critical
Publication of RU2384567C2 publication Critical patent/RU2384567C2/en

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Способ получения 2-[(диметиламино)метил]фенола формулы (1): ! ! взаимодействием фенола с бисамином (N,N,N,N-тетраметилметилендиамином), отличающийся тем, что реакцию проводят в присутствии катализатора хлорида меди (I) при мольном соотношении реагентов фенол: бисамин: CuCl=10:(10-11):(0,2-0,4) при температуре 50°С и атмосферном давлении в течение 3,5-4,5 ч.The method of obtaining 2 - [(dimethylamino) methyl] phenol of the formula (1):! ! the interaction of phenol with bisamine (N, N, N, N-tetramethylmethylenediamine), characterized in that the reaction is carried out in the presence of a catalyst of copper (I) chloride at a molar ratio of reagents phenol: bisamine: CuCl = 10: (10-11) :( 0 , 2-0.4) at a temperature of 50 ° C and atmospheric pressure for 3.5-4.5 hours

Claims (1)

Способ получения 2-[(диметиламино)метил]фенола формулы (1):The method of obtaining 2 - [(dimethylamino) methyl] phenol of the formula (1):
Figure 00000001
Figure 00000001
 взаимодействием фенола с бисамином (N,N,N,N-тетраметилметилендиамином), отличающийся тем, что реакцию проводят в присутствии катализатора хлорида меди (I) при мольном соотношении реагентов фенол: бисамин: CuCl=10:(10-11):(0,2-0,4) при температуре 50°С и атмосферном давлении в течение 3,5-4,5 ч. the interaction of phenol with bisamine (N, N, N, N-tetramethylmethylenediamine), characterized in that the reaction is carried out in the presence of a catalyst of copper (I) chloride at a molar ratio of reagents phenol: bisamine: CuCl = 10: (10-11) :( 0 , 2-0.4) at a temperature of 50 ° C and atmospheric pressure for 3.5-4.5 hours
RU2008108332/04A 2008-03-03 2008-03-03 Method of producing 2-[(dimethylamino)methyl]phenol RU2384567C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2008108332/04A RU2384567C2 (en) 2008-03-03 2008-03-03 Method of producing 2-[(dimethylamino)methyl]phenol

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2008108332/04A RU2384567C2 (en) 2008-03-03 2008-03-03 Method of producing 2-[(dimethylamino)methyl]phenol

Publications (2)

Publication Number Publication Date
RU2008108332A true RU2008108332A (en) 2009-09-10
RU2384567C2 RU2384567C2 (en) 2010-03-20

Family

ID=41166109

Family Applications (1)

Application Number Title Priority Date Filing Date
RU2008108332/04A RU2384567C2 (en) 2008-03-03 2008-03-03 Method of producing 2-[(dimethylamino)methyl]phenol

Country Status (1)

Country Link
RU (1) RU2384567C2 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2490378C1 (en) * 2012-03-23 2013-08-20 Общество с ограниченной ответственностью Научно-производственный центр "УВИКОМ" (ООО НПЦ "УВИКОМ") Method of producing carbon fiber material
CN103923073B (en) * 2014-04-16 2016-06-29 中国农业科学院兰州畜牧与兽药研究所 The preparation method of puerarin derivate
CA3214437A1 (en) * 2021-03-31 2022-10-06 Chevron Oronite Company Llc Fuel additives for reducing low speed pre-ignition events

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2146666C1 (en) * 1998-03-18 2000-03-20 ЗАО "Стерлитамакский нефтехимический завод" Method of preparing mixture of phenol mannich bases
RU2144529C1 (en) * 1998-03-18 2000-01-20 ЗАО "Стерлитамакский нефтехимический завод" Method of preparing 2-(n,n-dimethylaminomethyl)phenol

Also Published As

Publication number Publication date
RU2384567C2 (en) 2010-03-20

Similar Documents

Publication Publication Date Title
RU2008108332A (en) METHOD FOR PRODUCING 2 - [(2-DIMETHYLAMINO) METHYL] PHENOL
ES2667220T3 (en) Procedure for the production of 3- (methylthio) propanal
RU2010132919A (en) METHOD FOR SELECTIVE OBTAINING α, ω-BIS- (1,3,5-DITIAZINAN-5-IL) -3-OXOPENTANE And α, ω-BIS- (1,3,5-DITIAZINAN-5-IL) -3,6 -DIOXOACTANE
RU2010108950A (en) METHOD FOR PRODUCING 3,7-DIARIL-1,3,5,7-DITIADIAZAOCTANES
RU2008132383A (en) METHOD FOR PRODUCING N1, N1, N4, N4-TETRAMETHYL-2-BUTIN-1,4-DIAMINE
RU2008139744A (en) METHOD FOR PRODUCING 2,5-THIOPHENIC CARBONIC ACID OF DIMETHYL ETHER FROM 2-THIOPHENCARBOXYLIC ACID
RU2005114640A (en) METHOD FOR PRODUCING N-METHYLENE-4H-1,3,5-Dithiazinyl-5 (6H) AMINE
RU2012100111A (en) METHOD FOR PRODUCING 2- AND 2,3-SUBSTITUTED QUINOLINS
RU2008152916A (en) METHOD FOR PRODUCING 4- (DIMETHYLAMINO) -2-BUTINYLalkanoates
RU2011124568A (en) METHOD FOR PRODUCING α, ω-BIS- (1,5,3-DITIAZEPINAN-3-IL) ALKANOV
RU2007122003A (en) METHOD FOR PRODUCING 1-HYDROXY-1,2-DIHYDRO [60] FULLERENA
EA201100377A1 (en) METHOD OF OBTAINING SULPHONAMIDES
RU2008103305A (en) METHOD FOR PRODUCING 1-PHENOXY-1,2-DIHYDRO [60] FULLERENA
RU2008134295A (en) METHOD FOR PRODUCING 1-AMINOMETHYL-ALPHA, OMEGA-ALKADIINS
RU2008111405A (en) METHOD FOR PRODUCING SYMMETRIC HEM DIAMINES
RU2009145310A (en) METHOD FOR PRODUCING 3- (PHENYLMETHYLIDENE) -2-THIIRTHION
RU2012154466A (en) METHOD FOR PRODUCING 3-ARIL-1,5,3-DIOXAZEPANES
RU2010137370A (en) METHOD FOR PRODUCING N, N-DIMETHYL-N - [(Alkylsulfanyl) methyl] amines
RU2008122309A (en) METHOD FOR PRODUCING ALPHA, GAMMA-DI (AMINOMETHYL) -ALKADIINS
RU2010100064A (en) METHOD FOR PRODUCING N- [4-NITRO (2,4-dinitro) phenyl] -1,3,5-dithiazinan-5-amines
RU2008143821A (en) METHOD FOR PRODUCING EXO-TRICYCLO [4.2.1.02,5] NONAN-3-SPIRO-1 '- (3'-SELENIUM) CYCLOPENTANE
RU2009146601A (en) METHOD FOR PRODUCING N, N-DIMETHYL-5-ALKyl-2-Thiophenamines
RU2008102177A (en) METHOD FOR PRODUCING 4- (DIMETHYLAMINO) -1-ALKYL-1-METHYL-2-BUTIN-1-OLOV
RU2012155395A (en) METHOD FOR PRODUCING 3-ARYL-1,5,3-DITIAZOCANES
RU2007132632A (en) METHOD FOR PRODUCING SPIRO [3,4] OKTAN-6-OLA

Legal Events

Date Code Title Description
MM4A The patent is invalid due to non-payment of fees

Effective date: 20110304