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RU2005114640A - METHOD FOR PRODUCING N-METHYLENE-4H-1,3,5-Dithiazinyl-5 (6H) AMINE - Google Patents

METHOD FOR PRODUCING N-METHYLENE-4H-1,3,5-Dithiazinyl-5 (6H) AMINE Download PDF

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Publication number
RU2005114640A
RU2005114640A RU2005114640/04A RU2005114640A RU2005114640A RU 2005114640 A RU2005114640 A RU 2005114640A RU 2005114640/04 A RU2005114640/04 A RU 2005114640/04A RU 2005114640 A RU2005114640 A RU 2005114640A RU 2005114640 A RU2005114640 A RU 2005114640A
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RU
Russia
Prior art keywords
dithiazinyl
methylene
amine
producing
hydrogen sulfide
Prior art date
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RU2005114640/04A
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Russian (ru)
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RU2291864C1 (en
Inventor
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Внира Рахимовна Ахметова (RU)
Внира Рахимовна Ахметова
Гузель Ражаповна Надыргулова (RU)
Гузель Ражаповна Надыргулова
Светлана Ринатовна Хафизова (RU)
Светлана Ринатовна Хафизова
Райхана Валиулловна Кунакова (RU)
Райхана Валиулловна Кунакова
Тать на Викторовна Тюмкина (RU)
Татьяна Викторовна Тюмкина
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Priority to RU2005114640/04A priority Critical patent/RU2291864C1/en
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Claims (1)

Способ получения N-метилен-4H-1,3,5-дитиазинил-5(6H)амина (1) общей формулыThe method of obtaining N-methylene-4H-1,3,5-dithiazinyl-5 (6H) amine (1) of the General formula
Figure 00000001
Figure 00000001
 отличающийся тем, что насыщенный сероводородом водный раствор формальдегида взаимодействует с гидразином в буферном растворе бутанол-бутилата натрия (BuONa) в мольном соотношении гидразин: формальдегид: сероводород: бутилат натрия равном 1:4:2:4, при комнатной температуре 20-21°С и перемешивании в течение 3 ч.characterized in that the aqueous solution of formaldehyde saturated with hydrogen sulfide interacts with hydrazine in a buffer solution of sodium butanol-butylate (BuONa) in a molar ratio hydrazine: formaldehyde: hydrogen sulfide: sodium butylate equal to 1: 4: 2: 4, at room temperature 20-21 ° С and stirring for 3 hours
RU2005114640/04A 2005-05-13 2005-05-13 Method for preparing n-methylene-4h-1,3,5-dithiazinyl-5(6h)-amine RU2291864C1 (en)

Priority Applications (1)

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RU2005114640/04A RU2291864C1 (en) 2005-05-13 2005-05-13 Method for preparing n-methylene-4h-1,3,5-dithiazinyl-5(6h)-amine

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RU2005114640/04A RU2291864C1 (en) 2005-05-13 2005-05-13 Method for preparing n-methylene-4h-1,3,5-dithiazinyl-5(6h)-amine

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RU2005114640A true RU2005114640A (en) 2006-11-20
RU2291864C1 RU2291864C1 (en) 2007-01-20

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Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2342371C2 (en) * 2007-02-06 2008-12-27 Институт нефтехимии и катализа РАН Method of obtaining 5-acetylsaliciloyl-1,3,5-dithiazinan
RU2342369C1 (en) * 2007-07-09 2008-12-27 Институт нефтехимии и катализа РАН Method of obtaining 5-(1,3,5-dithiazinan-5-sulfanyl)-phenyl) -1,3,5-dithiazinan
RU2342370C1 (en) * 2007-07-16 2008-12-27 Институт нефтехимии и катализа РАН "method of obtaining n-[1',3',5'-dithiazinan-5'-yl-carbonyl]-1,3,5-dithiazinan-5-carboxamide"
RU2481337C2 (en) * 2009-01-26 2013-05-10 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing 2,4,6-trimethyl-(1,3,5-dithiazinan-5-yl)amine
RU2434857C2 (en) * 2010-01-11 2011-11-27 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing n-[4-nitro(2,4-dinitro)phenyl]-1,3,5-dithiazinane-5-amines
RU2448107C2 (en) * 2010-06-02 2012-04-20 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing 3,3'-bi-1,5,3-dithiazepinane and use thereof as fungicidally active agent
RU2464265C2 (en) * 2010-07-28 2012-10-20 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing n-aryl(benzyl)-(1,3,5-dithiazin-5-yl)amines
RU2447068C1 (en) * 2010-08-05 2012-04-10 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing n-phenyl(benzyl)-1,5,3-dithiazepinane-3-amines and 2,4-dimethyl-n-phenyl(benzyl)-1,5,3-dithiazepinane-3-amines
RU2478626C1 (en) * 2011-08-15 2013-04-10 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing n-(1,5,3-dithiazepan-3-yl)amides

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU782337A1 (en) * 1979-06-19 1988-06-07 Иркутский институт органической химии СО АН СССР 2h,4h-2,4-dimethyl-6-amino-1.3,5-dithiazine possessing radioprotective action
DE19700062A1 (en) * 1997-01-03 1998-07-09 Bayer Ag S-aryldithiazine dioxides

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Effective date: 20070514