RU2014148431A - Способы обработки лигноцеллюлозных материалов - Google Patents
Способы обработки лигноцеллюлозных материалов Download PDFInfo
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- RU2014148431A RU2014148431A RU2014148431A RU2014148431A RU2014148431A RU 2014148431 A RU2014148431 A RU 2014148431A RU 2014148431 A RU2014148431 A RU 2014148431A RU 2014148431 A RU2014148431 A RU 2014148431A RU 2014148431 A RU2014148431 A RU 2014148431A
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- amine
- weight
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- 238000000034 method Methods 0.000 title claims abstract 38
- 150000001412 amines Chemical class 0.000 claims abstract 27
- 235000000346 sugar Nutrition 0.000 claims abstract 18
- 239000003085 diluting agent Substances 0.000 claims abstract 8
- 150000001768 cations Chemical class 0.000 claims abstract 6
- 239000012535 impurity Substances 0.000 claims abstract 6
- 239000002253 acid Substances 0.000 claims abstract 4
- 230000002378 acidificating effect Effects 0.000 claims abstract 4
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims abstract 4
- 239000000203 mixture Substances 0.000 claims abstract 4
- 150000008163 sugars Chemical class 0.000 claims abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 3
- 125000004432 carbon atom Chemical group C* 0.000 claims abstract 2
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000003350 kerosene Substances 0.000 claims abstract 2
- 238000007670 refining Methods 0.000 claims abstract 2
- SWZDQOUHBYYPJD-UHFFFAOYSA-N tridodecylamine Chemical group CCCCCCCCCCCCN(CCCCCCCCCCCC)CCCCCCCCCCCC SWZDQOUHBYYPJD-UHFFFAOYSA-N 0.000 claims abstract 2
- 238000005406 washing Methods 0.000 claims 2
- 150000001450 anions Chemical class 0.000 claims 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
- B01D15/1828—Simulated moving beds characterised by process features
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
- B01D15/361—Ion-exchange
- B01D15/362—Cation-exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/26—Cation exchangers for chromatographic processes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
- C07G1/00—Lignin; Lignin derivatives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0057—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid beta-D-Xylans, i.e. xylosaccharide, e.g. arabinoxylan, arabinofuronan, pentosans; (beta-1,3)(beta-1,4)-D-Xylans, e.g. rhodymenans; Hemicellulose; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H8/00—Macromolecular compounds derived from lignocellulosic materials
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/007—Separation of sugars provided for in subclass C13K
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0042—Fractionating or concentration of spent liquors by special methods
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0042—Fractionating or concentration of spent liquors by special methods
- D21C11/005—Treatment of liquors with ion-exchangers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C07H1/08—Separation; Purification from natural products
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P30/00—Technologies relating to oil refining and petrochemical industry
- Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Materials Engineering (AREA)
- Polymers & Plastics (AREA)
- Emergency Medicine (AREA)
- Sustainable Development (AREA)
- Molecular Biology (AREA)
- Biotechnology (AREA)
- Genetics & Genomics (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Saccharide Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Management, Administration, Business Operations System, And Electronic Commerce (AREA)
- Medicinal Preparation (AREA)
- Financial Or Insurance-Related Operations Such As Payment And Settlement (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
1. Способ рафинирования потока сахаров, содержащий(i) приведение потока сахаров в контакт с аминовым экстрагентом для образования смеси;(ii) отделение от смеси первого потока, содержащего аминовый экстрагент и кислоту или примесь; и второго потока, содержащего один или несколько сахаров.2. Способ по п. 1, в котором первый поток представляет собой органический поток, и второй поток представляет собой водный поток.3. Способ по п. 1, в котором первый поток содержит меньше, чем 0,5% вес/вес сахаров.4. Способ по п. 1, в котором второй поток содержит меньше, чем 0,5% вес/вес кислоты.5. Способ по п. 1, в котором второй поток содержит меньше, чем 0,5% вес/вес амина.6. Способ по п. 1, в котором второй поток содержит меньше, чем 0,5% вес/вес примесей.7. Способ по п. 1, в котором примеси экстрагируют из потока сахаров в аминовый экстрагент.8. Способ по п. 1, дополнительно содержащий перед стадией (i) приведение потока сахаров в контакт с сильнокислым катионообменником для удаления остаточных катионов.9. Способ по п. 1, в котором аминовый экстрагент содержит амин и разбавитель.10. Способ по п. 9, в котором соотношение амина и разбавителя составляет между 3:7 и 6:4.11. Способ по п. 9, в котором разбавитель содержит C6, C8, C10, C12, C14, C16 спирт или керосин.12. Способ по п. 9, в котором разбавитель содержит гексанол.13. Способ по п. 9, в котором амин представляет собой амин, содержащий по меньшей мере 20 атомов углерода.14. Способ по п. 9, в котором амин представляет собой трилауриламин.15. Способ по п. 1, дополнительно содержащий приведение потока сахаров в контакт с сильнокислым катионообменником для удаления остаточных аминов, посредством чего образуется очищенный от аминов гидролизат.16. Способ по п. 15, дополнительно содержащий приведение очищенного от аминов гидролизата в кон
Claims (21)
1. Способ рафинирования потока сахаров, содержащий
(i) приведение потока сахаров в контакт с аминовым экстрагентом для образования смеси;
(ii) отделение от смеси первого потока, содержащего аминовый экстрагент и кислоту или примесь; и второго потока, содержащего один или несколько сахаров.
2. Способ по п. 1, в котором первый поток представляет собой органический поток, и второй поток представляет собой водный поток.
3. Способ по п. 1, в котором первый поток содержит меньше, чем 0,5% вес/вес сахаров.
4. Способ по п. 1, в котором второй поток содержит меньше, чем 0,5% вес/вес кислоты.
5. Способ по п. 1, в котором второй поток содержит меньше, чем 0,5% вес/вес амина.
6. Способ по п. 1, в котором второй поток содержит меньше, чем 0,5% вес/вес примесей.
7. Способ по п. 1, в котором примеси экстрагируют из потока сахаров в аминовый экстрагент.
8. Способ по п. 1, дополнительно содержащий перед стадией (i) приведение потока сахаров в контакт с сильнокислым катионообменником для удаления остаточных катионов.
9. Способ по п. 1, в котором аминовый экстрагент содержит амин и разбавитель.
10. Способ по п. 9, в котором соотношение амина и разбавителя составляет между 3:7 и 6:4.
11. Способ по п. 9, в котором разбавитель содержит C6, C8, C10, C12, C14, C16 спирт или керосин.
12. Способ по п. 9, в котором разбавитель содержит гексанол.
13. Способ по п. 9, в котором амин представляет собой амин, содержащий по меньшей мере 20 атомов углерода.
14. Способ по п. 9, в котором амин представляет собой трилауриламин.
15. Способ по п. 1, дополнительно содержащий приведение потока сахаров в контакт с сильнокислым катионообменником для удаления остаточных аминов, посредством чего образуется очищенный от аминов гидролизат.
16. Способ по п. 15, дополнительно содержащий приведение очищенного от аминов гидролизата в контакт со слабоосновным анионообменником для образования нейтрализованного гидролизата.
17. Способ по любому из пп. 15 или 16, дополнительно содержащий фракционирование гидролизата на поток мономерных сахаров и поток олигомерных сахаров.
18. Способ по п. 1, дополнительно содержащий приведение первого потока в контакт с раствором основания для образования нейтрализованного аминового экстрагента.
19. Способ по п. 18, перед приведением первого потока в контакт с раствором основания дополнительно содержащий промывание первого потока с помощью водного потока для удаления сахара из третьего потока.
20. Способ по п. 19, в котором промытый первый поток содержит меньше, чем 0,1% вес/вес сахара.
21. Способ по п. 18, дополнительно содержащий промывание по меньшей мере части нейтрализованного аминового экстрагента с помощью воды и повторное использование промытого аминового экстрагента.
Applications Claiming Priority (27)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261642338P | 2012-05-03 | 2012-05-03 | |
| US61/642,338 | 2012-05-03 | ||
| US201261662830P | 2012-06-21 | 2012-06-21 | |
| US61/662,830 | 2012-06-21 | ||
| US201261672719P | 2012-07-17 | 2012-07-17 | |
| US61/672,719 | 2012-07-17 | ||
| US201261680183P | 2012-08-06 | 2012-08-06 | |
| US201261680181P | 2012-08-06 | 2012-08-06 | |
| US61/680,181 | 2012-08-06 | ||
| US61/680,183 | 2012-08-06 | ||
| US201261680661P | 2012-08-07 | 2012-08-07 | |
| US61/680,661 | 2012-08-07 | ||
| US201261681299P | 2012-08-09 | 2012-08-09 | |
| US61/681,299 | 2012-08-09 | ||
| US201261693637P | 2012-08-27 | 2012-08-27 | |
| US61/693,637 | 2012-08-27 | ||
| US201261715703P | 2012-10-18 | 2012-10-18 | |
| US61/715,703 | 2012-10-18 | ||
| US201261720313P | 2012-10-30 | 2012-10-30 | |
| US201261720325P | 2012-10-30 | 2012-10-30 | |
| US61/720,313 | 2012-10-30 | ||
| US61/720,325 | 2012-10-30 | ||
| US201361785891P | 2013-03-14 | 2013-03-14 | |
| US201361786169P | 2013-03-14 | 2013-03-14 | |
| US61/785,891 | 2013-03-14 | ||
| US61/786,169 | 2013-03-14 | ||
| PCT/US2013/039585 WO2013166469A2 (en) | 2012-05-03 | 2013-05-03 | Methods for treating lignocellulosic materials |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2014148431A true RU2014148431A (ru) | 2016-06-20 |
| RU2634700C2 RU2634700C2 (ru) | 2017-11-03 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2014148431A RU2634700C2 (ru) | 2012-05-03 | 2013-05-03 | Способы обработки лигноцеллюлозных материалов |
Country Status (11)
| Country | Link |
|---|---|
| US (5) | US9650687B2 (ru) |
| EP (4) | EP2847202B1 (ru) |
| JP (3) | JP6374861B2 (ru) |
| CN (5) | CN104411712A (ru) |
| AU (2) | AU2013256049B2 (ru) |
| BR (4) | BR112014027474B1 (ru) |
| CA (3) | CA3060976C (ru) |
| GB (4) | GB2535435B (ru) |
| RU (1) | RU2634700C2 (ru) |
| SG (1) | SG11201407183SA (ru) |
| WO (1) | WO2013166469A2 (ru) |
Families Citing this family (68)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL3401410T3 (pl) | 2010-06-26 | 2021-11-29 | Virdia, Llc | Sposoby wytwarzania mieszanek cukrów |
| IL206678A0 (en) | 2010-06-28 | 2010-12-30 | Hcl Cleantech Ltd | A method for the production of fermentable sugars |
| IL207945A0 (en) | 2010-09-02 | 2010-12-30 | Robert Jansen | Method for the production of carbohydrates |
| EP2694594A4 (en) | 2011-04-07 | 2015-11-11 | Virdia Ltd | METHODS AND PRODUCTS FOR LIGNOCELLULOSE CONVERSION |
| WO2013055785A1 (en) | 2011-10-10 | 2013-04-18 | Virdia Ltd | Sugar compositions |
| CN104411712A (zh) | 2012-05-03 | 2015-03-11 | 威尔迪亚有限公司 | 用于处理木质纤维素材料的方法 |
| US9493851B2 (en) | 2012-05-03 | 2016-11-15 | Virdia, Inc. | Methods for treating lignocellulosic materials |
| NZ743055A (en) | 2013-03-08 | 2020-03-27 | Xyleco Inc | Equipment protecting enclosures |
| US9657146B2 (en) | 2013-03-14 | 2017-05-23 | Virdia, Inc. | Methods for treating lignocellulosic materials |
| US9683005B2 (en) | 2013-05-03 | 2017-06-20 | Virdia, Inc. | Methods for preparing thermally stable lignin fractions |
| BR112015027744B1 (pt) * | 2013-05-03 | 2022-05-24 | Virdia, Llc | Composição de lignina e produto compreendendo a dita composição |
| WO2015034964A1 (en) | 2013-09-03 | 2015-03-12 | Virdia, Inc. | Methods for extracting and converting hemicellulose sugars |
| WO2015054736A1 (en) * | 2013-10-18 | 2015-04-23 | Queensland University Of Technology | Lignin-based waterproof coating |
| FI128419B (en) * | 2014-01-13 | 2020-04-30 | Upm Kymmene Corp | A method for separating lignocellulose particle fraction and lignin particle fraction |
| GB201406366D0 (en) | 2014-04-09 | 2014-05-21 | Plaxica Ltd | Biomass processing method |
| JP6687594B2 (ja) * | 2014-07-09 | 2020-04-22 | ヴァーディア， インコーポレイテッド | 黒液からリグニンを分離および精製する方法ならびにその組成物 |
| CA2959384C (en) * | 2014-08-29 | 2022-08-16 | University Of Tennessee Research Foundation | Comprehensive process for selectively separating lignocellulosic biomass into purified components with high yield |
| WO2016053209A1 (en) * | 2014-10-01 | 2016-04-07 | Ptt Global Chemical Public Company Limited | A pretreatment process of lignocellulosic biomass |
| KR20160062559A (ko) * | 2014-11-25 | 2016-06-02 | 씨제이제일제당 (주) | 경질 폴리우레탄 폼 및 이의 제조방법 |
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