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RU2005121263A - Мезопористые материалы с активными металлами - Google Patents

Мезопористые материалы с активными металлами Download PDF

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Publication number
RU2005121263A
RU2005121263A RU2005121263/04A RU2005121263A RU2005121263A RU 2005121263 A RU2005121263 A RU 2005121263A RU 2005121263/04 A RU2005121263/04 A RU 2005121263/04A RU 2005121263 A RU2005121263 A RU 2005121263A RU 2005121263 A RU2005121263 A RU 2005121263A
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Russia
Prior art keywords
group
heteroatom
feedstock
combinations
processing method
Prior art date
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RU2005121263/04A
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English (en)
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RU2334554C2 (ru
Inventor
Чжипин ШАНЬ (US)
Чжипин ШАНЬ
Якобус Корнелиус ЯНСЕН (NL)
Якобус Корнелиус ЯНСЕН
Чэнь И. ЕХ (US)
Чэнь И. ЕХ
Филип Дж. ЭНДЖИВАЙН (US)
Филип Дж. ЭНДЖИВАЙН
Томас МАШМЕЙЕР (NL)
Томас МАШМЕЙЕР
Мохаммед С. ХАМДИ (NL)
Мохаммед С. ХАМДИ
Original Assignee
Абб Ламмус Глобал, Инк. (Us)
Абб Ламмус Глобал, Инк.
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Publication of RU2005121263A publication Critical patent/RU2005121263A/ru
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Publication of RU2334554C2 publication Critical patent/RU2334554C2/ru

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • C10G2/331—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals
    • C10G2/332—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals of the iron-group
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Claims (36)

1. Способ обработки органических соединений, который содержит
а) обеспечение композиции, которая включает в себя, по существу, мезопористую структуру, образованную одним или несколькими материалами, выбранными из группы, состоящей из диоксида кремния, оксида алюминия, диоксида титана, оксида хрома, оксида железа, диоксида молибдена, причем указанная мезопористая структура содержит, по меньшей мере, 97 об.% пор, имеющих размер пор в интервале от примерно 15 до примерно 300 Е, и имеет объем микропор, по меньшей мере, примерно 0,01 см3/г, и где мезопористая структура имеет введенный в нее в количестве, по меньшей мере, примерно 0,02 мас.%, по меньшей мере, один каталитически и/или химически активный гетероатом, выбранный из группы, состоящей из Al, Ti, V, Cr, Zn, Fe, Sn, Mo, Ga, Ni, Co, In, Zr, Mn, Cu, Mg, Pd, Ru, W и их комбинаций, причем упомянутый катализатор имеет рентгенограмму с одним пиком от 0,3 до примерно 3,5° при 2;
b) взаимодействие исходного сырья, содержащего органическое соединение, в условиях реакции с упомянутым катализатором, при этом способ обработки выбирают из группы, состоящей из алкилирования, ацилирования, олигомеризации, селективного окисления, гидроочистки, изомеризации, деметаллирования, каталитической депарафинизации, гидроксилирования, гидрирования, аммоксимирования, дегидрирования, процесса Фишера-Тропша, крекинга и адсорбции.
2. Способ по п.1, в котором способ обработки представляет собой алкилирование, и в котором исходное сырье, содержащее органическое соединение, содержит ароматическое соединение либо алкан и алкилирующий агент.
3. Способ по п.2, в котором ароматическое соединение выбрано из группы, состоящей из бензола, нафталина, фенантрена, толуола, ксилола, изо-пропилнафталина, дифенилоксида и 2,4-ди-трет-бутилфенола.
4. Способ по п.3, в котором алкилирующий агент представляет собой олефин или спирт.
5. Способ по п.4, в котором, по меньшей мере, один гетероатом представляет собой Al и/или Ga.
6. Способ по п.5, в котором ароматическое соединение представляет собой нафталин или бензол и олефин представляет собой 1-гексадецен или этилен.
7. Способ по п.3, в котором алкилирующий агент представляет собой органический галогенид и в котором, по меньшей мере, один гетероатом выбран из группы, состоящей из Sn, Ga, Fe и их комбинаций.
8. Способ по п.7, в котором ароматическое соединение представляет собой бензол и органический галогенид представляет собой хлорбензол.
9. Способ по п.1, в котором способ обработки представляет собой селективное окисление, исходное сырье включает в себя окисляющий агент и, по меньшей мере, один гетероатом, выбранный из группы, состоящей из Cu, Zn, Fe, Ti, V, Sn, Mn, Cr, Mo и их комбинаций.
10. Способ по п.9, в котором, по меньшей мере, один гетероатом включает в себя, по меньшей мере, один атом, выбранный из группы, состоящей из Ti, Cr и Mo, исходное сырье включает в себя этилбензол, и в котором продукт, полученный в процессе селективного окисления, включает в себя ацетофенон.
11. Способ по п.9, в котором исходное сырье включает в себя спирт и, по меньшей мере, один гетероатом включает в себя Cu и/или Zn.
12. Способ по п.9, в котором органическое исходное сырье включает в себя циклогексанол, а продукт, получаемый в процессе селективного окисления, включает в себя циклогексанон.
13. Способ по п.1, в котором способ обработки представляет собой олигомеризацию, исходное сырье содержит, по меньшей мере, один олефин и, по меньшей мере, один гетероатом, выбранный из группы, состоящей из Al, Cr, Ga, Fe и их комбинаций.
14. Способ по п.13, в котором органическое исходное сырье включает в себя 1-децен и, по меньшей мере, один гетероатом включает в себя Al.
15. Способ по п.1, в котором способ обработки представляет собой ацилирование, исходное сырье содержит, по меньшей мере, одно ароматическое соединение и, по меньшей мере, один ацилирующий агент и, по меньшей мере, один гетероатом выбран из Al, Fe, Ga, In и их комбинаций.
16. Способ по п.15, в котором исходное сырье включает в себя 2-метоксинафталин и уксусный ангидрид.
17. Способ по п.1, в котором способ обработки включает в себя гидроочистку и, по меньшей мере, один гетероатом выбран из группы, состоящей из Ni, Mo, Co, W, Pt, Pd и их комбинаций.
18. Способ по п.17, в котором органическое исходное сырье включает в себя горючий сланец, или производную угольную жидкость, или остаточные нефтяные фракции, гидроочистка включает в себя один или несколько процессов из числа деазотирования, десульфирования, КУО-восстановления и деметаллирования.
19. Способ по п.18, в котором деметаллирование включает в себя удаление железа, никеля, меди, ванадия и мышьяка.
20. Способ по п.19, в котором исходное сырье представляет собой нефтяной остаток, гидроочистка включает в себя один или несколько процессов из числа деазотирования, десульфирования, деметаллирования и КУО-восстановления.
21. Способ по п.1, в котором способ обработки включает в себя крекинг.
22. Способ по п.21, в котором крекинг представляет собой гидрокрекинг и, по меньшей мере, один гетероатом включает в себя один или несколько металлов, выбранных из группы, состоящей из Ni, W, Mo, Co, Al и Ga.
23. Способ по п.20, в котором крекинг представляет собой каталитический крекинг и, по меньшей мере, один гетероатом включает в себя Al.
24. Способ по п.1, в котором способ обработки представляет собой каталитическую депарафинизацию и, по меньшей мере, один гетероатом включает в себя, по меньшей мере, один атом, выбранный из группы, состоящей из Al, Pt и Pd.
25. Способ по п.1, в котором способ обработки представляет собой гидроксилирование, по меньшей мере, один гетероатом выбран из группы, состоящей из Ti, Fe, Cu, Co, V, Cr и их комбинаций.
26. Способ по п.25, в котором исходное сырье содержит фенол и/или нафтол.
27. Способ по п.1, в котором способ обработки представляет собой изомеризацию и, по меньшей мере, один гетероатом выбран из группы, состоящей из Pd, Pt, Ni, Zr, W, Ga, Fe, Ti, Al и их комбинаций.
28. Способ по п.27, в котором исходное сырье включает в себя, по меньшей мере, один углеводород, выбранный из группы, состоящей из н-бутана, н-пентана, 1-бутена, ксилола и парафинистого нефтяного потока со средним числом атомов углерода большим, чем 20.
29. Способ по п.1, в котором способ обработки представляет собой дегидрирование и, по меньшей мере, один гетероатом выбран из группы, состоящей из V, Fe, Ga, Co, Cr и их комбинаций.
30. Способ по п.29, в котором исходное сырье включает в себя один или несколько насыщенных углеводородов.
31. Способ по п.29, в котором исходное сырье содержит один или несколько углеводородов, выбранных из группы, состоящей из пропана, изобутана и этилбензола.
32. Способ по п.1, в котором способ обработки представляет собой способ Фишера-Тропша и, по меньшей мере, один гетероатом выбран из группы, состоящей из Fe, Co, Ni и Ru и их сочетаний.
33. Способ по п.1, в котором катализатор взаимодействует с исходным сырьем, содержащим водород и монооксид углерода, при условиях: давление от примерно 5 до примерно 60 бар, предпочтительно от 8 до примерно 30 бар, ЧОСП от примерно 100 до примерно 10000 ч-1, предпочтительно от 300 ч-1 до примерно 2000 ч-1, температура от примерно 160 до примерно 300°С, предпочтительно от примерно 190 до примерно 260°С.
34. Способ по п.1, в котором композиция дополнительно включает в себя цеолит.
35. Каталитический материал, содержащий по существу мезопористую структуру, образованную одним или несколькими материалами, выбранными из группы, состоящей из диоксида кремния, оксида алюминия, диоксида титана, оксида хрома (III), оксида железа, диоксида молибдена, причем указанная мезопористая структура содержит, по меньшей мере, 97 об.% пор, имеющих размер пор в интервале от примерно 15 до примерно 300 Е, и имеет объем микропор, по меньшей мере, примерно 0,01 см3/г, и имеет площадь поверхности от 300 до примерно 1100 м2/г, и где мезопористая структура имеет введенный в нее, по меньшей мере, один каталитически и/или химически активный гетероатом, выбранный из группы, состоящей из Al, Ti, V, Cr, Zn, Fe, Sn, Mo, Ga, Ni, Co, In, Zr, Mn, Cu, Mg, Pd, Ru, W и их комбинаций в количестве, по меньшей мере, примерно 0,02 мас.%, причем упомянутый катализатор имеет рентгенограмму с одним пиком от 0,3° до примерно 3,5° при 2.
36. Каталитический материал по п.35, содержащий по существу мезопористую структуру, образованную одним или несколькими материалами, выбранными из группы, состоящей из диоксида кремния, оксида алюминия, диоксида титана, оксида хрома, оксида железа, диоксида молибдена, причем указанная мезопористая структура содержит, по меньшей мере, 97 об.% пор, имеющих размер пор в интервале от примерно 15 до примерно 300 Е и имеет дополнительно содержащий связующее вещество, выбранное из группы, состоящей из диоксида кремния, оксида алюминия, глины и их комбинации.
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