DE56866C - Procedure for uninterrupted10 E.xtxic.ti <50. by means of a Calou.u.e.i3Latj <j ^: a.te.s.- - ~ Dr - Google Patents
Procedure for uninterrupted10 E.xtxic.ti <50. by means of a Calou.u.e.i3Latj <j ^: a.te.s.- - ~ DrInfo
- Publication number
- DE56866C DE56866C DENDAT56866D DE56866DA DE56866C DE 56866 C DE56866 C DE 56866C DE NDAT56866 D DENDAT56866 D DE NDAT56866D DE 56866D A DE56866D A DE 56866DA DE 56866 C DE56866 C DE 56866C
- Authority
- DE
- Germany
- Prior art keywords
- extraction
- floor
- agitator
- continuously
- xtxic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title claims description 6
- 238000000605 extraction Methods 0.000 claims description 27
- 239000000463 material Substances 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000004927 clay Substances 0.000 claims description 2
- 229910052570 clay Inorganic materials 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- 229910052573 porcelain Inorganic materials 0.000 claims description 2
- 239000003921 oil Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 235000002639 sodium chloride Nutrition 0.000 description 2
- 210000002268 wool Anatomy 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- QGJOPFRUJISHPQ-NJFSPNSNSA-N carbon disulfide-14c Chemical compound S=[14C]=S QGJOPFRUJISHPQ-NJFSPNSNSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003502 gasoline Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/102—Production of fats or fatty oils from raw materials by extracting in counter-current; utilisation of an equipment wherein the material is conveyed by a screw
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
KLASSE 23: Fettindustrie.CLASS 23: Fat Industry.
Die bisher bekannten Extractions-Verfahren und -Apparate leiden an dem Mangel, dafs das Extractionsgut, sofern es nicht flüssig ist, von dem Extractionsmittel in den meisten Fällen schwer vollständig durchdrungen wird, weil es im Extractionsapparat zu dick und fest lagert. Durchdringt aber auch das Extractionsmittel das Extractionsgut, so bedarf es eines öfteren Kreislaufes, um das Gut vollständig zu extrahiren, und es kann daher eine Extraction immer nur mit einer bestimmten Menge Extractionsgut vorgenommen werden, nach dessen Extraction eine Pause eintreten mufs, um den Extractionsapparat zu entleeren und wieder neu zu füllen.The extraction methods and devices known to date suffer from the deficiency that the extraction material, if it is not liquid, of the extraction agent in most of them In cases it is difficult to penetrate completely because it is too thick and firm in the extraction apparatus stores. But if the extraction agent penetrates the extraction material, one is required frequent cycle in order to completely extract the material, and an extraction can therefore be carried out can only ever be made with a certain amount of extraction material, according to which Extraction a pause must occur in order to empty the extraction apparatus and then again to fill.
Diesem ersichtlichen Mangel wird durch die vorliegende Erfindung abgeholfen, indem durch dieselbe unter Anwendung eines eigenartig eingerichteten Colonnenapparates eine leichte, vollständige Durchdringung des Extractionsgutes mit dem Extractionsmittel und eine ununterbrochene Extraction ermöglicht wird.This apparent deficiency is remedied by the present invention by the same, with the use of a peculiarly arranged column apparatus, a light, complete one Penetration of the extraction material with the extraction agent and uninterrupted Extraction is made possible.
Der Colonnenapparat besteht aus einer beliebigen Anzahl runder Gefäfse aus Eisen, Porzellan, Thon oder sonstigem Material mit je einem Boden α und einem (oder mehreren) Zwischenböden b; die Gefäfse sind über einander angeordnet und dicht verbunden. Die Böden besitzen Oeffnungen, welche sich abwechselnd in der Mitte und am Umfange befinden. Durch die Mitte der Böden hindurch geht die Achse c eines Rührwerkes, an welcher sich Rührflügel, bestehend aus Rechen, Bürsten, Brettchen oder dergleichen, befinden, welche über je einen Boden streichen.The column apparatus consists of any number of round vessels made of iron, porcelain, clay or other material, each with a base α and one (or more) intermediate bases b; the vessels are arranged one above the other and tightly connected. The floors have openings, which are located alternately in the middle and on the periphery. The axis c of an agitator passes through the middle of the floors, on which there are agitator blades, consisting of rakes, brushes, boards or the like, which each sweep over a floor.
Wird nun oben (bei f) das Extractionsgut ununterbrochen in den Apparat eingebracht und gleichzeitig von unten, bei d, der Apparat mit dem Extractionsmittel gefüllt und durch ununterbrochenen Nachflufs gefüllt erhalten, so wird bei Bewegung des Rührwerkes das Extractionsgut nach und nach von einem Boden zum andern nach unten geführt, dabei von selbst fortwährend durch einander gemengt und mit dem Extractionsmittel in innigste Berührung gebracht. Infolge der Gegenströmung des Extractionsmittels gelangt dasselbe alsdann gesättigt oben an und fliefst bei e ununterbrochen ab, während das extrahirte Gut unten in den Raum A gelangt und bei g ebenfalls ununterbrochen abgeht.If the extraction material is now continuously introduced into the apparatus at the top (at f) and at the same time the apparatus is filled with the extraction medium from below, at d, and is kept filled by uninterrupted refilling, the extraction material is gradually moved from a floor to the bottom when the agitator is moved others led downwards, constantly mingling one another by themselves and brought into intimate contact with the extractant. As a result of the countercurrent of the extraction agent, it then arrives saturated at the top and flows off uninterruptedly at e , while the extracted material arrives at the bottom in space A and likewise leaves uninterruptedly at g.
Je naghdem eine Substanz leichter oder schwerer ausziehbar ist, wird die Colonne niedriger oder höher angeordnet und das Rührwerk schneller oder langsamer bewegt.The column becomes the easier or harder it is to pull out a substance placed lower or higher and the agitator moves faster or slower.
Zur Erzielung einer bestimmten, stets gleich bleibenden Temperatur während des Extrahirens wird der ganze Colonnenapparat mit einem Mantel umgeben, durch welchen bei h zufliefsend'es und bei i abfliefsendes Wasser oder unter Umständen auch Dampf von der erforderlichen Temperatur strömt.In order to achieve a certain, constant temperature during extraction, the entire column apparatus is surrounded by a jacket through which flows water flowing in at h and flowing out at i, or, under certain circumstances, steam at the required temperature.
Die Einrichtung des vorliegenden Apparates unterscheidet sich von den in den Patenten No. 24S00 und 2295 angegebenen Apparaten in folgenden Punkten:The setup of the present apparatus differs from that in the patents No. 24S00 and 2295 in the following points:
Bei den beiden letzteren bewegt sich je eine obere Scheibe über je eine gleichartige untere Scheibe, was zwar dem Zwecke, Gase mit Flüssigkeiten in innige Berührung zu bringen,In the latter two, an upper disk moves over a similar lower disk Disc, which is intended to bring gases into intimate contact with liquids,
entspricht, aber sich nicht zur Extraction von festen Substanzen, z. B. gemahlenem Oelsamen, eignet, welche sich nicht, wie das Salz im Patent No. 2295, in der zufliefsenden Flüssigkeit auflösen, sondern durch den ganzen Apparat hindurch ihren festen Zustand beibehalten und nur ihr OeI an die hindurchströmende Flüssigkeit: Benzin, Schwefelkohlenstoff, Aether oder dergleichen, abgeben. Auch wird dort das Extractionsmaterial nicht von einem Boden zum anderen abwärts befördert, wie es durch die Rührflügel des neuen Apparates geschieht. Abgesehen von dieser constructiven Verschiedenheit sind auch Zweck und Verfahren im vorliegenden Falle andere als in den Patenten No. 24600 und 2295. Bei letzteren handelt es sich nur um Gase und Flüssigkeiten, welche in innige Berührung mit einander gebracht werden sollen. In Patent No. 2295 kommt das Kochsalz nicht als fester Stoff in Betracht, da es sofort beim Einbringen in den Appaaat vom zufliefsenden Wasser aufgelöst wird.corresponds, but is not suitable for the extraction of solid substances, e.g. B. ground oil seed, which is not suitable, like the salt in patent no. 2295, in the inflowing liquid dissolve, but maintain their solid state throughout the entire apparatus and only your oil to the liquid flowing through it: gasoline, carbon disulfide, Ether or the like. The extraction material is not there either conveyed down one tray to the other as it is done by the impeller of the new one Apparatus happens. Apart from this constructive difference, there are also purposes and methods in the present case other than those described in patents no. 24600 and 2295. At the latter are only gases and liquids which are in intimate contact with to be brought to each other. In patent no. In 2295 table salt does not come as a solid Substance into consideration, as it is immediately dissolved by the inflowing water when it is introduced into the apparatus will.
Dahingegen bezweckt das angemeldete Verfahren, feste, gemahlene oder breiige Stoffe zu extrahiren, d. h. denselben einen Bestandlheil zu entziehen, nicht eine Mischung derselben mit einem anderen Stoff zu bewirken.In contrast, the notified process aims to produce solid, ground or pulpy substances extract, d. H. to withdraw a component from them, not a mixture of them to effect with another substance.
Das neue Verfahren kann zur Extraction von gemahlenem Oelsamen dienen, ferner zur Extraction von Droguen, Gewürzen, Harzen, Fetten, Oelen und fetthaltigen Schlammmassen, Knochen, gebrauchter Putzwolle, Wollabfällen u. dgl., gebrauchter Gasreinigungsmasse, Mineralien u. s. w., überhaupt allen zur Extraction geeigneten Stoffen.The new process can be used for the extraction of ground oil seeds, also for Extraction of drugs, spices, resins, fats, oils and fatty sludge masses, Bones, used cleaning wool, wool waste and the like, used gas cleaning compound, minerals and so on, generally all substances suitable for extraction.
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE56866C true DE56866C (en) |
Family
ID=331273
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT56866D Expired - Lifetime DE56866C (en) | Procedure for uninterrupted10 E.xtxic.ti <50. by means of a Calou.u.e.i3Latj <j ^: a.te.s.- - ~ Dr |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE56866C (en) |
-
0
- DE DENDAT56866D patent/DE56866C/en not_active Expired - Lifetime
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0076871A1 (en) | Apparatus and process for continuous solid-liquid extraction | |
| DE56866C (en) | Procedure for uninterrupted10 E.xtxic.ti <50. by means of a Calou.u.e.i3Latj <j ^: a.te.s.- - ~ Dr | |
| DE3329249A1 (en) | METHOD FOR EXTRACTION OF FORMABLE FLOWABLE MEASURES | |
| DE666880C (en) | Device for opening up and / or drying animal bodies, slaughterhouse waste, fish and the like. like | |
| DE637526C (en) | Device for washing and subsequent separation of liquids of different specific gravity | |
| DE2729937A1 (en) | DEVICE FOR TREATMENT OF SOUR CREAM | |
| DE83820C (en) | ||
| AT144004B (en) | Method and device for the intimate mixing of immiscible or not completely miscible liquids. | |
| DE577626C (en) | Device for the treatment of liquids with volatile extractants | |
| DE55052C (en) | Apparatus for extracting fats and other substances using volatile solvents | |
| DE69905140T2 (en) | DEVICE AND METHOD FOR CLEANING WORKPIECES | |
| DE696499C (en) | Extraction system, especially for the extraction of substances containing fat and oil | |
| AT95707B (en) | Method and device for the extraction of oil from flour-like vegetables. | |
| DE607120C (en) | Device for processing animal bodies | |
| DE732294C (en) | Device for extracting e.g. Oil, fat, wax | |
| DE744815C (en) | Device and method for distilling, especially high-boiling liquids | |
| DE956538C (en) | Self-filtering extraction device for vegetable oil | |
| DE628240C (en) | Method and device for leaching substances suspended in a solvent | |
| DE123659C (en) | ||
| DE870833C (en) | Method and device for separating fabrics by allowing columns of foam to drip out | |
| AT38743B (en) | Method and device for emulsifying or homogenizing milk, cream and similar liquids or liquid mixtures. | |
| DE73271C (en) | Method and apparatus for mixing fats with sulfuric acid | |
| DE860635C (en) | Method and arrangement for maintaining the bed height of a liquid-like layer of a finely divided solid substance in reaction vessels | |
| DE27333C (en) | Apparatus for extracting the paraffin from the mass used to decolorize the same | |
| DE156997C (en) |