DE1212509B - Verfahren zur Herstellung von beta-Chlor-beta'-cyan-diaethylaether - Google Patents
Verfahren zur Herstellung von beta-Chlor-beta'-cyan-diaethylaetherInfo
- Publication number
- DE1212509B DE1212509B DEC32941A DEC0032941A DE1212509B DE 1212509 B DE1212509 B DE 1212509B DE C32941 A DEC32941 A DE C32941A DE C0032941 A DEC0032941 A DE C0032941A DE 1212509 B DE1212509 B DE 1212509B
- Authority
- DE
- Germany
- Prior art keywords
- beta
- mol
- chloro
- hydroxide
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 title claims description 12
- 238000000034 method Methods 0.000 title claims description 6
- 238000002360 preparation method Methods 0.000 title claims description 3
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 19
- 229910001854 alkali hydroxide Inorganic materials 0.000 claims description 12
- SZIFAVKTNFCBPC-UHFFFAOYSA-N 2-chloroethanol Chemical compound OCCCl SZIFAVKTNFCBPC-UHFFFAOYSA-N 0.000 claims description 9
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 229910052801 chlorine Inorganic materials 0.000 claims 2
- 239000000460 chlorine Substances 0.000 claims 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- 235000011121 sodium hydroxide Nutrition 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 4
- 238000001816 cooling Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 229910000039 hydrogen halide Inorganic materials 0.000 description 2
- 239000012433 hydrogen halide Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 125000003700 epoxy group Chemical group 0.000 description 1
- JXBPSENIJJPTCI-UHFFFAOYSA-N ethyl cyanate Chemical compound CCOC#N JXBPSENIJJPTCI-UHFFFAOYSA-N 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical class ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH637663A CH451105A (de) | 1963-05-21 | 1963-05-21 | Verfahren zur Herstellung von B-Cyanäthyl-halogen-alkyläthern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1212509B true DE1212509B (de) | 1966-03-17 |
Family
ID=4308592
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEC32941A Pending DE1212509B (de) | 1963-05-21 | 1964-05-20 | Verfahren zur Herstellung von beta-Chlor-beta'-cyan-diaethylaether |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3297744A (es) |
| BE (1) | BE648168A (es) |
| CH (1) | CH451105A (es) |
| DE (1) | DE1212509B (es) |
| ES (1) | ES300037A1 (es) |
| GB (1) | GB1012891A (es) |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE743224C (de) * | 1940-05-19 | 1943-12-31 | Ig Farbenindustrie Ag | Verfahren zur Herstellung von Chloraethercarbonsaeurenitrilen |
| US2280792A (en) * | 1941-02-27 | 1942-04-28 | Resinous Prod & Chemical Co | Cyanoalkyl ethers of ether alcohols |
-
1963
- 1963-05-21 CH CH637663A patent/CH451105A/de unknown
-
1964
- 1964-04-17 GB GB16065/64A patent/GB1012891A/en not_active Expired
- 1964-04-30 US US364026A patent/US3297744A/en not_active Expired - Lifetime
- 1964-05-20 DE DEC32941A patent/DE1212509B/de active Pending
- 1964-05-20 BE BE648168A patent/BE648168A/xx unknown
- 1964-05-20 ES ES300037A patent/ES300037A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| GB1012891A (en) | 1965-12-08 |
| BE648168A (es) | 1964-11-20 |
| CH451105A (de) | 1968-05-15 |
| US3297744A (en) | 1967-01-10 |
| ES300037A1 (es) | 1964-11-16 |
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