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CN1368244A - Nano universal gynecologic medicine and its preparing process - Google Patents

Nano universal gynecologic medicine and its preparing process Download PDF

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Publication number
CN1368244A
CN1368244A CN 01102578 CN01102578A CN1368244A CN 1368244 A CN1368244 A CN 1368244A CN 01102578 CN01102578 CN 01102578 CN 01102578 A CN01102578 A CN 01102578A CN 1368244 A CN1368244 A CN 1368244A
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nanometer
parts
nano
part nanometer
chinese
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CN 01102578
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Chinese (zh)
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杨孟君
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Abstract

A nanometre (0.1-200 nm) medicine "Fuke Wanying" for treating gynopathy is prepared from the nanometre powders of 17 Chinese medicinal materials including sappan wood, Chuan-xiong rhizome, green tangerine peel, dried ginger, etc. through proportioning, microwave extracting, pressure reduction concentrating and supersonic-jet spray drying. Its grain fineness reaches 1200-1500 meshes and grain diameters are 0.1-200 nm. Its advantages are high biological utilization rate and high curative effect.

Description

Nano universal gynecologic medicine and preparation method thereof
The present invention relates to the nano universal gynecologic medicine of a kind of dispelling cold by warming the meridian, blood circulation promoting and blood stasis dispelling, regulating QI to relieve pain, the invention still further relates to the method for this medication preparation.
Universal gynecologic cream is a kind of classical Chinese patent medicine, mainly contains effects such as dispelling cold by warming the meridian, blood circulation promoting and blood stasis dispelling, regulating QI to relieve pain, and it is inferior to be used for the cold amenorrhea of menoxenia, abdominal pain in menstruation, abdomen, lumbago belt that the cold womb stasis causes.But traditional universal gynecologic cream absorbs not exclusively, and bioavailability is not high, slow curative effect.
The object of the present invention is to provide a kind of bioavailability height, solid dispersion is good, absorbs fully the nano universal gynecologic medicine of increase evident in efficacy.
Another object of the present invention provides the preparation method of this nano universal gynecologic medicine.
To achieve these goals, the present invention takes following technical scheme:
Medicine of the present invention is to make (consumption is a weight portion) by following component:
Nanometer Lignum Sappan 6-14 part nanometer Rhizoma Chuanxiong 12-24 part nanometer Pericarpium Citri Reticulatae Viride 6-14 part
Nanometer Radix Ampelopsis 12-24 part nanometer Rhizoma Zingiberis 6-14 part nanometer Caulis et Folium piperis 12-24 part
Nanometer Semen Trigonellae 6-14 part nanometer Herba Lycopi 10-35 part nanometer Fructus Foeniculi 6-14 part
Nanometer Fructus Leonuri 10-35 part nanometer Aspongopus 6-14 part nanometer Folium Artemisiae Argyi 15-35 part
Nano angelica root 6-14 part nanometer Rhizoma Bistortae 20-40 part nano safflower 6-14 part
Nano Chinese angelica 25-45 part nanometer Oleum Eucalypti 10-30 part
The formula optimization weight proportion scope of medicine of the present invention is:
Nanometer Lignum Sappan 8-12 part nanometer Rhizoma Chuanxiong 15-21 part nanometer Pericarpium Citri Reticulatae Viride 8-12 part
Nanometer Radix Ampelopsis 15-21 part nanometer Rhizoma Zingiberis 8-12 part nanometer Caulis et Folium piperis 15-21 part
Nanometer Semen Trigonellae 8-12 part nanometer Herba Lycopi 15-30 part nanometer Fructus Foeniculi 8-12 part
Nanometer Fructus Leonuri 15-30 part nanometer Aspongopus 8-12 part nanometer Folium Artemisiae Argyi 20-30 part
Nano angelica root 8-12 part nanometer Rhizoma Bistortae 25-35 part nano safflower 8-12 part
Nano Chinese angelica 30-40 part nanometer Oleum Eucalypti 15-25 part
The optimum weight proportioning of medicine of the present invention is:
9 parts on 18 parts of nanometer Pericarpium Citri Reticulatae Virides of 9 parts of nanometer Rhizoma Chuanxiongs of nanometer Lignum Sappan
18 parts of 9 parts of nanometer Caulis et Folium piperis of 18 parts of nanometer Rhizoma Zingiberiss of nanometer Radix Ampelopsis
9 parts of 21 parts of nanometer Fructus Foeniculi of 9 parts of nanometer Herba Lycopi of nanometer Semen Trigonellae
24 parts of 9 parts of nanometer Folium Artemisiae Argyis of 21 parts of nanometer Aspongopuss of nanometer Fructus Leonuri
9 parts of 27 parts of nano safflowers of 9 parts of nanometer Rhizoma Bistortaes of nano angelica root
20 parts of 36 parts of nanometer Oleum Eucalyptis of nano Chinese angelica
Technical scheme of the present invention is based on the modern material technology.One of modern material Developing Trend in Technology is to develop to the more and more littler direction of yardstick.The granule of the past composition material, its size all are at micron or more than the millimeter magnitude, and have occurred the material to the nanoscale development now.Because extremely refinement of granule, the shared percentage by volume of crystal boundary increases, and makes some performance of material that outstanding variation take place.
The property of nano material be since special construction----the material grains size of nano material less than the ultra-micro powder of 100nm, its body surface area is very big, the atom number ratio at crystal boundary place makes it to produce four big effects up to 15--50%: i.e. small-size effect, quantum effect (containing macro quanta tunnel effect), skin effect and interfacial effect.Thereby has the not available physical and chemical performance of traditional material.Nanotechnology will bring a technological revolution of the field of Chinese medicines.
One of method of above-mentioned each component being made medicine of the present invention is:
1. divide and get the Chinese crude drug of respectively distinguishing the flavor of, be processed into the common Chinese decoction pieces according to process of preparing Chinese medicine of Chinese Pharmacopoeia version in 2000.
2. divide and get the common Chinese decoction pieces of respectively distinguishing the flavor of, be processed into the nanometer prepared slices of Chinese crude drugs, its method comprises the following steps:
1. the common Chinese decoction pieces is placed extraction pot, solubilizer also imports microwave extracting, makes its speed with 20--30 hundred million times/second do the change in polarity motion, and the temperature of its microwave extracting is 30 ℃--and 60 ℃, time 1-10 hour;
2. above-mentioned extract is carried out concentrating under reduced pressure, temperature is 30 ℃--60 ℃, the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition;
3. decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 330 meters of effluxvelocities--990 meter per seconds, at 30 ℃--60 ℃ of temperature, under 0 to the 0.05MPa pressure,, promptly make the nanometer prepared slices of Chinese crude drugs with hypersonic velocity instantaneous jet drying.
3. the nanometer prepared slices of Chinese crude drugs (powder) are prepared mixing in described ratio, according to Chinese Pharmacopoeia version two-shift system in 2000 agent standard, make pill, powder, tablet, suppository, granule, membrane, capsule, microcapsule, drop pill, aerosol, injection, unguentum, medicated wine, syrup, oral solution.
Two of medicine method for making of the present invention is:
1. be equipped with whole common Chinese decoction pieces in the proportioning ratio, place extraction pot, solubilizer also imports microwave extracting, makes its speed with 20--30 hundred million times/second do the change in polarity motion, and the temperature of its microwave extracting is 30 ℃-60 ℃, time 1-10 hour;
2. above-mentioned extract is carried out concentrating under reduced pressure, temperature is 30 ℃--60 ℃, the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition;
3. decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 330 meters of effluxvelocities--990 meter per seconds, at 30 ℃--60 ℃ of temperature, under 0 to the 0.05MPa pressure,, get universal gynecologic preparation nano powder with hypersonic velocity instantaneous jet drying;
4. its nano powder is made aforementioned various preparation according to Chinese Pharmacopoeia version standard preparation in 2000.
The pharmacological effect that above-mentioned two kinds of methods are made nano universal gynecologic medicine is identical.
A kind of important feature of the present invention is: the made drug material of the present invention has reached nanoscale, common universal gynecologic paste formulation material is micron or the above particle diameter of millimeter, can only cross the 80-120 mesh sieve, the drug material that the present invention is made, particle diameter is at 0.1--200nm, the overwhelming majority can be crossed the 1200-1500 mesh sieve less than 100nm.
Another important feature of the present invention is: solid preparation of the present invention disintegrate rapidly, and solid dispersion is good in water, absorb fully, the bioavailability height, the pharmacological action effect that mainly contains effective constituent is significantly higher than conventional formulation.
The pharmaceutical preparation that the present invention is made does not need to add any adjuvant, and is more favourable to human body.
The present invention has also created the novel form that pill, powder, tablet, suppository, granule, membrane, capsule, microcapsule, drop pill, aerosol, injection, medicated wine, syrup, oral solution of nano universal gynecologic medicine etc. had no precedent in the past.
Pharmaceutical preparation of the present invention can be used for the cold amenorrhea of menoxenia, abdominal pain in menstruation, abdomen, the inferior treatment of conditions of lumbago belt that the cold womb stasis causes, clinical efficacy significantly is better than traditional universal gynecologic cream.
The present invention's added solvent in microwave extracting is water or ethanol.
The present invention carries out in the concentrating under reduced pressure step at extract, and its concentrating under reduced pressure is conventional scheme.
Embodiment 1:
Prepare nano raw material by preceding method:
9 parts on 18 parts of nanometer Pericarpium Citri Reticulatae Virides of 9 parts of nanometer Rhizoma Chuanxiongs of nanometer Lignum Sappan
18 parts of 9 parts of nanometer Caulis et Folium piperis of 18 parts of nanometer Rhizoma Zingiberiss of nanometer Radix Ampelopsis
9 parts of 21 parts of nanometer Fructus Foeniculi of 9 parts of nanometer Herba Lycopi of nanometer Semen Trigonellae
24 parts of 9 parts of nanometer Folium Artemisiae Argyis of 21 parts of nanometer Aspongopuss of nanometer Fructus Leonuri
9 parts of 27 parts of nano safflowers of 9 parts of nanometer Rhizoma Bistortaes of nano angelica root
20 parts of 36 parts of nanometer Oleum Eucalyptis of nano Chinese angelica
Production method is as follows:
In the GMP cleaning shop, after the above-mentioned nanometer prepared slices of Chinese crude drugs or powder prepared mixing in described ratio, according to Chinese Pharmacopoeia version two-shift system in 2000 agent capsules agent standard, do not add adjuvant, do not granulate, directly divide encapsulated with the fully-automatic capsule racking machine, make capsule, every capsules content of dispersion is the 0.1--0.6 gram, and the patient takes the 1-5 grain at every turn, and take 1-4 every day.
Embodiment 2:
Prepare nano raw material by preceding method:
9 parts on 18 parts of nanometer Pericarpium Citri Reticulatae Virides of 9 parts of nanometer Rhizoma Chuanxiongs of nanometer Lignum Sappan
18 parts of 9 parts of nanometer Caulis et Folium piperis of 18 parts of nanometer Rhizoma Zingiberiss of nanometer Radix Ampelopsis
9 parts of 21 parts of nanometer Fructus Foeniculi of 9 parts of nanometer Herba Lycopi of nanometer Semen Trigonellae
24 parts of 9 parts of nanometer Folium Artemisiae Argyis of 21 parts of nanometer Aspongopuss of nanometer Fructus Leonuri
9 parts of 27 parts of nano safflowers of 9 parts of nanometer Rhizoma Bistortaes of nano angelica root
20 parts of 36 parts of nanometer Oleum Eucalyptis of nano Chinese angelica
Production method is as follows:
In the GMP cleaning shop, with the above-mentioned nanometer prepared slices of Chinese crude drugs or the described mixed of powder good after, according to 2000 editions two-shift system agent of Chinese Pharmacopoeia powder needle injection standard, do not add any adjuvant, make the nano universal gynecologic powder needle injection, every injection content is the 5-20 milligram, each consumption is that 1-2 props up, and use 1-3 every day.
Embodiment 3:
Prepare nano raw material by preceding method:
9 parts on 18 parts of nanometer Pericarpium Citri Reticulatae Virides of 9 parts of nanometer Rhizoma Chuanxiongs of nanometer Lignum Sappan
18 parts of 9 parts of nanometer Caulis et Folium piperis of 18 parts of nanometer Rhizoma Zingiberiss of nanometer Radix Ampelopsis
9 parts of 21 parts of nanometer Fructus Foeniculi of 9 parts of nanometer Herba Lycopi of nanometer Semen Trigonellae
24 parts of 9 parts of nanometer Folium Artemisiae Argyis of 21 parts of nanometer Aspongopuss of nanometer Fructus Leonuri
9 parts of 27 parts of nano safflowers of 9 parts of nanometer Rhizoma Bistortaes of nano angelica root
20 parts of 36 parts of nanometer Oleum Eucalyptis of nano Chinese angelica
Production method is as follows:
In the GMP cleaning shop, with the above-mentioned nanometer prepared slices of Chinese crude drugs or powder by described mixed good after, according to 2000 editions two-shift system agent of Chinese Pharmacopoeia membrane standard, filmogen adopts polyvinyl alcohol, make the nano universal gynecologic membrane, every membrane area size is the 2-100 square centimeter, and content of dispersion is the 1-50 gram, every medicine film pasted 1-7 days, pasted the medicine position: abdominal part, back, chest.

Claims (6)

1, a kind of nano universal gynecologic medicine is characterized in that it is the medicament that the nano raw material of following weight proportioning is made:
Nanometer Lignum Sappan 6-14 part nanometer Rhizoma Chuanxiong 12-24 part nanometer Pericarpium Citri Reticulatae Viride 6-14 part
Nanometer Radix Ampelopsis 12-24 part nanometer Rhizoma Zingiberis 6-14 part nanometer Caulis et Folium piperis 12-24 part
Nanometer Semen Trigonellae 6-14 part nanometer Herba Lycopi 10-35 part nanometer Fructus Foeniculi 6-14 part
Nanometer Fructus Leonuri 10-35 part nanometer Aspongopus 6-14 part nanometer Folium Artemisiae Argyi 15-35 part
Nano angelica root 6-14 part nanometer Rhizoma Bistortae 20-40 part nano safflower 6-14 part
Nano Chinese angelica 25-45 part nanometer Oleum Eucalypti 10-30 part
And adopt following method to make: to select the formula Chinese drug material to concoct and be processed into the prepared slices of Chinese crude drugs; Place extraction pot, solubilizer also imports microwave extracting, makes it do the change in polarity motion with hundred million times/second speed of 20--30, and the temperature of its microwave extracting is 30--60 ℃, time 1-10 hour; Above-mentioned extract is carried out concentrating under reduced pressure, and temperature is 30--60 ℃, and the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition; Decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 30--60 ℃ of temperature, under 0 to the 0.05MPa pressure, with hypersonic velocity instantaneous jet drying, wherein supersonic jet speed is 330 meters-990 meter per seconds, promptly makes the nanometer prepared slices of Chinese crude drugs.
2, nano universal gynecologic medicine according to claim 1, wherein the weight proportion of each nano raw material is:
Nanometer Lignum Sappan 8-12 part nanometer Rhizoma Chuanxiong 15-21 part nanometer Pericarpium Citri Reticulatae Viride 8-12 part
Nanometer Radix Ampelopsis 15-21 part nanometer Rhizoma Zingiberis 8-12 part nanometer Caulis et Folium piperis 15-21 part
Nanometer Semen Trigonellae 8-12 part nanometer Herba Lycopi 15-30 part nanometer Fructus Foeniculi 8-12 part
Nanometer Fructus Leonuri 15-30 part nanometer Aspongopus 8-12 part nanometer Folium Artemisiae Argyi 20-30 part
Nano angelica root 8-12 part nanometer Rhizoma Bistortae 25-35 part nano safflower 8-12 part
Nano Chinese angelica 30-40 part nanometer Oleum Eucalypti 15-25 part
3, nano universal gynecologic medicine according to claim 1, wherein the weight proportion of each nano raw material is:
9 parts on 18 parts of nanometer Pericarpium Citri Reticulatae Virides of 9 parts of nanometer Rhizoma Chuanxiongs of nanometer Lignum Sappan
18 parts of 9 parts of nanometer Caulis et Folium piperis of 18 parts of nanometer Rhizoma Zingiberiss of nanometer Radix Ampelopsis
9 parts of 21 parts of nanometer Fructus Foeniculi of 9 parts of nanometer Herba Lycopi of nanometer Semen Trigonellae
24 parts of 9 parts of nanometer Folium Artemisiae Argyis of 21 parts of nanometer Aspongopuss of nanometer Fructus Leonuri
9 parts of 27 parts of nano safflowers of 9 parts of nanometer Rhizoma Bistortaes of nano angelica root
20 parts of 36 parts of nanometer Oleum Eucalyptis of nano Chinese angelica
4,, it is characterized in that said medicine is pill, powder, tablet, suppository, granule, membrane, capsule, microcapsule, drop pill, aerosol, injection, unguentum, medicated wine, syrup, oral solution according to claim 1 or 2 or 3 described nano universal gynecologic medicines.
5,, it is characterized in that this method comprises the steps: to select the formula Chinese drug material to concoct and is processed into the prepared slices of Chinese crude drugs according to the pharmaceutical methods of claim 1 or 2 or 3 described nano universal gynecologic medicines; Place extraction pot, solubilizer also imports microwave extracting, makes it do the change in polarity motion with hundred million times/second speed of 20--30, and the temperature of its microwave extracting is 30--60 ℃, time 1-10 hour; Above-mentioned extract is carried out concentrating under reduced pressure, and temperature is 30--60 ℃, and the time is 3-72 hour, collects volatile material in the Chinese medicine simultaneously in addition; Decompressed concentrate and volatile material merging are placed spray drying tower, use the supersonic jet technology, 30--60 ℃ of temperature, under 0 to the 0.05MPa pressure, with hypersonic velocity instantaneous jet drying, wherein supersonic jet speed is 330 meters-990 meter per seconds, promptly makes the nanometer prepared slices of Chinese crude drugs.
6, wherein respectively distinguish the flavor of Chinese medicine in the ratio of prescription or Chinese crude drug concoct be processed into the prepared slices of Chinese crude drugs after mixing, or after making the nanometer prepared slices of Chinese crude drugs mixing.
CN 01102578 2001-02-01 2001-02-01 Nano universal gynecologic medicine and its preparing process Pending CN1368244A (en)

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100413515C (en) * 2005-08-31 2008-08-27 张瑞友 Chinese medicine composition for treating male's sterility and its prepn
CN102218129A (en) * 2010-08-13 2011-10-19 辽宁玉皇药业有限公司 New drug delivery system of gynaecologic panchrest plaster
CN107670014A (en) * 2017-11-21 2018-02-09 安徽金马药业有限公司 A kind of universal gynecologic cream medicinal extract and its preparation technology

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100413515C (en) * 2005-08-31 2008-08-27 张瑞友 Chinese medicine composition for treating male's sterility and its prepn
CN102218129A (en) * 2010-08-13 2011-10-19 辽宁玉皇药业有限公司 New drug delivery system of gynaecologic panchrest plaster
CN107670014A (en) * 2017-11-21 2018-02-09 安徽金马药业有限公司 A kind of universal gynecologic cream medicinal extract and its preparation technology

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