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AR057032A1 - Tigeciclina y metodos de preparacion - Google Patents

Tigeciclina y metodos de preparacion

Info

Publication number
AR057032A1
AR057032A1 ARP060102154A ARP060102154A AR057032A1 AR 057032 A1 AR057032 A1 AR 057032A1 AR P060102154 A ARP060102154 A AR P060102154A AR P060102154 A ARP060102154 A AR P060102154A AR 057032 A1 AR057032 A1 AR 057032A1
Authority
AR
Argentina
Prior art keywords
compound
methods
branched
alkyl
preparing
Prior art date
Application number
ARP060102154A
Other languages
English (en)
Original Assignee
Wyeth Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wyeth Corp filed Critical Wyeth Corp
Publication of AR057032A1 publication Critical patent/AR057032A1/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C237/00Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups
    • C07C237/24Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atom of at least one of the carboxamide groups bound to a carbon atom of a ring other than a six-membered aromatic ring of the carbon skeleton
    • C07C237/26Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atom of at least one of the carboxamide groups bound to a carbon atom of a ring other than a six-membered aromatic ring of the carbon skeleton of a ring being part of a condensed ring system formed by at least four rings, e.g. tetracycline
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/65Tetracyclines
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/04Antibacterial agents
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00Preparation of carboxylic acid amides
    • C07C231/02Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00Systems containing at least three condensed rings
    • C07C2603/02Ortho- or ortho- and peri-condensed systems
    • C07C2603/40Ortho- or ortho- and peri-condensed systems containing four condensed rings
    • C07C2603/42Ortho- or ortho- and peri-condensed systems containing four condensed rings containing only six-membered rings
    • C07C2603/44Naphthacenes; Hydrogenated naphthacenes
    • C07C2603/461,4,4a,5,5a,6,11,12a- Octahydronaphthacenes, e.g. tetracyclines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Medicinal Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Oncology (AREA)
  • Communicable Diseases (AREA)
  • Epidemiology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

Se revelan en la presente métodos para preparar y purificar tetraciclinas, tales como tigeciclina. También se revelan composiciones de tetraciclina, tales como composiciones de tigeciclina, preparadas mediante estos métodos. Reivindicacion 1: Un método para preparar al menos un compuesto de formula (1) o una sal aceptable para uso farmacéutico del mismo, donde R1 y R2 se seleccionan cada uno en forma independiente de H, alquilo C1-6 de cadena recta y ramificada, y cicloalquilo, o R1 y R2, junto con N, forman un heterociclo; R es -NR3R4, donde R3 y R4 se seleccionan cada uno en forma independiente de H, alquilo C1-4 de cadena recta o ramificada; y n oscila entre 1-4, que comprende hacer reaccionar al menos un compuesto de formula (4) o una sal del mismo, con al menos un compuesto con grupo aminoacilo en un medio de reaccion seleccionado de un medio acuoso, y al menos un solvente básico en ausencia de una base reactiva.
ARP060102154A 2005-05-27 2006-05-24 Tigeciclina y metodos de preparacion AR057032A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US68528505P 2005-05-27 2005-05-27

Publications (1)

Publication Number Publication Date
AR057032A1 true AR057032A1 (es) 2007-11-14

Family

ID=37023025

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP060102154A AR057032A1 (es) 2005-05-27 2006-05-24 Tigeciclina y metodos de preparacion

Country Status (21)

Country Link
US (1) US20070049562A1 (es)
EP (1) EP1888507A1 (es)
JP (1) JP2008545701A (es)
KR (1) KR20080015470A (es)
CN (1) CN101228112A (es)
AR (1) AR057032A1 (es)
AU (1) AU2006252783A1 (es)
BR (1) BRPI0610648A2 (es)
CA (1) CA2609306A1 (es)
CR (1) CR9541A (es)
EC (1) ECSP078059A (es)
GT (1) GT200600221A (es)
IL (1) IL187360A0 (es)
MX (1) MX2007014731A (es)
NI (1) NI200700301A (es)
NO (1) NO20076001L (es)
PE (1) PE20070009A1 (es)
RU (1) RU2007143157A (es)
TW (1) TW200718676A (es)
WO (1) WO2006130418A1 (es)
ZA (1) ZA200710153B (es)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR057649A1 (es) * 2005-05-27 2007-12-12 Wyeth Corp Formas solidas cristalinas de tigeciclina y metodos para preparar las mismas
US20070244335A1 (en) * 2006-04-17 2007-10-18 Teva Pharmaceutical Industries Ltd. Isolation of tetracycline derivatives
DE202007019460U1 (de) * 2006-04-24 2012-10-24 Teva Pharmaceutical Industries Ltd. Kristalline Tigecyclin-Formen
US8198470B2 (en) * 2006-04-24 2012-06-12 Teva Pharmaceutical Industries Ltd. Crystalline form II of tigecycline and processes for preparation thereof
US8198469B2 (en) * 2006-11-29 2012-06-12 Teva Pharmaceutical Industries Ltd. Crystalline forms of tigecycline and processes for preparation thereof
BRPI0706517A2 (pt) * 2006-11-30 2011-03-29 Teva Pharma processos para preparação de f 9-haloacetamidominociclinas
WO2008106234A1 (en) * 2007-03-01 2008-09-04 Teva Pharmaceutical Industries Ltd. Processes for purification of tigecycline
US20090099376A1 (en) * 2007-10-16 2009-04-16 Wyeth Tigecycline and methods of preparing intermediates
ES2532880T3 (es) 2007-11-14 2015-04-01 Sandoz Ag Formas cristalinas del Clorhidrato de Tigeciclina
US20110124893A1 (en) * 2008-01-23 2011-05-26 Sandoz Ag Antibiotic compounds
WO2010032219A1 (en) * 2008-09-18 2010-03-25 Ranbaxy Laboratories Limited Process for the preparation of tigecycline
CA2746585C (en) 2008-12-18 2017-08-29 Sandoz Ag Crystalline form c of tigecycline dihydrochloride and methods for its preparation
CA2751238A1 (en) 2009-03-12 2010-10-07 Wyeth Llc Nitration of tetracyclines
ES2469829T3 (es) * 2009-11-26 2014-06-20 Sandoz Ag Reacción de compuestos orgánicos con bajas cantidades de hidrógeno
CN102821769A (zh) * 2010-03-10 2012-12-12 大学健康网络 替加环素用于治疗癌症的用途
CN102276497A (zh) * 2010-06-10 2011-12-14 武汉启瑞药业有限公司 替加环素的合成方法
CN102746183B (zh) * 2011-04-20 2014-12-17 胡梨芳 替加环素结晶水合物及其制备方法和用途
DK2900634T3 (en) 2012-09-27 2017-05-22 Bayer Cropscience Ag PROCEDURE FOR PREPARING SUBSTITUTED SUBSTITUTED PHENYL AND PYRIDYLPYRROLIDINES
CN102911077B (zh) * 2012-11-12 2015-01-07 成都百裕科技制药有限公司 4r-替加环素的制备方法
CN103044281A (zh) * 2013-01-02 2013-04-17 湖南赛隆药业有限公司 高纯度替加环素的制法
CN104230744B (zh) * 2014-09-01 2016-06-08 湖南尔康制药股份有限公司 一种替加环素原料药的生产方法
CN107365359B (zh) * 2017-07-17 2021-06-04 昆明理工大学 一种万古霉素手性功能单体合成方法
WO2019160037A1 (ja) * 2018-02-14 2019-08-22 国立大学法人 東京大学 酸ハロゲン化物による化合物の製造方法

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US3043875A (en) * 1959-10-22 1962-07-10 Pfizer & Co C Halogenated tetracycline derivatives and processes for their preparation
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Also Published As

Publication number Publication date
NI200700301A (es) 2008-07-24
BRPI0610648A2 (pt) 2010-07-13
WO2006130418A1 (en) 2006-12-07
PE20070009A1 (es) 2007-01-29
US20070049562A1 (en) 2007-03-01
RU2007143157A (ru) 2009-07-10
CR9541A (es) 2008-02-20
ECSP078059A (es) 2008-01-23
TW200718676A (en) 2007-05-16
AU2006252783A1 (en) 2006-12-07
IL187360A0 (en) 2008-04-13
KR20080015470A (ko) 2008-02-19
MX2007014731A (es) 2008-02-15
CA2609306A1 (en) 2006-12-07
ZA200710153B (en) 2009-08-26
EP1888507A1 (en) 2008-02-20
CN101228112A (zh) 2008-07-23
GT200600221A (es) 2009-08-28
NO20076001L (no) 2008-02-19
JP2008545701A (ja) 2008-12-18

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