MX2017015606A - Proceso para preparar 3-metilciclopentadecan-1,5-diona. - Google Patents
Proceso para preparar 3-metilciclopentadecan-1,5-diona.Info
- Publication number
- MX2017015606A MX2017015606A MX2017015606A MX2017015606A MX2017015606A MX 2017015606 A MX2017015606 A MX 2017015606A MX 2017015606 A MX2017015606 A MX 2017015606A MX 2017015606 A MX2017015606 A MX 2017015606A MX 2017015606 A MX2017015606 A MX 2017015606A
- Authority
- MX
- Mexico
- Prior art keywords
- dione
- formula
- methylcyclopentadecane
- preparing
- oxidation
- Prior art date
Links
- FRTDAFYYAIXLRJ-UHFFFAOYSA-N 3-methylcyclopentadecane-1,5-dione Chemical compound CC1CC(=O)CCCCCCCCCCC(=O)C1 FRTDAFYYAIXLRJ-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 abstract 2
- 239000007800 oxidant agent Substances 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- FZZSWFPKTUMIPD-UHFFFAOYSA-N 2-methyl-2,3,5,6,7,8,9,10,11,12,13,13a-dodecahydro-1H-cyclopenta[12]annulene Chemical compound CC1CC2CCCCCCCCCC=C2C1 FZZSWFPKTUMIPD-UHFFFAOYSA-N 0.000 abstract 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 235000019253 formic acid Nutrition 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/28—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/385—Saturated compounds containing a keto group being part of a ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La presente invención se refiere a un proceso para producir 3-metilciclopentadecan-1,5-diona de la Fórmula (I), que comprende la oxidación de 14-metilbiciclo[10.3.0]pentadecen[1(12)] de la Fórmula (II) con un agente oxidante, en donde la oxidación se lleva a cabo usando una mezcla de ácido fórmico con H2O2 como único agente oxidante en presencia de agua y en donde la cantidad de H2O2 es al menos 1,1 mol de H2O2 por mol del compuesto de la Fórmula (II). (ver Fórmulas).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP15170490 | 2015-06-03 | ||
| PCT/EP2016/062434 WO2016193330A1 (en) | 2015-06-03 | 2016-06-02 | Process for preparing 3-methylcyclopentadecane-1,5-dione |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2017015606A true MX2017015606A (es) | 2018-04-24 |
| MX384710B MX384710B (es) | 2025-03-14 |
Family
ID=53385503
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2017015606A MX384710B (es) | 2015-06-03 | 2016-06-02 | Proceso para preparar 3-metilciclopentadecan-1,5-diona. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10053409B2 (es) |
| EP (1) | EP3303278B1 (es) |
| JP (1) | JP6789989B6 (es) |
| CN (1) | CN107709283B (es) |
| ES (1) | ES2806203T3 (es) |
| MX (1) | MX384710B (es) |
| WO (1) | WO2016193330A1 (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3170828A1 (de) * | 2015-11-23 | 2017-05-24 | Basf Se | Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten |
| WO2017140909A1 (de) | 2016-02-19 | 2017-08-24 | Basf Se | Enzymatische zyklisierung von homofarnesylsäure |
| US10981885B2 (en) | 2016-05-31 | 2021-04-20 | Basf Se | Tetrahydropyranyl lower alkyl esters and the production of same using a ketene compound |
| WO2018011386A1 (en) | 2016-07-15 | 2018-01-18 | Basf Se | Preparation of 14-methyl-16-oxabicyclo[10.3.1]pentadecenes from 3-methyl-1,5-cyclopentadecanedione |
| JP7707121B2 (ja) * | 2022-03-31 | 2025-07-14 | 花王株式会社 | 環状ジケトン化合物の製造方法 |
| JP7738514B2 (ja) * | 2022-03-31 | 2025-09-12 | 花王株式会社 | 環状ジケトン化合物の製造方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH519454A (de) | 1966-02-08 | 1972-02-29 | Firmenich & Cie | Verfahren zur Herstellung von makrocyclischen Verbindungen |
| CH513791A (de) * | 1966-12-08 | 1971-10-15 | Firmenich & Cie | Verfahren zur Herstellung von makrocyclischen Verbindungen |
| CH482637A (de) | 1966-11-01 | 1969-12-15 | Eschenmoser Albert Dr Prof | Verfahren zur Herstellung von Acetylenverbindungen |
| CH503680A (de) | 1966-12-08 | 1971-02-28 | Firmenich & Cie | Verfahren zur Herstellung von makrocyclischen Ketonen |
| GB1232010A (es) | 1967-09-04 | 1971-05-19 | ||
| DE2916418A1 (de) | 1979-04-23 | 1980-11-06 | Basf Ag | Verfahren zur herstellung von 14- methyl-bicyclo- eckige klammer auf 10.3.0. eckige klammer zu -pentadecen- eckige klammer auf 1(12) eckige klammer zu und neue zwischenprodukte dieses verfahrens |
| CN100494148C (zh) * | 2006-09-15 | 2009-06-03 | 济南宏济堂制药有限责任公司 | 4-甲基环十五烷酮及应用 |
| MX2013003752A (es) * | 2010-10-07 | 2013-12-02 | Basf Se | Proceso para la preparación de cetonas, en particular cetonas macrociclicas. |
| CN102786398A (zh) | 2012-08-30 | 2012-11-21 | 新乡医学院 | 一种经济环保的高纯度麝香酮规模化生产工艺 |
| CN107001214B (zh) * | 2014-12-26 | 2021-03-23 | 花王株式会社 | 环状二酮化合物的制造方法 |
| ES2775502T3 (es) | 2015-05-20 | 2020-07-27 | Basf Se | Procedimiento de preparación de una dicetona macrocíclica |
-
2016
- 2016-06-02 WO PCT/EP2016/062434 patent/WO2016193330A1/en not_active Ceased
- 2016-06-02 JP JP2017562770A patent/JP6789989B6/ja active Active
- 2016-06-02 EP EP16726323.5A patent/EP3303278B1/en active Active
- 2016-06-02 US US15/578,959 patent/US10053409B2/en active Active
- 2016-06-02 CN CN201680032030.8A patent/CN107709283B/zh active Active
- 2016-06-02 MX MX2017015606A patent/MX384710B/es unknown
- 2016-06-02 ES ES16726323T patent/ES2806203T3/es active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN107709283B (zh) | 2021-02-02 |
| US10053409B2 (en) | 2018-08-21 |
| CN107709283A (zh) | 2018-02-16 |
| JP2018516271A (ja) | 2018-06-21 |
| JP6789989B2 (ja) | 2020-11-25 |
| EP3303278A1 (en) | 2018-04-11 |
| WO2016193330A1 (en) | 2016-12-08 |
| EP3303278B1 (en) | 2020-04-22 |
| JP6789989B6 (ja) | 2020-12-16 |
| ES2806203T3 (es) | 2021-02-16 |
| MX384710B (es) | 2025-03-14 |
| US20180179136A1 (en) | 2018-06-28 |
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