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WO2009022676A1 - 五フッ化リン及び六フッ化リン酸塩の製造方法 - Google Patents

五フッ化リン及び六フッ化リン酸塩の製造方法 Download PDF

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Publication number
WO2009022676A1
WO2009022676A1 PCT/JP2008/064392 JP2008064392W WO2009022676A1 WO 2009022676 A1 WO2009022676 A1 WO 2009022676A1 JP 2008064392 W JP2008064392 W JP 2008064392W WO 2009022676 A1 WO2009022676 A1 WO 2009022676A1
Authority
WO
WIPO (PCT)
Prior art keywords
solution
phosphorus pentafluoride
hexafluorophosphate
phosphorus
pentavalent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/064392
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English (en)
French (fr)
Inventor
Masahide Waki
Shinji Hashiguchi
Kazutaka Hirano
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stella Chemifa Corp
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Stella Chemifa Corp
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Filing date
Publication date
Application filed by Stella Chemifa Corp filed Critical Stella Chemifa Corp
Priority to EP08792375A priority Critical patent/EP2189418A4/en
Priority to KR1020107005691A priority patent/KR101519683B1/ko
Priority to CA2696544A priority patent/CA2696544C/en
Priority to CN200880102790A priority patent/CN101778793A/zh
Priority to US12/673,058 priority patent/US9034290B2/en
Publication of WO2009022676A1 publication Critical patent/WO2009022676A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/04—Construction or manufacture in general
    • H01M10/0422—Cells or battery with cylindrical casing
    • H01M10/0427—Button cells
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/10—Halides or oxyhalides of phosphorus
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/455—Phosphates containing halogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/005—Lithium hexafluorophosphate
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/04—Construction or manufacture in general
    • H01M10/0413—Large-sized flat cells or batteries for motive or stationary systems with plate-like electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/04—Construction or manufacture in general
    • H01M10/0468—Compression means for stacks of electrodes and separators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566—Liquid materials
    • H01M10/0568—Liquid materials characterised by the solutes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/582—Halogenides
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/42—Methods or arrangements for servicing or maintenance of secondary cells or secondary half-cells
    • H01M10/44—Methods for charging or discharging
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Secondary Cells (AREA)

Abstract

　５価のリン化合物若しくはその溶液、又は前記５価のリン化合物若しくはその溶液とフッ化水素とを反応させて得られた組成物から五フッ化リンを分離・抽出して当該五フッ化リンを製造する五フッ化リンの製造方法、及び得られた五フッ化リンを原料として純度の高い六フッ化リン酸塩を製造する六フッ化リン酸塩の製造方法を提供する。本発明の五フッ化リンの製造方法は、５価のリン化合物若しくはその溶液、又は前記５価のリン化合物若しくはその溶液とフッ化水素とを反応させて得られた組成物を溶解させた溶液にキャリアガスを接触させることにより、前記キャリアガス中に五フッ化リンを抽出させて分離することを特徴とする。
PCT/JP2008/064392 2007-08-16 2008-08-11 五フッ化リン及び六フッ化リン酸塩の製造方法 Ceased WO2009022676A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP08792375A EP2189418A4 (en) 2007-08-16 2008-08-11 PROCESS FOR PRODUCING PHOSPHORUS PENTAFLUORIDE AND HEXAFLUOROPHOSPHATE
KR1020107005691A KR101519683B1 (ko) 2007-08-16 2008-08-11 ５불화인 및 ６불화인산염의 제조방법
CA2696544A CA2696544C (en) 2007-08-16 2008-08-11 Processes for producing phosphorus tetrafluoride and phosphate hexafluoride
CN200880102790A CN101778793A (zh) 2007-08-16 2008-08-11 五氟化磷和六氟磷酸盐的制造方法
US12/673,058 US9034290B2 (en) 2007-08-16 2008-08-11 Processes for producing phosphorus pentafluoride and phosphate hexafluoride

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2007212277 2007-08-16
JP2007-212277 2007-08-16
JP2008009484A JP5307409B2 (ja) 2007-08-16 2008-01-18 五フッ化リン及び六フッ化リン酸塩の製造方法
JP2008-009484 2008-01-18

Publications (1)

Publication Number Publication Date
WO2009022676A1 true WO2009022676A1 (ja) 2009-02-19

Family

ID=40350728

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/064392 Ceased WO2009022676A1 (ja) 2007-08-16 2008-08-11 五フッ化リン及び六フッ化リン酸塩の製造方法

Country Status (9)

Country Link
US (1) US9034290B2 (ja)
EP (1) EP2189418A4 (ja)
JP (1) JP5307409B2 (ja)
KR (1) KR101519683B1 (ja)
CN (3) CN103058155A (ja)
CA (1) CA2696544C (ja)
SG (1) SG183730A1 (ja)
TW (1) TWI455872B (ja)
WO (1) WO2009022676A1 (ja)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010105120A3 (en) * 2009-03-13 2011-01-13 Honeywell International Inc. Methods and reactor designs for producing phosphorus pentafluoride
JP2013531606A (ja) * 2010-06-30 2013-08-08 ハネウェル・インターナショナル・インコーポレーテッド ＨＦを用いるＡｓＦ５及びＰＦ５の抽出蒸留
JP5532181B1 (ja) * 2013-10-31 2014-06-25 Ｊｏｉｎｔエンジニアリング株式会社 リチウム電池及び／又はリチウムイオン電池の電解質用リチウム塩の製造方法及び製造装置
US9731968B2 (en) 2008-08-08 2017-08-15 Stella Chemifa Corporation Process for producing fluoride gas

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JP5254555B2 (ja) * 2007-02-08 2013-08-07 ステラケミファ株式会社 五フッ化リン及び六フッ化リン酸塩の製造方法
JP5307409B2 (ja) 2007-08-16 2013-10-02 ステラケミファ株式会社 五フッ化リン及び六フッ化リン酸塩の製造方法
JP2010042937A (ja) * 2008-08-08 2010-02-25 Stella Chemifa Corp 五フッ化リン及び六フッ化リン酸塩の製造方法
US20130004402A1 (en) * 2011-06-28 2013-01-03 Honeywell International Inc. Methods and apparatuses for purifying phosphorus pentafluoride
WO2014097861A1 (ja) * 2012-12-20 2014-06-26 Ｊｏｉｎｔエンジニアリング株式会社 リチウム電池及び／又はリチウムイオン電池の電解質用リチウム塩の製造方法及び製造装置
JP5824013B2 (ja) * 2013-08-21 2015-11-25 ステラケミファ株式会社 五フッ化リン及び六フッ化リン酸塩の製造方法
JP5865314B2 (ja) * 2013-08-21 2016-02-17 ステラケミファ株式会社 五フッ化リン及び六フッ化リン酸塩の製造方法
US9975771B2 (en) 2013-10-04 2018-05-22 Kanto Denka Kogyo Co., Ltd. Process for purifying phosphorus pentafluoride
JP6380883B2 (ja) * 2013-10-16 2018-08-29 ナガセケムテックス株式会社 正極合材及びその製造方法、並びに、全固体型リチウム硫黄電池
WO2018168752A1 (ja) * 2017-03-13 2018-09-20 関東電化工業株式会社 五フッ化リンの製造方法
US10875781B2 (en) 2018-03-28 2020-12-29 Gene Lee Hunsucker Phosphorus pentafluoride reactions
CN110911752A (zh) * 2019-12-06 2020-03-24 广州天赐高新材料股份有限公司 一种低内阻的锂二次电池电解液及锂二次电池
CN111410182A (zh) * 2020-03-31 2020-07-14 福建省龙德新能源股份有限公司 一种回用六氟磷酸锂合成尾气中五氟化磷的方法
CN111439735A (zh) * 2020-03-31 2020-07-24 福建省龙德新能源股份有限公司 一种利用胺及其衍生物回用六氟磷酸锂合成尾气中五氟化磷的方法
CN111320154A (zh) * 2020-03-31 2020-06-23 福建省龙德新能源股份有限公司 一种利用酯及其衍生物回用六氟磷酸锂合成尾气中五氟化磷的方法
CN111285340A (zh) * 2020-03-31 2020-06-16 福建省龙德新能源股份有限公司 一种利用碳酸二乙基酯回用六氟磷酸锂合成尾气中五氟化磷的方法
CN111410181A (zh) * 2020-03-31 2020-07-14 福建省龙德新能源股份有限公司 一种利用醚及其衍生物回用六氟磷酸锂合成尾气中五氟化磷的方法
CN116282085B (zh) * 2021-12-20 2025-03-14 浙江蓝天环保高科技股份有限公司 一种六氟磷酸锂的制备方法
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CN114132912B (zh) * 2021-12-24 2023-04-07 浙江中欣氟材股份有限公司 一种六氟磷酸盐的合成方法
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CN115924867A (zh) * 2022-11-22 2023-04-07 福建省德旭新材料有限公司 三氟氧磷的连续反应精馏制备系统及制备方法
CN116253301B (zh) * 2022-12-30 2025-09-05 浙江研一新能源科技有限公司 一种五氟化磷气体的制备方法
CN115947351A (zh) * 2022-12-30 2023-04-11 浙江研一新能源科技有限公司 一种联产六氟磷酸钠和二氟磷酸钠的方法
CN119430102A (zh) * 2024-11-07 2025-02-14 苏州福氢氢能科技有限公司 一种制备五氟化磷的方法
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CN120247056A (zh) * 2025-06-03 2025-07-04 池州天赐高新材料有限公司 一种以三氯氧磷为原料制备六氟磷酸锂的方法
CN120246947B (zh) * 2025-06-03 2025-09-05 池州天赐高新材料有限公司 采用管式反应器以连续性反应制备五氟化磷的方法和系统

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KR101519683B1 (ko) 2015-05-12
CA2696544A1 (en) 2009-02-19
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JP5307409B2 (ja) 2013-10-02
US9034290B2 (en) 2015-05-19
SG183730A1 (en) 2012-09-27
US20110286905A1 (en) 2011-11-24
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CN103058155A (zh) 2013-04-24
TW200927644A (en) 2009-07-01
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EP2189418A1 (en) 2010-05-26
CN103011104B (zh) 2015-12-02

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