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WO2008096723A1 - 六フッ化リン酸塩の製造方法 - Google Patents

六フッ化リン酸塩の製造方法 Download PDF

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Publication number
WO2008096723A1
WO2008096723A1 PCT/JP2008/051806 JP2008051806W WO2008096723A1 WO 2008096723 A1 WO2008096723 A1 WO 2008096723A1 JP 2008051806 W JP2008051806 W JP 2008051806W WO 2008096723 A1 WO2008096723 A1 WO 2008096723A1
Authority
WO
WIPO (PCT)
Prior art keywords
hexafluorophosphate salt
producing
mpf6
raw materials
producing hexafluorophosphate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/051806
Other languages
English (en)
French (fr)
Inventor
Masahide Waki
Kazuhiro Miyamoto
Kenji Aoki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stella Chemifa Corp
Original Assignee
Stella Chemifa Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stella Chemifa Corp filed Critical Stella Chemifa Corp
Priority to CN2008800044869A priority Critical patent/CN101605723B/zh
Priority to US12/525,900 priority patent/US8383075B2/en
Priority to EP08704433A priority patent/EP2123601A4/en
Priority to KR1020097018708A priority patent/KR101459804B1/ko
Priority to CA2677301A priority patent/CA2677301C/en
Publication of WO2008096723A1 publication Critical patent/WO2008096723A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/005—Lithium hexafluorophosphate
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/455—Phosphates containing halogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D13/00—Compounds of sodium or potassium not provided for elsewhere

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Secondary Cells (AREA)
  • Removal Of Specific Substances (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

　本発明の六フッ化リン酸塩（ＭＰＦ６：Ｍ＝Ｌｉ，Ｎａ，Ｋ，Ｒｂ，Ｃｓ，ＮＨ４，Ａｇ）の製造方法は、少なくともＨｘＰＯｙＦｚ水溶液とフッ酸水溶液とＭＦ・ｒ（ＨＦ）とを原料とする（但し、ｒ≧０、０≦ｘ≦３、０≦ｙ≦４、０≦ｚ≦６）。これにより、原料の入手が容易で、さらに反応の制御が可能であり、且つ作業性に優れた六フッ化リン酸塩（ＭＰＦ６：Ｍ＝Ｌｉ，Ｎａ，Ｋ，Ｒｂ，Ｃｓ，ＮＨ４，Ａｇ）を安価で製造することが可能な六フッ化リン酸塩の製造方法を提供することができる。
PCT/JP2008/051806 2007-02-08 2008-02-05 六フッ化リン酸塩の製造方法 Ceased WO2008096723A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
CN2008800044869A CN101605723B (zh) 2007-02-08 2008-02-05 六氟磷酸盐的制造方法
US12/525,900 US8383075B2 (en) 2007-02-08 2008-02-05 Manufacturing method of hexafluorophosphate
EP08704433A EP2123601A4 (en) 2007-02-08 2008-02-05 METHOD FOR PRODUCING HEXAFLUOROPHOSPHATE SALT
KR1020097018708A KR101459804B1 (ko) 2007-02-08 2008-02-05 6불화인산염의 제조방법
CA2677301A CA2677301C (en) 2007-02-08 2008-02-05 Manufacturing method of hexafluorophosphate

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007029405A JP5148125B2 (ja) 2007-02-08 2007-02-08 六フッ化リン酸塩の製造方法
JP2007-029405 2007-02-08

Publications (1)

Publication Number Publication Date
WO2008096723A1 true WO2008096723A1 (ja) 2008-08-14

Family

ID=39681632

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/051806 Ceased WO2008096723A1 (ja) 2007-02-08 2008-02-05 六フッ化リン酸塩の製造方法

Country Status (8)

Country Link
US (1) US8383075B2 (ja)
EP (1) EP2123601A4 (ja)
JP (1) JP5148125B2 (ja)
KR (1) KR101459804B1 (ja)
CN (1) CN101605723B (ja)
CA (1) CA2677301C (ja)
TW (1) TWI439414B (ja)
WO (1) WO2008096723A1 (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110097626A1 (en) * 2008-08-08 2011-04-28 Stella Chemifa Corporation Process for production hexafluorophosphates
CN106536412A (zh) * 2014-03-31 2017-03-22 南非核能源股份有限公司 六氟磷酸盐和五氟化磷的生产

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2421396C1 (ru) * 2009-10-12 2011-06-20 Государственное образовательное учреждение высшего профессионального образования Томский политехнический университет Способ получения гексафторофосфата лития
KR102036924B1 (ko) * 2019-03-15 2019-10-25 (주)후성 육불화인산알칼리금속염 제조방법, 육불화인산알칼리금속염, 육불화인산알칼리금속염 함유 전해농축액 제조방법, 및 이차전지 제조방법
CN111268700A (zh) * 2020-03-09 2020-06-12 江苏九九久科技有限公司 一种高效六氟磷酸锂生产方法
CN114291805A (zh) * 2021-03-17 2022-04-08 多氟多新材料股份有限公司 一种六氟磷酸钾的制备方法
CN114590823B (zh) * 2022-03-31 2023-11-17 河南省氟基新材料科技有限公司 一种六氟磷酸钾的制备方法
CN115092944B (zh) * 2022-06-29 2024-05-14 张家港博威新能源材料研究所有限公司 一种六氟磷酸盐的合成方法
CN115367774A (zh) * 2022-10-26 2022-11-22 如鲲(江苏)新材料科技有限公司 一种六氟磷酸盐的制备方法及其应用
CN115845428B (zh) * 2023-02-28 2023-04-25 福建省龙德新能源有限公司 用于诱导六氟磷酸结晶的超声波装置及其控制方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2488299A (en) 1947-07-17 1949-11-15 Ozark Mahoning Co Method of producing hexafluorophosphoric acid
JPS6345108A (ja) * 1986-08-12 1988-02-26 Hashimoto Kasei Kogyo Kk ６−フツ化りん酸カリウムの製造方法
JP2004075413A (ja) 2002-08-12 2004-03-11 Lithdyne Llc 六フッ化リン酸錯体の製造方法および合成物並びに六フッ化リン酸およびその製造方法
JP2005507849A (ja) 1999-08-17 2005-03-24 リスダイン・リミテッド・ライアビリティ・カンパニー 五フッ化リンの製造方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2488298A (en) * 1946-09-12 1949-11-15 Ozark Mahoning Co Method of producing hexafluorophosphoric acid
DE1567405A1 (de) 1965-12-23 1970-04-16 Albert Ag Chem Werke Verfahren zur Herstellung von Metallfluorphosphaten
JPH0572324A (ja) 1991-09-10 1993-03-26 Mitsubishi Heavy Ind Ltd パルスレーダ装置
JPH05279003A (ja) 1992-03-31 1993-10-26 Morita Kagaku Kogyo Kk ６フッ化リン酸リチウムの製造法
JP3204415B2 (ja) 1992-08-10 2001-09-04 セントラル硝子株式会社 六フッ化リン酸塩の製造方法
US5378445A (en) 1993-12-23 1995-01-03 Fmc Corporation Preparation of lithium hexafluorophosphate solutions
EP0816288B1 (de) * 1996-06-26 2000-01-26 Solvay Fluor und Derivate GmbH Herstellung von Lithiumhexafluormetallaten
IT1290083B1 (it) * 1997-03-14 1998-10-19 Pirelli Pneumatico a bassa temperatura d'esercizio
FR2768427B1 (fr) * 1997-06-06 1999-10-29 Atochem Elf Sa Procede de fabrication d'hexafluorophosphate de lithium
JP3973329B2 (ja) * 1999-12-09 2007-09-12 ステラケミファ株式会社 六フッ化リン酸リチウムの製造方法
US6540969B1 (en) * 2000-11-28 2003-04-01 Lithdyne Llc Preparation of hexafluorophosphoric acid
CN1151960C (zh) * 2001-06-11 2004-06-02 山东省肥城市化肥厂 六氟磷酸锂非水溶剂法规模化生产工艺
US7465517B2 (en) 2004-08-23 2008-12-16 Air Products And Chemicals, Inc. High purity lithium polyhalogenated boron cluster salts useful in lithium batteries
JP4810867B2 (ja) 2005-04-19 2011-11-09 セントラル硝子株式会社 リチウムイオン電池用電解液の製造方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2488299A (en) 1947-07-17 1949-11-15 Ozark Mahoning Co Method of producing hexafluorophosphoric acid
JPS6345108A (ja) * 1986-08-12 1988-02-26 Hashimoto Kasei Kogyo Kk ６−フツ化りん酸カリウムの製造方法
JPH0572324B2 (ja) 1986-08-12 1993-10-12 Hashimoto Kasei Kogyo Kk
JP2005507849A (ja) 1999-08-17 2005-03-24 リスダイン・リミテッド・ライアビリティ・カンパニー 五フッ化リンの製造方法
JP2004075413A (ja) 2002-08-12 2004-03-11 Lithdyne Llc 六フッ化リン酸錯体の製造方法および合成物並びに六フッ化リン酸およびその製造方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP2123601A4 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110097626A1 (en) * 2008-08-08 2011-04-28 Stella Chemifa Corporation Process for production hexafluorophosphates
US9059480B2 (en) * 2008-08-08 2015-06-16 Stella Chemifa Corporation Process for production hexafluorophosphates
CN106536412A (zh) * 2014-03-31 2017-03-22 南非核能源股份有限公司 六氟磷酸盐和五氟化磷的生产
CN106536412B (zh) * 2014-03-31 2019-10-18 南非核能源股份有限公司 六氟磷酸盐和五氟化磷的生产

Also Published As

Publication number Publication date
EP2123601A1 (en) 2009-11-25
CA2677301C (en) 2015-06-16
CN101605723B (zh) 2011-10-05
TWI439414B (zh) 2014-06-01
US8383075B2 (en) 2013-02-26
CA2677301A1 (en) 2008-08-14
TW200906714A (en) 2009-02-16
JP5148125B2 (ja) 2013-02-20
EP2123601A4 (en) 2012-04-04
JP2008195547A (ja) 2008-08-28
CN101605723A (zh) 2009-12-16
KR101459804B1 (ko) 2014-11-07
KR20090108666A (ko) 2009-10-15
US20100317511A1 (en) 2010-12-16

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