US2064883A - Mercerizing - Google Patents
Mercerizing Download PDFInfo
- Publication number
- US2064883A US2064883A US733337A US73333734A US2064883A US 2064883 A US2064883 A US 2064883A US 733337 A US733337 A US 733337A US 73333734 A US73333734 A US 73333734A US 2064883 A US2064883 A US 2064883A
- Authority
- US
- United States
- Prior art keywords
- mercerizing
- crude
- indicated
- chlorphenol
- xylenols
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 235000011121 sodium hydroxide Nutrition 0.000 description 4
- 238000009736 wetting Methods 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 3
- 150000003739 xylenols Chemical class 0.000 description 3
- QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 2
- WADQOGCINABPRT-UHFFFAOYSA-N 3-chloro-2-methylphenol Chemical compound CC1=C(O)C=CC=C1Cl WADQOGCINABPRT-UHFFFAOYSA-N 0.000 description 2
- OJFZXRZZXBFEAP-UHFFFAOYSA-N 5-chloro-1,6-dimethylcyclohexa-2,4-dien-1-ol Chemical compound ClC=1C(C(C=CC1)(C)O)C OJFZXRZZXBFEAP-UHFFFAOYSA-N 0.000 description 2
- 229930003836 cresol Natural products 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- ISPYQTSUDJAMAB-UHFFFAOYSA-N 2-chlorophenol Chemical compound OC1=CC=CC=C1Cl ISPYQTSUDJAMAB-UHFFFAOYSA-N 0.000 description 1
- SZPWGEZWBLCYCZ-UHFFFAOYSA-N 3,4-dichloro-2-methylphenol Chemical compound CC1=C(O)C=CC(Cl)=C1Cl SZPWGEZWBLCYCZ-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001896 cresols Chemical class 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/12—Fermented milk preparations; Treatment using microorganisms or enzymes
- A23C9/122—Apparatus for preparing or treating fermented milk products
- A23C9/1226—Apparatus for preparing or treating fermented milk products for making set yoghurt in containers without stirring, agitation or transport of the yoghurt or the containers during incubation, heating or cooling; Domestic yoghurt apparatus without agitating means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
- B01D1/18—Evaporating by spraying to obtain dry solids
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B5/00—Treatment of metallurgical slag ; Artificial stone from molten metallurgical slag
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B7/00—Hydraulic cements
- C04B7/14—Cements containing slag
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B7/00—Hydraulic cements
- C04B7/14—Cements containing slag
- C04B7/147—Metallurgical slag
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/10—Production of cement, e.g. improving or optimising the production methods; Cement grinding
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
- Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
Definitions
- a process for treating cellulosic fibers with alkali consisting in submitting them to the action of a bath consisting of a mercerizing lye and a monochlorxylenol.
- Mercerizing bath consisting of a caustic soda solution and monochlorxylenol.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Textile Engineering (AREA)
- Microbiology (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatment Of Fiber Materials (AREA)
- Disintegrating Or Milling (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Description
Patented Dec. 22, 1936 UNITED STATES PATENT OFFICE MERCERIZING Karl Brodersen, Dessair in Anhait, Germany, assignor to I. G. Farbenindustrie Aktiengesellschaft, Frankfort-on-the-Main, Germany No Drawing. Application June so, 1934, Serial No. 733,337. In Germany June 30, 1933 2 Claims. (Cl. 8-20) The shrinkage observed after 10, 20, and 30 secends, is indicated in percentage of the original length of the threads.
For comparison, the action of a number of other phenolic compounds suggested for the purpose in question, likewise,
is indicated in this table.
xylenols, chlorphenol, chlorcresol or polyhalogen cresol with or without addition of, for instance,
saturated or unsaturated polyhydric alcohols of 25 wherein Hlg means halogen, impart to mercerizing lyes an outstanding good wetting capacity. Contrary to other'monohalogenated phenol derivatives they may be used without addition of a solvent or of another assistant, they surpass 30 even the polyhalogenated cresols with respect to their wetting capacity. It is not necessary to add these halogenated xylenols to the mercerizing lyes in a pure state, but one may use the halogenated technical mixtures of the xylenols 5 in question.
' In the table following hereafter; the wetting capacity of some of my new assistants for mercerizing cotton may be seen. The wetting capa city of the different products is indicated in this ,40 table by the shrinkageof a crude cotton yarn that is immersed into a mercerizing lye of 30 IE6. at about 20 C. for 5 seconds with a tension corresponding to 10 grams per four threads.
.ihrinkege of the crude Grs. cotton thread indicated Substance added to the lye addgd 1 ter 10 sec. 20 sec. 30 sec.
(1 Without addition, 0. 2 l. 5 2. 5 (2 P on 0.3 1.6 3.0 (3 Para-chlorphenol 1.0 3. 8 6. 7 (4 Para-chlorphenol 0.3 l. 6 3. 5 (5) Monochloreresol prepared from crude cres 2. 5 7. 5 ll. 6 (6) Monochlorcresol prepared from crude cresol 0. 3 1. 7 3. 4 (7) Crude dichlorcresol repared from crude or en 1. 5. 0 10. 8; Purified .hlorxy-nnnl 8.0 15. 9 17.8
9 Monochiorxyleno prepared 11:05 te gl gca crude xy one o X oiling 8t 209to 225 0 7. 5 16. 0 17.5
handling, dosing and packing.
What I claim is:
1. A process for treating cellulosic fibers with alkali, consisting in submitting them to the action of a bath consisting of a mercerizing lye and a monochlorxylenol.
2. Mercerizing bath consisting of a caustic soda solution and monochlorxylenol.
KARL BRODERSEN.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE1933I0047494 DE686592C (en) | 1933-07-01 | 1933-07-01 | Process for increasing the wetting ability of mercerising liquors |
| BE993757X | 1948-09-03 | ||
| FR2819172X | 1953-06-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US2064883A true US2064883A (en) | 1936-12-22 |
Family
ID=32329370
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US733337A Expired - Lifetime US2064883A (en) | 1933-07-01 | 1934-06-30 | Mercerizing |
| US432882A Expired - Lifetime US2819172A (en) | 1933-07-01 | 1954-05-27 | Method for producing a hydraulic binder in powder form |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US432882A Expired - Lifetime US2819172A (en) | 1933-07-01 | 1954-05-27 | Method for producing a hydraulic binder in powder form |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US2064883A (en) |
| BE (1) | BE484660A (en) |
| CH (1) | CH284313A (en) |
| DE (1) | DE686592C (en) |
| FR (3) | FR775797A (en) |
| GB (3) | GB441070A (en) |
| LU (1) | LU29684A1 (en) |
| NL (4) | NL89851C (en) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1046997B (en) * | 1953-12-21 | 1958-12-18 | Fischer & Krecke Kg | Device for producing a gusseted flat hose |
| GB951679A (en) * | 1961-07-24 | 1964-03-11 | Smidth & Co As F L | Manufacture of cement |
| US3341342A (en) * | 1963-06-14 | 1967-09-12 | Southwestern Portland Cement C | Method of grinding and cooling cement |
| BE755854A (en) * | 1969-09-10 | 1971-02-15 | Niro Atomizer As | IMPROVEMENTS IN CEMENT MANUFACTURING PROCESSES AND FACILITIES FROM THICK SLUDGE |
| FR2249140B1 (en) * | 1973-10-24 | 1976-10-01 | Lafarge Sa | |
| FR2249139B1 (en) * | 1973-10-24 | 1976-10-01 | Lafarge Sa | |
| US4081287A (en) * | 1974-11-01 | 1978-03-28 | Lafarge S.A. | Manufacturing process of mineral charges, products obtained and their application |
| FR2463755A1 (en) * | 1979-08-24 | 1981-02-27 | Panis Rene | Soil improving hydraulic binder compsn. - contains ground slag and free lime |
| US5569314A (en) * | 1995-01-30 | 1996-10-29 | Energy Mines & Resources-Canada | Thermal stabilization of steelmaking slag |
| JP3045380B2 (en) * | 1996-09-17 | 2000-05-29 | 順三 豊田 | Method and system for preventing solidification of granulated blast furnace slag |
| US9233485B1 (en) * | 2012-09-16 | 2016-01-12 | Michael Gurin | Low energy slag and cement production |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1609993A (en) * | 1922-11-03 | 1926-12-07 | Ind Waste Products Corp | Process of desiccation and products obtained thereby |
| US1561971A (en) * | 1923-10-16 | 1925-11-17 | Naugatuck Chem Co | Method for treating pulverulent material and product |
| US1523632A (en) * | 1924-11-11 | 1925-01-20 | China Frederick John Edwin | Minute disintegration of substances |
| BE358780A (en) * | 1928-06-28 | |||
| US2110167A (en) * | 1933-12-02 | 1938-03-08 | Food Concentrates Inc | Spray drying apparatus |
| US2287795A (en) * | 1938-12-08 | 1942-06-30 | Drying & Concentrating Company | Mechanism for removing moisture from liquid products |
| US2421648A (en) * | 1943-02-13 | 1947-06-03 | American Cyanamid Co | Bauxite beneficiation by hydration of gangue |
| US2632711A (en) * | 1948-09-03 | 1953-03-24 | Trief Victor | Method for producing iron cement in powder form |
| US2514064A (en) * | 1949-05-06 | 1950-07-04 | A M Phippen | Ore milling and screening apparatus |
| US2670036A (en) * | 1949-08-03 | 1954-02-23 | American Cyanamid Co | Spray drying |
| US2698815A (en) * | 1950-06-08 | 1955-01-04 | Instant Drying Corp | Drying method and apparatus |
| US2656119A (en) * | 1951-02-14 | 1953-10-20 | Gruendler Crusher & Pulverizer | Refining blender |
-
0
- NL NL37967D patent/NL37967C/xx active
- NL NLAANVRAGE7408261,A patent/NL178965B/en unknown
- LU LU29684D patent/LU29684A1/fr unknown
- NL NL70021D patent/NL70021C/xx active
- NL NL89851D patent/NL89851C/xx active
-
1933
- 1933-07-01 DE DE1933I0047494 patent/DE686592C/en not_active Expired
-
1934
- 1934-06-30 US US733337A patent/US2064883A/en not_active Expired - Lifetime
- 1934-07-11 GB GB20344/34A patent/GB441070A/en not_active Expired
- 1934-07-12 FR FR775797D patent/FR775797A/en not_active Expired
-
1948
- 1948-09-03 BE BE484660D patent/BE484660A/fr unknown
-
1949
- 1949-08-25 FR FR993757D patent/FR993757A/en not_active Expired
- 1949-08-26 GB GB22288/49A patent/GB673866A/en not_active Expired
- 1949-08-31 CH CH284313D patent/CH284313A/en unknown
-
1953
- 1953-06-01 FR FR63974D patent/FR63974E/en not_active Expired
-
1954
- 1954-05-26 GB GB15513/54A patent/GB774907A/en not_active Expired
- 1954-05-27 US US432882A patent/US2819172A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| BE484660A (en) | 1949-03-03 |
| NL178965B (en) | |
| FR63974E (en) | 1955-10-14 |
| GB774907A (en) | 1957-05-15 |
| CH284313A (en) | 1952-07-31 |
| NL37967C (en) | 1900-01-01 |
| US2819172A (en) | 1958-01-07 |
| LU29684A1 (en) | |
| GB441070A (en) | 1936-01-13 |
| FR775797A (en) | 1935-01-09 |
| FR993757A (en) | 1951-11-07 |
| NL70021C (en) | 1900-01-01 |
| GB673866A (en) | 1952-06-11 |
| NL89851C (en) | 1900-01-01 |
| DE686592C (en) | 1940-01-12 |
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