US1864110A - Process for the treatment of textile fibers - Google Patents
Process for the treatment of textile fibers Download PDFInfo
- Publication number
- US1864110A US1864110A US382582A US38258229A US1864110A US 1864110 A US1864110 A US 1864110A US 382582 A US382582 A US 382582A US 38258229 A US38258229 A US 38258229A US 1864110 A US1864110 A US 1864110A
- Authority
- US
- United States
- Prior art keywords
- treatment
- fiber
- acid
- soluble
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000835 fiber Substances 0.000 title description 30
- 238000000034 method Methods 0.000 title description 12
- 239000004753 textile Substances 0.000 title description 10
- 239000002253 acid Substances 0.000 description 20
- 150000003839 salts Chemical class 0.000 description 19
- JWAZRIHNYRIHIV-UHFFFAOYSA-N 2-naphthol Chemical compound C1=CC=CC2=CC(O)=CC=C21 JWAZRIHNYRIHIV-UHFFFAOYSA-N 0.000 description 18
- -1 aromatic hydroxy compound Chemical class 0.000 description 18
- 229950011260 betanaphthol Drugs 0.000 description 9
- 239000003921 oil Substances 0.000 description 9
- 235000019198 oils Nutrition 0.000 description 9
- 239000004006 olive oil Substances 0.000 description 6
- 235000008390 olive oil Nutrition 0.000 description 6
- 239000002480 mineral oil Substances 0.000 description 5
- 235000010446 mineral oil Nutrition 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 2
- 238000009795 derivation Methods 0.000 description 2
- VNEBWJSWMVTSHK-UHFFFAOYSA-L disodium;3-hydroxynaphthalene-2,7-disulfonate Chemical compound [Na+].[Na+].C1=C(S([O-])(=O)=O)C=C2C=C(S([O-])(=O)=O)C(O)=CC2=C1 VNEBWJSWMVTSHK-UHFFFAOYSA-L 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- USWINTIHFQKJTR-UHFFFAOYSA-N 3-hydroxynaphthalene-2,7-disulfonic acid Chemical compound C1=C(S(O)(=O)=O)C=C2C=C(S(O)(=O)=O)C(O)=CC2=C1 USWINTIHFQKJTR-UHFFFAOYSA-N 0.000 description 1
- 102000014160 PTEN Phosphohydrolase Human genes 0.000 description 1
- 108010011536 PTEN Phosphohydrolase Proteins 0.000 description 1
- 125000000853 cresyl group Chemical class C1(=CC=C(C=C1)C)* 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
- Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
- Y10S516/03—Organic sulfoxy compound containing
Definitions
- Our invention relates to a process for the treatment of textile fibers and relates particularly to a process adapted for the treatment of silk.
- This softening of the silk fiber and gum has usually been accomplished by immersing the fiber in a bath of water and emulsified oil for about 12 hours, removing and whizscopic and can be knit wtihout back winding.
- the process of our invention comprises introducing an aromatic hydroxy compound
- a salt of a sulpho acid of an aromatic hydroxy compound or a derivation thereof into the treatment bath among which are a salt of'beta naphthol 3 :6 disulpho acid (R acid), a salt of beta naphthol 6 monosulpho acid (Schaflers acid), a salt of alpha naphthol 4 monosulpho acid (N. W. acid), a salt of sulphonated cresol.
- An emulsion is made of 14 pounds soluble olive oil (sulphonated olive oil) and 4.0 gal- Ions of water.
- the emulsion is added to, and thorougly mixed with, the solution of R salt and 100 pounds of silk are immersed therein for 12 hours, removed and whizzed.
- aromatic hydroxy compounds in our claims we mean the aromatic hydroxy compounds themselves, their salts, their sulpho acids and derivations, whether used singly or in combination with each other.
- the step which comprises treating the fiber with a soluble oil and an aqueous soluble salt of beta naphthol 3: 6 disulpho acid.
- the step which comprises treating the fiber with soluble olive oil and an aqueous soluble salt of beta naphthol 3:6 disulpho acid.
- the step which comprises treating the fiber with a soluble oil and an aqueous soluble salt of beta naphthol 3:6 disulpho acid.
- the step which comprises treating the fiber with soluble olive oil and an aqueous soluble salt of beta naphthol 3 6 disulpho acid.
- the step which comprises treating the fiber with a soluble mineral oil and an aqueous soluble salt of beta naphthol 3 :6 disulpho acid.
- the step which comprises treating the fiber with a soluble ioo mineral oil and an aqueous soluble salt of beta naphthol 3: 6 disulpho acid.
- the step which comprises treating the fiber with a soluble oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
- the step i which comprises treating the fiber with a s01- uble olive oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
- the step which comprises treating the fiber with a soluble oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
- the step which comprises treating the fiber with a soluble olive oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
- step which comprises treating the fiber with .a soluble mineral oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
- the step which comprises treating'the fiber with a soluble mineral oil and an aqueousv soluble salt of a sulpho acid of an aromatic hydroxy com pound.
- the step which comprises treating the fiber with soluble mineral oil and an aqueous soluble salt of beta naphthol 3:6 disulpho acid.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Description
Patented June 21,1932
UNITED STATS PTEN, OFFICE JACOB IITOLFSON, OF BROOKLYN, NEW YORK, AND DOROTHY LANGIDON POTTER, OF HAOKENSACK, NEW'J'ERSEY, ASSIGNORS TO NATIONAL OIL PRODUCTS COMPANY, OF
HARRISON, NEW JERSEY, A CORPORATION OF NEW JERSEY PROCESS FOR THE TREATMENT OF TEXTILE FIBERS Ilo Drawing. Application filed July 31,
. Our invention relates to a process for the treatment of textile fibers and relates particularly to a process adapted for the treatment of silk.
' In'the preparation of silk it is essential that the waxes and be softened and that it be converted into a soft, pliable condition and for certain uses, as for hosiery tram, it is desirable that the silk be hygro- 1 scopic in order that it may be knitted direct from the cone without the necessity of back winding, which requires an additional softening treatment.
This softening of the silk fiber and gum has usually been accomplished by immersing the fiber in a bath of water and emulsified oil for about 12 hours, removing and whizscopic and can be knit wtihout back winding.
Zing. This process allows a large amount of oil to remain in the bath, thus causing a loss thereof, the fibers are not uniformly pene- 'trated and are not hygroscopic. Attempts.
The process of our invention comprises introducing an aromatic hydroxy compound,
a salt of a sulpho acid of an aromatic hydroxy compound or a derivation thereof into the treatment bath, among which are a salt of'beta naphthol 3 :6 disulpho acid (R acid), a salt of beta naphthol 6 monosulpho acid (Schaflers acid), a salt of alpha naphthol 4 monosulpho acid (N. W. acid), a salt of sulphonated cresol.
We give the following as one example of our process: I
An emulsion is made of 14 pounds soluble olive oil (sulphonated olive oil) and 4.0 gal- Ions of water.
1929. Serial No. 382,582.
' 2 pounds of R salt are dissolved in 40 gallons of water.
The emulsion is added to, and thorougly mixed with, the solution of R salt and 100 pounds of silk are immersed therein for 12 hours, removed and whizzed.
By our process practically, all of the soluble oil is absorbed by. thejsilk from the bath, whereas in the present employed process about 18 pounds of oil would be emplo ed, only about 20 percent of which is absor ed, the remainder being wasted.
In addition to .this economic advantage, our process produced better and more even penetration and makes the silk hygroscopic, all of which qualities are of the greatest advantage in the further treatment of the fiber.
By aromatic hydroxy compounds in our claims we mean the aromatic hydroxy compounds themselves, their salts, their sulpho acids and derivations, whether used singly or in combination with each other.
We do not limit ourselves to the particular chemicals, time of treatment, or steps of procedure specifically mentioned, as these are given simply as a means for describing the process of our invention.
What we claim is 1. In the treatment of textile fibers, the step which comprises treating the fiber with a soluble oil and an aqueous soluble salt of beta naphthol 3: 6 disulpho acid.
2. In the treatment of textile fibers, the step which comprises treating the fiber with soluble olive oil and an aqueous soluble salt of beta naphthol 3:6 disulpho acid.
3. In the treatment of silk, the step which comprises treating the fiber with a soluble oil and an aqueous soluble salt of beta naphthol 3:6 disulpho acid.
4. In the treatment of silk, the step which comprises treating the fiber with soluble olive oil and an aqueous soluble salt of beta naphthol 3 6 disulpho acid.
5. In the treatment of textile fibers, the step which comprises treating the fiber with a soluble mineral oil and an aqueous soluble salt of beta naphthol 3 :6 disulpho acid.
6. In the treatment of silk, the step which comprises treating the fiber with a soluble ioo mineral oil and an aqueous soluble salt of beta naphthol 3: 6 disulpho acid.
7. In the treatment of textile fiber, the step which comprises treating the fiber with a soluble oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
8. In the treatment of textile fiber, the step i which comprises treating the fiber with a s01- uble olive oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
9. In the treatment of silk fiber, the step which comprises treating the fiber with a soluble oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
10. In the treatment of silk fiber, the step which comprises treating the fiber with a soluble olive oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
11. In the treatment of textile fiber, the
step which comprises treating the fiber with .a soluble mineral oil and an aqueous soluble salt of a sulpho acid of an aromatic hydroxy compound.
12. In the treatment of silk fiber, the step which comprises treating'the fiber with a soluble mineral oil and an aqueousv soluble salt of a sulpho acid of an aromatic hydroxy com pound.
13. In the treatment of textile fiber, the step which comprises treating the fiber with soluble mineral oil and an aqueous soluble salt of beta naphthol 3:6 disulpho acid.
Signed at Harrison, in the county of Hudson and State of New Jersey, this 25th day of July, 1929.
JACOB WOLFSON. DOROTHY LANGDON POTTER.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US382582A US1864110A (en) | 1929-07-31 | 1929-07-31 | Process for the treatment of textile fibers |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US382582A US1864110A (en) | 1929-07-31 | 1929-07-31 | Process for the treatment of textile fibers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US1864110A true US1864110A (en) | 1932-06-21 |
Family
ID=23509601
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US382582A Expired - Lifetime US1864110A (en) | 1929-07-31 | 1929-07-31 | Process for the treatment of textile fibers |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US1864110A (en) |
-
1929
- 1929-07-31 US US382582A patent/US1864110A/en not_active Expired - Lifetime
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