UA73514C2 - A method for making adipic acid - Google Patents
A method for making adipic acid Download PDFInfo
- Publication number
- UA73514C2 UA73514C2 UA2002010710A UA2002010710A UA73514C2 UA 73514 C2 UA73514 C2 UA 73514C2 UA 2002010710 A UA2002010710 A UA 2002010710A UA 2002010710 A UA2002010710 A UA 2002010710A UA 73514 C2 UA73514 C2 UA 73514C2
- Authority
- UA
- Ukraine
- Prior art keywords
- adipic acid
- crystals
- liquid medium
- range
- acid crystals
- Prior art date
Links
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 title claims abstract description 74
- 239000001361 adipic acid Substances 0.000 title claims abstract description 37
- 235000011037 adipic acid Nutrition 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 21
- 239000013078 crystal Substances 0.000 claims abstract description 50
- 239000007788 liquid Substances 0.000 claims abstract description 22
- 238000002425 crystallisation Methods 0.000 claims abstract description 11
- 230000008025 crystallization Effects 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 238000012876 topography Methods 0.000 claims 1
- 238000001035 drying Methods 0.000 abstract description 2
- 238000003756 stirring Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 description 5
- 238000000151 deposition Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- 239000004952 Polyamide Substances 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 229910017604 nitric acid Inorganic materials 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 229920002647 polyamide Polymers 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 2
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 238000004026 adhesive bonding Methods 0.000 description 1
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical class NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000001384 succinic acid Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C55/00—Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
- C07C55/02—Dicarboxylic acids
- C07C55/14—Adipic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9908591A FR2795721B1 (fr) | 1999-06-29 | 1999-06-29 | Procede de fabrication d'acide adipique |
| PCT/FR2000/001809 WO2001000557A1 (fr) | 1999-06-29 | 2000-06-28 | Procede de fabrication d'acide adipique |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA73514C2 true UA73514C2 (en) | 2005-08-15 |
Family
ID=9547672
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UA2002010710A UA73514C2 (en) | 1999-06-29 | 2000-06-28 | A method for making adipic acid |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US6822117B1 (zh) |
| EP (1) | EP1196369B1 (zh) |
| JP (1) | JP3806351B2 (zh) |
| KR (1) | KR100638130B1 (zh) |
| CN (1) | CN1173919C (zh) |
| AR (1) | AR024589A1 (zh) |
| BR (1) | BR0012028B1 (zh) |
| CA (1) | CA2377179A1 (zh) |
| CZ (1) | CZ20014610A3 (zh) |
| DE (1) | DE60009074T2 (zh) |
| ES (1) | ES2213592T3 (zh) |
| FR (1) | FR2795721B1 (zh) |
| PL (1) | PL356988A1 (zh) |
| RU (1) | RU2211828C1 (zh) |
| SK (1) | SK19082001A3 (zh) |
| TW (1) | TWI254041B (zh) |
| UA (1) | UA73514C2 (zh) |
| WO (1) | WO2001000557A1 (zh) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2829761B1 (fr) * | 2001-09-18 | 2004-02-20 | Rhodia Polyamide Intermediates | Procede de fabrication de cristaux d'acide adipique et cristaux ainsi obtenus |
| FR2946646B1 (fr) * | 2009-06-16 | 2012-09-21 | Rhodia Operations | Procede de production de cristaux d'acide adipique |
| CN106810442B (zh) | 2016-12-26 | 2018-04-13 | 河南神马尼龙化工有限责任公司 | 一种高品质己二酸的生产方法 |
| EP3728176B1 (en) * | 2017-12-22 | 2023-08-30 | Basf Se | Method of removing nitrate compounds from adipic acid |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3123635A (en) * | 1964-03-03 | Agitation of adipic acid crystals to | ||
| NL223106A (zh) * | 1957-12-09 | |||
| US4375552A (en) * | 1969-01-31 | 1983-03-01 | C. P. Hall Company | Nitric acid process for production of adipic acid from hydrocarbons |
| US3886153A (en) * | 1974-01-09 | 1975-05-27 | Fmc Corp | Purification of cyanuric acid |
| AT332362B (de) * | 1974-10-10 | 1976-09-27 | Erz & Stahl Ges M B H | Verfahren zur gewinnung von monocarbonsaureestern und dicarbonsauren oder deren estern aus den abfallsalzlosungen der cyclohexanonherstellung |
| US4254283A (en) * | 1979-06-07 | 1981-03-03 | Monsanto Company | Process for preparing adipic acid with recovery of glutaric and succinic acids |
| US5166421A (en) * | 1991-03-18 | 1992-11-24 | E. I. Du Pont De Nemours And Company | Process for the manufacture of adipic acid |
| US5471001A (en) * | 1994-12-15 | 1995-11-28 | E. I. Du Pont De Nemours And Company | Crystallization of adipic acid |
| US5710325A (en) * | 1996-11-01 | 1998-01-20 | E. I. Du Pont De Nemours And Company | Manufacture of adipic acid |
| DE19705329A1 (de) * | 1997-02-12 | 1998-08-13 | Basf Ag | Dicarbonsäurekristallisate |
-
1999
- 1999-06-29 FR FR9908591A patent/FR2795721B1/fr not_active Expired - Fee Related
-
2000
- 2000-06-28 AR ARP000103238A patent/AR024589A1/es unknown
- 2000-06-28 PL PL00356988A patent/PL356988A1/xx unknown
- 2000-06-28 BR BRPI0012028-6A patent/BR0012028B1/pt not_active IP Right Cessation
- 2000-06-28 UA UA2002010710A patent/UA73514C2/uk unknown
- 2000-06-28 EP EP00949565A patent/EP1196369B1/fr not_active Expired - Lifetime
- 2000-06-28 SK SK1908-2001A patent/SK19082001A3/sk unknown
- 2000-06-28 CN CNB008096651A patent/CN1173919C/zh not_active Expired - Fee Related
- 2000-06-28 JP JP2001506971A patent/JP3806351B2/ja not_active Expired - Fee Related
- 2000-06-28 DE DE60009074T patent/DE60009074T2/de not_active Expired - Lifetime
- 2000-06-28 CA CA002377179A patent/CA2377179A1/fr not_active Abandoned
- 2000-06-28 KR KR1020017016915A patent/KR100638130B1/ko not_active Expired - Lifetime
- 2000-06-28 CZ CZ20014610A patent/CZ20014610A3/cs unknown
- 2000-06-28 ES ES00949565T patent/ES2213592T3/es not_active Expired - Lifetime
- 2000-06-28 RU RU2002102070/04A patent/RU2211828C1/ru not_active IP Right Cessation
- 2000-06-28 US US10/018,814 patent/US6822117B1/en not_active Expired - Fee Related
- 2000-06-28 WO PCT/FR2000/001809 patent/WO2001000557A1/fr not_active Ceased
- 2000-09-20 TW TW089112740A patent/TWI254041B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE60009074T2 (de) | 2004-08-26 |
| ES2213592T3 (es) | 2004-09-01 |
| SK19082001A3 (sk) | 2002-06-04 |
| DE60009074D1 (de) | 2004-04-22 |
| JP3806351B2 (ja) | 2006-08-09 |
| EP1196369A1 (fr) | 2002-04-17 |
| BR0012028B1 (pt) | 2010-11-03 |
| CN1359364A (zh) | 2002-07-17 |
| TWI254041B (en) | 2006-05-01 |
| FR2795721B1 (fr) | 2003-04-18 |
| CA2377179A1 (fr) | 2001-01-04 |
| JP2003503377A (ja) | 2003-01-28 |
| US6822117B1 (en) | 2004-11-23 |
| PL356988A1 (en) | 2004-07-12 |
| FR2795721A1 (fr) | 2001-01-05 |
| KR100638130B1 (ko) | 2006-10-24 |
| BR0012028A (pt) | 2002-03-19 |
| WO2001000557A1 (fr) | 2001-01-04 |
| EP1196369B1 (fr) | 2004-03-17 |
| AR024589A1 (es) | 2002-10-16 |
| KR20020025096A (ko) | 2002-04-03 |
| CZ20014610A3 (cs) | 2002-05-15 |
| CN1173919C (zh) | 2004-11-03 |
| RU2211828C1 (ru) | 2003-09-10 |
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