[go: up one dir, main page]

TWI868553B - Granular structure with active compound of organic acids and method for preparing the same - Google Patents

Granular structure with active compound of organic acids and method for preparing the same Download PDF

Info

Publication number
TWI868553B
TWI868553B TW111150976A TW111150976A TWI868553B TW I868553 B TWI868553 B TW I868553B TW 111150976 A TW111150976 A TW 111150976A TW 111150976 A TW111150976 A TW 111150976A TW I868553 B TWI868553 B TW I868553B
Authority
TW
Taiwan
Prior art keywords
particle structure
acid
core
present disclosure
flavoring
Prior art date
Application number
TW111150976A
Other languages
Chinese (zh)
Other versions
TW202425955A (en
Inventor
黃玉鈴
楊鎧睿
尤品人
王婉馨
劉雅玲
許勝傑
陳勁初
Original Assignee
葡萄王生技股份有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 葡萄王生技股份有限公司 filed Critical 葡萄王生技股份有限公司
Priority to TW111150976A priority Critical patent/TWI868553B/en
Publication of TW202425955A publication Critical patent/TW202425955A/en
Application granted granted Critical
Publication of TWI868553B publication Critical patent/TWI868553B/en

Links

Images

Landscapes

  • Tea And Coffee (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

Provided is a granular structure for embedding Kombucha mushroom fermentation broth and fibers and a method for preparing the same, and the core thereof is prepared by mixing raw materials and coating granulation by a fluidized bed spray granulator to improve flowability and solubility and to preserve the organic acids in the Kombucha mushroom fermentation broth. Further, the core is embedded in a sustained-release flavoring layer with flavoring ingredients. The sustained-release flavoring layer is then coated with an anti-hygroscopic protective layer to achieve anti-hygroscopic preservation without adding an anti-caking agent.

Description

含有機酸活性物質之顆粒結構及其製備方法 Granular structure containing organic acid active substance and its preparation method

本揭露係關於一種顆粒結構,尤係關於一種包埋有機酸之顆粒結構。 The present disclosure relates to a particle structure, and more particularly to a particle structure encapsulating an organic acid.

含有機酸成分之飲品在進行粉末化之過程常使用高溫噴霧乾燥;然而,產品中的有機酸容易因高溫而被破壞或揮發逸散,因此無法有效達到保留有機酸以作為保健品的成分。再者,自製發酵飲品保存階段的低溫冷藏效期多僅能保存1周,且保存過程不可避免地將產生能耗成本。 Beverages containing organic acids are often dried by high-temperature spraying during the powdering process; however, the organic acids in the product are easily destroyed or volatilized by high temperatures, so it is not possible to effectively retain the organic acids as ingredients for health products. Furthermore, the low-temperature refrigeration period of homemade fermented beverages can only be preserved for 1 week at most, and the preservation process will inevitably generate energy consumption costs.

此外,為了增加產品溶解度,一般即溶粉末飲品係以不同配方組成的粉末混合而得,因其混拌過程中易產生吸濕的問題,故配方中常添加二氧化矽作為抗結塊劑。然而,抗結塊劑對於食用者之健康無益,食用過量反而造成身體負擔。 In addition, in order to increase the solubility of the product, instant powdered drinks are generally made by mixing powders of different formulas. Since the mixing process is prone to moisture absorption, silicon dioxide is often added to the formula as an anti-caking agent. However, anti-caking agents are not good for the health of consumers, and excessive consumption will cause a burden on the body.

因此,本領域亟需可同時克服上述問題的產品。 Therefore, this field is in urgent need of products that can overcome the above problems at the same time.

有鑑於上述問題,本揭露提供一種能包埋有機酸及其它活性物質之顆粒結構,其包含核心、包覆該核心的調味殼層及包覆該調味殼層的保護層,其中,該核心包含功能性成分,且該功能性成分包含纖維和紅茶菌菇發酵液。 In view of the above problems, the present disclosure provides a particle structure capable of encapsulating organic acids and other active substances, which comprises a core, a flavoring shell layer covering the core, and a protective layer covering the flavoring shell layer, wherein the core comprises functional ingredients, and the functional ingredients comprise fiber and kombucha mushroom fermentation liquid.

於本揭露之至少一具體實施例中,該核心進一步包含紅茶粉。 In at least one specific embodiment of the present disclosure, the core further comprises black tea powder.

於本揭露之至少一具體實施例中,該顆粒結構之平均粒徑至少為0.2mm。於本揭露之一些具體實施例中,該顆粒結構之平均粒徑為0.2mm至0.5mm。 In at least one specific embodiment of the present disclosure, the average particle size of the particle structure is at least 0.2 mm. In some specific embodiments of the present disclosure, the average particle size of the particle structure is 0.2 mm to 0.5 mm.

於本揭露之至少一具體實施例中,該纖維係選自由可溶性纖維、菊苣纖維、果寡糖所組成群組之其中之一或其組合。 In at least one specific embodiment of the present disclosure, the fiber is selected from one of the group consisting of soluble fiber, chicory fiber, and fructooligosaccharide or a combination thereof.

於本揭露之至少一具體實施例中,該功能性成分另包含幫助保存有機酸之有效成分、載劑、賦形劑或其組合。 In at least one specific embodiment of the present disclosure, the functional ingredient further comprises an active ingredient that helps preserve organic acids, a carrier, a formulator, or a combination thereof.

於本揭露之至少一具體實施例中,該紅茶菌菇發酵液包含有機酸或益生菌。於本揭露之一些具體實施例中,該益生菌為乳酸菌。 In at least one specific embodiment of the present disclosure, the fermented Kombucha mushroom liquid contains organic acid or probiotics. In some specific embodiments of the present disclosure, the probiotics are lactic acid bacteria.

於本揭露之至少一具體實施例中,該有機酸係選自由醋酸、檸檬酸、琥珀酸、草酸、葡萄糖醛酸及葡萄糖酸所組成群組之其中之一或其組合。 In at least one specific embodiment of the present disclosure, the organic acid is selected from one or a combination of the group consisting of acetic acid, citric acid, succinic acid, oxalic acid, glucuronic acid and gluconic acid.

於本揭露之至少一具體實施例中,該調味殼層包含香氣微膠囊及調味成分。 In at least one specific embodiment of the present disclosure, the flavoring shell comprises aroma microcapsules and flavoring ingredients.

於本揭露的一些具體實施例中,該核心係由紅茶菌菇發酵液經噴霧造粒而製成,故能有效防止紅茶菌菇發酵液中的有機酸成分被破壞或揮發逸散,且將粉體原料製備成顆粒狀能改善粉體的流動性及溶解性。 此外,調味殼層除了具有調味或調香成分,還具有保護包埋其中有機酸成分之功效,亦可視實際需求設計為緩釋型調味殼層。另外,保護層具有抗吸濕功能,以取代一般粉末混拌工段所添加的抗結塊劑。 In some specific embodiments disclosed herein, the core is made of kombucha fermented liquid by spray granulation, so that the organic acid components in the kombucha fermented liquid can be effectively prevented from being destroyed or volatilized, and the powder raw material is prepared into granules to improve the fluidity and solubility of the powder. In addition, the seasoning shell layer not only has the flavoring or fragrance components, but also has the effect of protecting and encapsulating the organic acid components therein, and can also be designed as a slow-release seasoning shell layer according to actual needs. In addition, the protective layer has an anti-moisture absorption function to replace the anti-caking agent added in the general powder mixing stage.

本揭露另提供一種製備上述顆粒結構之方法,其包含將該功能性成分過篩;混合及乾燥該功能性成分;將該功能性成分進行噴霧造粒以形成該核心;以及形成包覆該核心之調味殼層及保護層。 The present disclosure also provides a method for preparing the above-mentioned particle structure, which comprises screening the functional ingredients; mixing and drying the functional ingredients; spraying and granulating the functional ingredients to form the core; and forming a flavoring shell layer and a protective layer covering the core.

於本揭露之至少一具體實施例中,該紅茶菌菇發酵液係藉由噴霧造粒以形成該核心。於本揭露之一些具體實施例中,係使用流動床噴霧造粒製程將該紅茶粉、纖維和紅茶菌菇發酵液或其他功能性成分快速且均勻包覆混合。 In at least one specific embodiment of the present disclosure, the fermented kombucha mushroom liquid is granulated by spraying to form the core. In some specific embodiments of the present disclosure, the black tea powder, fiber and fermented kombucha mushroom liquid or other functional ingredients are quickly and evenly coated and mixed using a fluidized bed spray granulation process.

於本揭露之至少一具體實施例中,該噴霧造粒之溫度為30℃至90℃、37℃至43℃、40℃至80℃、77℃至83℃、52℃至74℃、57℃至63℃、49℃至62℃或61℃至69℃。於一些具體實施例中,該噴霧造粒之溫度可為約31℃、33℃、35℃、37℃、39℃、41℃、43℃、45℃、47℃、49℃、51℃、53℃、55℃、57℃、59℃、61℃、63℃、65℃、67℃、69℃、71℃、73℃、75℃、77℃、79℃、81℃、83℃、85℃、87℃、89℃,但本揭露不以此為限。 In at least one specific embodiment of the present disclosure, the temperature of the spray granulation is 30°C to 90°C, 37°C to 43°C, 40°C to 80°C, 77°C to 83°C, 52°C to 74°C, 57°C to 63°C, 49°C to 62°C, or 61°C to 69°C. In some specific embodiments, the temperature of the spray granulation may be about 31°C, 33°C, 35°C, 37°C, 39°C, 41°C, 43°C, 45°C, 47°C, 49°C, 51°C, 53°C, 55°C, 57°C, 59°C, 61°C, 63°C, 65°C, 67°C, 69°C, 71°C, 73°C, 75°C, 77°C, 79°C, 81°C, 83°C, 85°C, 87°C, 89°C, but the present disclosure is not limited thereto.

於本揭露之至少一具體實施例中,係使用流動床噴霧造粒機以約57℃至63℃進行顆粒原料混拌與包覆造粒,該顆粒原料包含纖維和紅茶菌菇發酵液;在核心表面以調味成分做包覆形成調味殼層;以及在該調味殼層之外層以再以包埋技術形成保護層。於本揭露的一些具體實施例中,該保護層為抗吸濕保護層,以形成微膠囊顆粒之設計,故無需額外添 加抗結塊劑。 In at least one specific embodiment of the present disclosure, a fluidized bed spray granulator is used to mix and coat the granule raw materials at about 57°C to 63°C. The granule raw materials include fiber and fermented tea mushroom liquid; a flavoring shell is formed by coating the core surface with a flavoring component; and a protective layer is formed on the outer layer of the flavoring shell by an embedding technique. In some specific embodiments of the present disclosure, the protective layer is an anti-hygroscopic protective layer to form a microcapsule particle design, so there is no need to add an anti-caking agent.

本揭露之顆粒結構較一般紅茶菌菇飲品產品結構均勻,故可改善粉體之流動性與溶解性。此外,本揭露所採用之特定溫度範圍的噴霧造粒製程,除了保留有機酸成分外,還在表面以調味成分做包覆形成調味殼層,包埋並保護其有機酸成分,最後以包覆形成保護層進行微膠囊顆粒的設計,以取代一般粉末混拌工段所添加的抗結塊劑,達到粉末的抗吸濕之保存性。整體而言,本揭露改善即溶茶飲品粉體之均勻性,並提升其流動性與即溶沖泡下的溶解性;以特定溫度包埋與保存發酵紅茶菌菇中的機能有機酸成分,以達到健康化的效果;提升即溶茶飲品的抗吸濕與保存性,無添加抗結塊劑的配方組合符合食品潔淨標籤(Clean label)的演進概念,強化保健品的健康價值。 The particle structure of the present invention is more uniform than that of general kombucha mushroom drink products, so the fluidity and solubility of the powder can be improved. In addition, the spray granulation process in a specific temperature range adopted by the present invention not only retains the organic acid components, but also forms a flavoring shell layer on the surface with a flavoring component to embed and protect the organic acid components. Finally, the microcapsule particles are designed with a protective layer formed by coating to replace the anti-caking agent added in the general powder mixing stage, so as to achieve the anti-hygroscopic preservation of the powder. In general, the present invention improves the uniformity of instant tea powder, and enhances its fluidity and solubility under instant brewing; embeds and preserves the functional organic acid components in fermented kombucha mushrooms at a specific temperature to achieve a health-enhancing effect; enhances the moisture absorption resistance and preservation of instant tea, and the formula combination without adding anti-caking agents complies with the evolution concept of food clean label (Clean label), enhancing the health value of health products.

本揭露之顆粒結構可直接添加至飲用水或其他飲品中,以增添風味。當本揭露之顆粒結構接觸飲品後,該顆粒結構之調味殼層可使功能性成分及調味劑釋放。於本案之一具體實施例中,該保護層接觸該飲品後將產生崩解、分解或溶解,使該功能性成分及該調味劑釋放於該飲品中。該功能性成分例如有機酸及纖維,有益於食用者之身體健康,且該功能性成分還可包括促進保存有機酸之有效成分,有益於促進吸收有機酸。此外,本揭露減少使用抗結塊劑,以包埋技術取代一般粉末混拌工段所添加的抗結塊劑,達到粉末的抗吸濕之保存性,因此增加整體保存時間。 The particle structure disclosed herein can be directly added to drinking water or other beverages to add flavor. When the particle structure disclosed herein contacts the beverage, the flavoring shell layer of the particle structure can release the functional ingredients and flavoring. In a specific embodiment of the present case, the protective layer will disintegrate, decompose or dissolve after contacting the beverage, so that the functional ingredients and the flavoring are released into the beverage. The functional ingredients, such as organic acids and fibers, are beneficial to the health of the consumer, and the functional ingredients may also include active ingredients that promote the preservation of organic acids, which are beneficial to promoting the absorption of organic acids. In addition, the present invention reduces the use of anti-caking agents and uses encapsulation technology to replace the anti-caking agents added in the general powder mixing stage, thereby achieving the anti-hygroscopic preservation of the powder, thereby increasing the overall shelf life.

因此,本揭露之顆粒結構可兼顧飲品之方便性、健康益處及保存效果,強化作為保健品的健康價值。 Therefore, the particle structure disclosed herein can take into account the convenience, health benefits and preservation effects of the beverage, and enhance the health value as a health product.

100:顆粒結構 100: Particle structure

11:紅茶粉 11: Black tea powder

12:纖維 12: Fiber

13:紅茶菌菇發酵液 13: Kombucha mushroom fermented liquid

21:香氣微膠囊 21: Aroma microcapsule

22:調味殼層 22: Seasoning the crust

23:保護層 23: Protective layer

圖1係本揭露之一具體實施例中製備顆粒結構的方法流程圖。 Figure 1 is a flow chart of a method for preparing a particle structure in one specific embodiment of the present disclosure.

圖2係本揭露之一具體實施例中之顆粒結構的剖面示意圖。 Figure 2 is a schematic cross-sectional view of a particle structure in one specific embodiment of the present disclosure.

以下係藉由特定的具體實施例說明本揭露之實施方式,本揭露所屬技術領域中具有通常知識者可依據本說明書所揭示之內容輕易地瞭解本揭露之精神、優點及功效。然而,本揭露之具體實施例並非用以限定本揭露,本揭露亦可藉由其它不同之實施方式加以實現或應用,本說明書所載各項細節亦可根據不同的觀點與應用,在不悖離本揭露之精神下賦予不同的變化或修飾。 The following is a specific embodiment to illustrate the implementation of the present disclosure. Those with ordinary knowledge in the technical field to which the present disclosure belongs can easily understand the spirit, advantages and effects of the present disclosure based on the content disclosed in this manual. However, the specific embodiment of the present disclosure is not used to limit the present disclosure. The present disclosure can also be implemented or applied through other different implementation methods. The details contained in this manual can also be given different changes or modifications based on different viewpoints and applications without deviating from the spirit of the present disclosure.

本文所述「包括」或「包含」組成分或步驟時,除非另有說明,否則可另包含其他組成分或其他步驟,而非排除該等其他組成分或其他步驟。此外,除非本文另有明確說明,否則本文所述單數形式之「一」及「該」包含複數指示物,且本文所述「或」係與「及/或」互換使用。 When "including" or "comprising" components or steps are described herein, other components or other steps may be included, but such other components or other steps are not excluded, unless otherwise specified herein. In addition, unless otherwise clearly specified herein, the singular forms "a", "an" and "the" described herein include plural referents, and "or" described herein is used interchangeably with "and/or".

本文所述之數值範圍係包含及可合併的,落在本文所述數值範圍內之任何數值,都可以作為最大值或最小值以導出次範圍;舉例而言,「0.2mm至0.5mm」之數值範圍應可理解為包含最小值0.2mm及最大值0.5mm之間的任何次範圍,例如:0.2mm至0.4mm、0.3mm至0.5mm及0.35mm至0.45mm等次範圍。此外,本文所述的多個數值可以選擇性被選為最大值或最小值以導出數值範圍;舉例而言,41℃、53℃、65℃ 可以導出41℃至53℃、41℃至65℃、53℃至65℃的數值範圍。另外,本文所述之百分比符號「%」,除非另有特別說明,否則表示重量百分比。 The numerical ranges described herein are inclusive and combinable. Any numerical value falling within the numerical range described herein can be used as the maximum or minimum value to derive a sub-range. For example, the numerical range of "0.2mm to 0.5mm" should be understood to include any sub-range between the minimum value of 0.2mm and the maximum value of 0.5mm, such as: 0.2mm to 0.4mm, 0.3mm to 0.5mm, and 0.35mm to 0.45mm. In addition, the multiple numerical values described herein can be selectively selected as the maximum or minimum value to derive a numerical range; for example, 41℃, 53℃, 65℃ can derive a numerical range of 41℃ to 53℃, 41℃ to 65℃, and 53℃ to 65℃. In addition, the percentage symbol "%" described herein, unless otherwise specified, represents weight percentage.

如本文中所使用,術語「約」通常係指數值旨在包含於給定的數值或範圍具有±20%、±10%、±5%、±1%、±0.5%、±0.1%的偏差。該數值偏差可因為,如實驗誤差;製備化合物、組成物、濃縮物、配方之測量標準誤或處理流程;本揭露之來源、製造、起始材料或成分的純度;類似的考量因素而出現。或者,當由所屬領域具中具有通常知識者考量時,術語「約」意指介於可接受的平均值的標準誤差內。除非明確地界定,所有數值範圍、量、數值、比例像是於本文中所揭露的材料、時段的持續時間、溫度、執行的條件、含量的比例、其類似物之定量,應理解為在所有情況下皆由術語「約」修飾。 As used herein, the term "about" generally means that the numerical value is intended to include a deviation of ±20%, ±10%, ±5%, ±1%, ±0.5%, ±0.1% from the given numerical value or range. Such numerical deviations may occur due to, for example, experimental errors; measurement standard errors or process flows in preparing compounds, compositions, concentrates, formulations; the purity of the source, manufacture, starting materials or components of the present disclosure; and similar considerations. Alternatively, when considered by one of ordinary skill in the art, the term "about" means within the standard error of an acceptable mean. Unless expressly defined otherwise, all numerical ranges, amounts, values, ratios, such as materials, durations of time, temperatures, conditions of execution, ratios of contents, and the like disclosed herein, should be understood to be modified in all cases by the term "about".

本揭露包埋有機酸及活性物質之顆粒結構包含核心、調味殼層及保護層,其中,該核心包含功能性成分,且該功能性成分可包含幫助保存有機酸之有效成分、載劑、賦形劑或其組合;該調味殼層包覆該核心;該保護層包覆整個顆粒結構。 The disclosed particle structure encapsulating organic acids and active substances comprises a core, a flavoring shell layer and a protective layer, wherein the core comprises a functional ingredient, and the functional ingredient may comprise an active ingredient that helps preserve the organic acid, a carrier, a formulator or a combination thereof; the flavoring shell layer encapsulates the core; and the protective layer encapsulates the entire particle structure.

本揭露用於製備包埋有機酸及活性物質之顆粒結構的方法包含:將功能性成分與載劑或賦形劑混合,將顆粒原料製成均勻的顆粒狀和核心,其中,該功能性成分包含纖維和紅茶菌菇發酵液;以及在該核心之表面以調味成分形成調味殼層,以包覆該核心;最後,以包埋技術完成保護層以包覆該調味殼層。上述載劑或賦形劑為食品上或生理上可接受之載劑或賦形劑。 The method disclosed herein for preparing a particle structure encapsulating organic acids and active substances comprises: mixing a functional ingredient with a carrier or a formulator, making the particle raw material into a uniform particle shape and a core, wherein the functional ingredient comprises fiber and fermented tea mushroom liquid; and forming a flavoring shell layer on the surface of the core with a flavoring ingredient to coat the core; finally, completing a protective layer with an encapsulation technique to coat the flavoring shell layer. The above-mentioned carrier or formulator is a carrier or formulator that is acceptable to food or physiologically.

於本揭露之一具體實施例中,該顆粒結構幫助保存有機酸, 故有益於促進吸收有機酸,該顆粒結構包含以下:核心、調味殼層及保護層。較佳地,平均粒徑為至少0.2mm。於本揭露之另一具體實施例中,該顆粒結構之平均粒徑為0.2mm至0.5mm,例如但不限於約0.25mm、0.30mm、0.35mm、0.4mm、0.45mm或0.5mm。於本揭露之又一具體實施例中,該顆粒結構之平均粒徑為0.3mm至0.5mm,較佳地,該顆粒結構之平均粒徑為0.4mm至0.5mm。於本揭露之至少一具體實施例中,該顆粒結構之粒徑為0.1mm至1.5mm,例如但不限於0.1mm、0.2mm、0.3mm、0.4mm、0.5mm、0.6mm、0.7mm、0.8mm、0.9mm、1.0mm、1.1mm、1.2mm、mm、1.3mm、1.4mm或1.5mm。 In one embodiment of the present disclosure, the particle structure helps preserve organic acids, and is therefore beneficial for promoting the absorption of organic acids. The particle structure comprises the following: a core, a seasoning shell layer, and a protective layer. Preferably, the average particle size is at least 0.2 mm. In another embodiment of the present disclosure, the average particle size of the particle structure is 0.2 mm to 0.5 mm, for example but not limited to about 0.25 mm, 0.30 mm, 0.35 mm, 0.4 mm, 0.45 mm, or 0.5 mm. In another embodiment of the present disclosure, the average particle size of the particle structure is 0.3 mm to 0.5 mm, preferably, the average particle size of the particle structure is 0.4 mm to 0.5 mm. In at least one specific embodiment of the present disclosure, the particle size of the particle structure is 0.1mm to 1.5mm, for example but not limited to 0.1mm, 0.2mm, 0.3mm, 0.4mm, 0.5mm, 0.6mm, 0.7mm, 0.8mm, 0.9mm, 1.0mm, 1.1mm, 1.2mm, mm, 1.3mm, 1.4mm or 1.5mm.

於本揭露之一具體實施例中,該顆粒結構之形狀係選自由圓球體、橢圓球體、立方體、圓柱體、長方體、四面體、椎體、星形、心形、扇形及貝殼形所組成群組之其中之一或其組合。 In a specific embodiment of the present disclosure, the shape of the particle structure is selected from one or a combination of the group consisting of sphere, ellipse, cube, cylinder, cuboid, tetrahedron, pyramid, star, heart, fan and shell.

於本揭露之一具體實施例中,該核心之粒徑或平均粒徑為0.01mm至0.3mm,例如但不限於0.02mm至0.1mm、0.02mm至0.15mm、0.06mm至0.08mm或0.1mm至0.3mm。 In one specific embodiment of the present disclosure, the particle size or average particle size of the core is 0.01mm to 0.3mm, for example but not limited to 0.02mm to 0.1mm, 0.02mm to 0.15mm, 0.06mm to 0.08mm or 0.1mm to 0.3mm.

於本揭露之一具體實施例中,該核心、調味殼層及保護層進一步包含食品上或生理上可接受之載劑或賦形劑。本揭露之食品上或生理上可接受之載劑或賦形劑包括但不限於澱粉(例如:米澱粉、小麥澱粉、玉米澱粉及小麥澱粉)、乳糖、蔗糖、葡萄糖、玉米甜味劑、糊精、環糊精、麥芽糖糊精、抗性澱粉、玉米來源可溶性纖維、菊苣纖維、寡糖、木質素、幾丁質、半纖維素、戊聚糖、β-葡聚糖、半乳甘露聚糖、甲殼素、樹膠、大豆膳食纖維、羧甲基澱粉鈉、丙酸羧基化澱粉、微晶纖維素、羧 甲基纖維素、羧甲基纖維素鈉、羥丙基甲基纖維素、甘露醇、山梨糖醇、硬脂酸鎂、磷酸二鈣、明膠、瓊脂、果膠、阿拉伯膠、海藻酸鈉、鹿角菜膠、刺槐豆膠、關華豆膠、塔拉膠、蒟蒻膠、黃耆膠、玉米糖膠、結蘭膠、卡德蘭膠、蟲膠、水或其中二者以上之組合。較佳地,該食品上或生理上可接受之載劑或賦形劑為澱粉、乳糖或其組合。較佳地,該食品上或生理上可接受之載劑或賦形劑為澱粉、寡糖、糊精、玉米來源可溶性纖維、菊苣纖維、果寡糖或其中兩者以上之組合。於本揭露之一具體實施例中,該保護層包含膠體,例如但不限於明膠、阿拉伯膠、海藻酸鈉、瓊脂、果膠、蟲膠、羧甲基纖維素、鹿角菜膠、玉米糖膠、褐藻酸鈉、結蘭膠、關華豆膠、塔拉膠或羥丙基甲基纖維素或其中兩者以上之組合。 In one embodiment of the present disclosure, the core, the seasoning shell layer and the protective layer further comprise a food or physiologically acceptable carrier or excipient. The food or physiologically acceptable carrier or excipient of the present disclosure includes but is not limited to starch (e.g., rice starch, wheat starch, corn starch and wheat starch), lactose, sucrose, glucose, corn sweetener, dextrin, cyclodextrin, maltodextrin, resistant starch, corn-derived soluble fiber, chicory fiber, oligosaccharides, lignin, chitin, hemicellulose, pentosan, β-glucan, galactomannan, chitosan, gum, soy Dietary fiber, sodium carboxymethyl starch, carboxylated starch propionate, microcrystalline cellulose, carboxymethyl cellulose, sodium carboxymethyl cellulose, hydroxypropyl methyl cellulose, mannitol, sorbitol, magnesium stearate, dicalcium phosphate, gelatin, agar, pectin, gum arabic, sodium alginate, carrageenan, locust bean gum, Guanhua bean gum, tara gum, konjac gum, astragalus gum, corn syrup, jelly gum, curdlan gum, worm gum, water or a combination of two or more thereof. Preferably, the food- or physiologically acceptable carrier or formulator is starch, lactose or a combination thereof. Preferably, the food- or physiologically acceptable carrier or excipient is starch, oligosaccharide, dextrin, corn-derived soluble fiber, chicory fiber, fructooligosaccharide, or a combination of two or more thereof. In a specific embodiment of the present disclosure, the protective layer comprises a colloid, such as but not limited to gelatin, gum arabic, sodium alginate, agar, pectin, wormwood, carboxymethyl cellulose, carrageenan, corn syrup, sodium alginate, gellan gum, guanyin, tara gum, or hydroxypropyl methyl cellulose, or a combination of two or more thereof.

本文中的術語「功能性成分」係指於食品中提供食用者超出基本營養價值且對健康有益處的成分,可增進食用者之身體健康及/或降低食用者罹患疾病之風險,例如:促進腸胃道健康、幫助消化、強健骨骼、保健牙齒、清新口氣、緩解壓力及緊張、改善或預防心血管疾病、糖尿病、肥胖症或骨質疏鬆症等。本揭露之功能性成分包括但不限於纖維、紅茶菌菇發酵液、益生質、益生菌、提升專注力之有效成分、膳食纖維、維生素、礦物質、類胡蘿蔔素、類黃酮、酶、抗氧化劑、植物雌激素、植物固醇、軟磷脂、脂肪酸、胺基酸、肌酸、蛋白質(例如大豆蛋白質或膠原蛋白)、咖啡因、胜肽、植物萃取物、菇菌類菌絲體、菇菌類子實體、蟲草類菌絲體、蟲草類子實體或其中二者以上之組合。於本揭露之一具體實施例中,該功能性成分係選自由紅茶菌菇發酵飲品製造過程中產生的有機酸包含但不限於醋酸。 The term "functional ingredient" in this article refers to ingredients in food that provide consumers with health benefits beyond basic nutritional value, which can improve the consumer's physical health and/or reduce the consumer's risk of disease, such as: promoting gastrointestinal health, aiding digestion, strengthening bones, protecting teeth, freshening breath, relieving stress and tension, improving or preventing cardiovascular disease, diabetes, obesity or osteoporosis, etc. The functional ingredients disclosed herein include but are not limited to fiber, fermented kombucha mushroom liquid, prebiotics, probiotics, active ingredients for improving concentration, dietary fiber, vitamins, minerals, carotenoids, flavonoids, enzymes, antioxidants, phytoestrogens, plant sterols, lecithin, fatty acids, amino acids, creatine, proteins (such as soy protein or collagen), caffeine, peptides, plant extracts, mushroom mycelium, mushroom fruiting bodies, cordyceps mycelium, cordyceps fruiting bodies, or a combination of two or more thereof. In a specific embodiment of the disclosure, the functional ingredient is selected from organic acids produced in the production process of kombucha mushroom fermented beverages, including but not limited to acetic acid.

本文中的術語「益生質」係指一種或多種食品成份,其可選擇性刺激益生菌在宿主消化道中的生長或活性,進而達到促進宿主健康之效果。於本揭露之一具體實施例中,該益生質係選自由醣類、糖醇及地靈粉末所組成群組之其中之一或其組合。較佳地,該醣類為寡醣或多醣。較佳地,該醣類係選自由木寡醣、大豆寡醣、膳食纖維、果寡醣(fructo-oligosaccharide,FOS)、異麥芽寡醣、乳果寡醣、乳酮糖、半乳寡醣(galacto-oligosaccharide,GOS)、棉子糖、菊苣纖維(菊糖)、聚糊精、聚葡萄糖、葡萄寡醣、甘露寡醣、阿拉伯寡醣、岩藻寡醣(fuco-oligosaccharide)、殼寡醣(chito-oligosaccharide)、乳糖醇及乳酮糖所組成群組之其中之一或其組合。於本揭露之一具體實施例中,該益生質係選自由膳食纖維、寡糖、低聚醣所組成群組之其中之一或其組合,較佳地,該寡糖為果寡糖、半乳寡糖、菊苣纖維或其中兩者以上之組合。 The term "prebiotic" herein refers to one or more food ingredients that can selectively stimulate the growth or activity of probiotics in the digestive tract of the host, thereby achieving the effect of promoting the health of the host. In a specific embodiment of the present disclosure, the prebiotic is selected from one or a combination of the group consisting of carbohydrates, sugar alcohols and dilinolenic acid powder. Preferably, the carbohydrate is an oligosaccharide or a polysaccharide. Preferably, the carbohydrate is selected from the group consisting of xylo-oligosaccharide, soybean oligosaccharide, dietary fiber, fructo-oligosaccharide (FOS), isomalto-oligosaccharide, lacto-oligosaccharide, lactulose, galacto-oligosaccharide (GOS), raffinose, chicory fiber (inulin), polydextrin, polydextrose, glucooligosaccharide, manno-oligosaccharide, arabino-oligosaccharide, fuco-oligosaccharide, chito-oligosaccharide, lactitol and lactulose, or a combination thereof. In a specific embodiment of the present disclosure, the prebiotic is selected from one of the groups consisting of dietary fiber, oligosaccharides, and oligosaccharides, or a combination thereof. Preferably, the oligosaccharide is fructooligosaccharide, galacto-oligosaccharide, chicory fiber, or a combination of two or more thereof.

本文中的術語「益生菌」係指有益於宿主健康且無致病性或低致病性的微生物。於本揭露之至少一具體實施例中,該益生菌係選自由芽孢乳酸菌(Bacillus coagulans)、比菲德氏菌(Bifidobacterium bifidum)、短雙歧桿菌(Bifidobacterium breve)、長雙歧桿菌(Bifidobacterium infants)、動物雙歧桿菌(Bifidobacterium lactis)、比菲德氏龍根菌(Bifidobacterium longum)、嗜酸乳桿菌(Lactobacillus acidophilus)、短乳桿菌(Lactobacillus brevis)、保加利亞乳桿菌(Lactobacillus bulgaricus)、乾酪乳桿菌(Lactobacillus casei)、酵素乳桿菌(Lactobacillus fermentum)、加氏乳桿菌(Lactobacillus gasseri)、瑞士乳桿菌(Lactobacillus helveticus)、約氏乳桿菌(Lactobacillus johnsonii)、副乾酪乳桿菌(Lactobacillus paracasei)、戊糖乳桿菌(Lactobacillus pentosus)、胚芽乳酸菌(Lactobacillus plantarum)、洛德乳桿菌(Lactobacillus reuteri)、鼠李糖乳桿菌(Lactobacillus rhamnosus)、唾液乳桿菌(Lactobacillus salivarius)、乳酸乳球菌(Lactococcus lactis)、嗜熱鏈球菌(Streptococcus thermophiles)、戊糖片球菌(Pediococcus pentosaceus)、乳酸片球菌(Pediococcus acidilactici)及青春雙歧桿菌(Bifidobacterium adolescentis)所組成群組之其中之一或其組合。較佳地,該益生菌係選自由動物雙歧桿菌(Bifidobacterium lactis)、酵素乳桿菌(Lactobacillus fermentum)、胚芽乳酸菌(Lactobacillus plantarum)及副乾酪乳桿菌(Lactobacillus paracasei)所組成群組之其中之一或其組合。 The term "probiotics" herein refers to microorganisms that are beneficial to the health of the host and are non-pathogenic or low-pathogenic. In at least one embodiment of the present disclosure, the probiotic is selected from the group consisting of Bacillus coagulans , Bifidobacterium bifidum , Bifidobacterium breve , Bifidobacterium infants , Bifidobacterium lactis , Bifidobacterium longum, Lactobacillus acidophilus , Lactobacillus brevis , Lactobacillus bulgaricus , Lactobacillus casei , Lactobacillus fermentum , Lactobacillus gasseri, Lactobacillus gasseri ), Lactobacillus helveticus , Lactobacillus johnsonii , Lactobacillus paracasei , Lactobacillus pentosus , Lactobacillus plantarum , Lactobacillus reuteri , Lactobacillus rhamnosus , Lactobacillus salivarius , Lactococcus lactis , Streptococcus thermophiles , Pediococcus pentosaceus , Pediococcus acidilactici ) and Bifidobacterium adolescentis or a combination thereof. Preferably, the probiotic is selected from the group consisting of Bifidobacterium lactis , Lactobacillus fermentum , Lactobacillus plantarum and Lactobacillus paracasei or a combination thereof.

於本揭露之至少一具體實施例中,該顆粒結構之紅茶粉係選自由錫蘭紅茶粉、伯爵紅茶粉、阿薩姆紅茶粉、大吉嶺紅茶粉所組成群組之其中之一或其組合。 In at least one specific embodiment of the present disclosure, the black tea powder in the particle structure is selected from one of the group consisting of Ceylon black tea powder, Earl Grey black tea powder, Assam black tea powder, and Darjeeling black tea powder, or a combination thereof.

於本揭露之至少一具體實施例中,該顆粒結構之纖維係選自由可溶性纖維、菊苣纖維、果寡糖所組成群組之其中之一或其組合。 In at least one specific embodiment of the present disclosure, the fiber of the particle structure is selected from one of the groups consisting of soluble fiber, chicory fiber, and fructooligosaccharide or a combination thereof.

於本揭露之至少一具體實施例中,該紅茶菌菇發酵液進一步包含有機酸或益生菌。於本揭露之一些具體實施例中,該紅茶菌菇發酵液之有機酸係選自由醋酸、檸檬酸、琥珀酸、草酸、葡萄糖醛酸及葡萄糖酸所組成群組之其中之一或其組合。於本揭露之一些具體實施例中,該益生菌為乳酸菌。 In at least one specific embodiment of the present disclosure, the fermented kombucha mushroom liquid further comprises an organic acid or a probiotic. In some specific embodiments of the present disclosure, the organic acid of the fermented kombucha mushroom liquid is selected from one or a combination of the group consisting of acetic acid, citric acid, succinic acid, oxalic acid, glucuronic acid and gluconic acid. In some specific embodiments of the present disclosure, the probiotic is a lactic acid bacterium.

本文中的術語「釋放」係指在特定外界環境下,例如但不限 於在液體中,本揭露之顆粒結構將其所包含之成分向外界遞送的特性。於本揭露之一具體實施例中,該保護層可以提升本揭露之顆粒結構之抗吸濕和保存性。於本揭露之一具體實施例中,該調味殼層具有釋放該功能性成分之作用,例如該保護層及調味殼層於液體中崩解、分解或溶解,以釋放該功能性成分。於本揭露之一具體實施例中,該液體為飲品,較佳為飲用水。 The term "release" herein refers to the property of the particle structure disclosed herein to deliver the components contained therein to the outside world in a specific external environment, such as but not limited to in a liquid. In one specific embodiment of the disclosure, the protective layer can enhance the moisture absorption resistance and preservation of the particle structure disclosed herein. In one specific embodiment of the disclosure, the flavoring shell layer has the function of releasing the functional component, for example, the protective layer and the flavoring shell layer disintegrate, decompose or dissolve in the liquid to release the functional component. In one specific embodiment of the disclosure, the liquid is a beverage, preferably drinking water.

本文中的術語「調味劑」係指食品上或生理上可接受之天然、合成或半合成物質,其在食用者體內誘發味覺、嗅覺、觸覺等感受,其中,在食用者體內誘發甜味感受者為「甜味劑」;在食用者體內誘發酸味感受者為「酸味劑」。本揭露之甜味劑包括但不限於天然植物來源所獲得之汁液、粉末、糖漿、萃取物、濃縮物或香料,該天然植物來源例如:巧克力、檸檬、草莓、香蕉、莓果、芒果、哈密瓜、百香果、鳳梨、水蜜桃、櫻桃、肉桂、蘋果、茴香、蜂蜜、梨、楓糖、葡萄、葡萄柚、柳橙、橘子、西瓜、羅漢果、蘑菇或香草;醣類甜味劑包括但不限於乳糖、半乳寡糖、蔗糖、果糖、麥芽糖、葡萄糖或砂糖;糖醇類甜味劑包括但不限於木糖醇、甘露糖醇、山梨糖醇、赤藻糖醇、異麥芽酮糖醇、甜菊糖苷、赤藻糖醇或乳糖醇;以及人工甜味劑包括但不限於阿斯巴甜或其衍生物、乙醯磺胺酸鉀、新橙皮苷二氫查耳酮、甘草素、醋磺內酯鉀或蔗糖素。於本揭露之一具體實施例中,該甜味劑為羅漢果萃取物、甜菊糖苷、蘑菇萃取物或其中兩者以上之組合。另一具體實施例中,該甜味劑為羅漢果萃取物、蔗糖素、醋磺內酯鉀、甜菊糖苷或兩者以上之組合。本揭露之酸味劑包括但不限於檸檬酸、檸檬酸鈉、檸檬酸三鈉、己二酸、丁二酸、丁二酸單鈉乳酸、乳酸 鈉、蘋果酸、蘋果酸鈉、磷酸、酒石酸、酒石酸鈉、葡萄糖酸、葡萄糖酸鉀、葡萄糖酸鈉、乙酸、冰乙酸或胺基乙酸。於本揭露之一具體實施例中,該保護層另包含甜味劑、酸味劑或其組合,較佳地,該甜味劑為天然植物來源所獲得之糖漿、萃取物、濃縮物或香料、糖醇類甜味劑或其組合;更佳地,該甜味劑為羅漢果萃取物、甜菊糖苷、蔗糖素、醋磺內酯鉀或其中兩者以上之組合。於本揭露之一具體實施例中,該保護層具有釋放該調味劑之作用,例如該保護層於液體中崩解、分解或溶解,以釋放該調味劑。於本揭露之一具體實施例中,該液體為飲用水。 The term "flavoring agent" herein refers to a natural, synthetic or semi-synthetic substance that is acceptable in food or physiologically, and which induces taste, smell, touch and other sensations in the body of the consumer. Among them, the one that induces sweetness in the body of the consumer is a "sweetener"; the one that induces sourness in the body of the consumer is a "sour agent". The sweeteners disclosed herein include but are not limited to juices, powders, syrups, extracts, concentrates or spices obtained from natural plant sources, such as chocolate, lemon, strawberry, banana, berry, mango, cantaloupe, passion fruit, pineapple, peach, cherry, cinnamon, apple, fennel, honey, pear, maple syrup, grape, grapefruit, orange, tangerine, watermelon, monk fruit, mushroom or vanilla; carbohydrate sweeteners The sweetener includes but is not limited to lactose, galacto-oligosaccharide, sucrose, fructose, maltose, glucose or granulated sugar; the sugar alcohol sweetener includes but is not limited to xylitol, mannitol, sorbitol, erythritol, isomalt, steviol glycoside, erythritol or lactitol; and the artificial sweetener includes but is not limited to aspartame or its derivatives, acesulfame potassium, neohesperidin dihydrochalcone, glycyrrhizin, acesulfame potassium or sucralose. In one embodiment of the present disclosure, the sweetener is a Luo Han Guo extract, steviol glycoside, mushroom extract or a combination of two or more thereof. In another embodiment, the sweetener is a Luo Han Guo extract, sucralose, acesulfame potassium, steviol glycoside or a combination of two or more thereof. The acidulants disclosed herein include but are not limited to citric acid, sodium citrate, trisodium citrate, adipic acid, succinic acid, monosodium succinate, lactic acid, sodium lactate, apple acid, sodium appleate, phosphoric acid, tartaric acid, sodium tartrate, gluconic acid, potassium gluconate, sodium gluconate, acetic acid, glacial acetic acid or aminoacetic acid. In a specific embodiment of the present disclosure, the protective layer further comprises a sweetener, an acidulant or a combination thereof. Preferably, the sweetener is a syrup, extract, concentrate or flavor obtained from a natural plant source, a sugar alcohol sweetener or a combination thereof; more preferably, the sweetener is a monk fruit extract, stevioside, sucralose, acesulfame potassium or a combination of two or more thereof. In one embodiment of the present disclosure, the protective layer has the function of releasing the flavoring agent, for example, the protective layer disintegrates, decomposes or dissolves in the liquid to release the flavoring agent. In one embodiment of the present disclosure, the liquid is drinking water.

於本揭露之一具體實施例中,該保護層無添加抗結塊劑。 In one specific embodiment of the present disclosure, the protective layer does not contain an anti-caking agent.

於本揭露之一具體實施例中,該保護層之厚度為0.01mm至0.02mm、0.03mm至0.05mm、或0.015mm至0.025mm。 In one specific embodiment of the present disclosure, the thickness of the protective layer is 0.01mm to 0.02mm, 0.03mm to 0.05mm, or 0.015mm to 0.025mm.

於本揭露之一具體實施例中,該顆粒結構包含65.5%至90.8%之功能性成分。較佳地,該顆粒結構包含10%至30%之含紅茶菌菇發酵液。於本揭露之一具體實施例中,該顆粒結構包含1%至10%之紅茶粉。較佳地,該顆粒結構包含50%至70%之纖維。更佳地,該顆粒結構包含20%至30%之紅茶菌菇發酵液、3%至8%之紅茶粉及60%至70%之纖維。 In one embodiment of the present disclosure, the particle structure contains 65.5% to 90.8% of functional ingredients. Preferably, the particle structure contains 10% to 30% of fermented tea containing tea. In one embodiment of the present disclosure, the particle structure contains 1% to 10% of black tea powder. Preferably, the particle structure contains 50% to 70% of fiber. More preferably, the particle structure contains 20% to 30% of fermented tea containing tea, 3% to 8% of black tea powder and 60% to 70% of fiber.

於本揭露之一具體實施例中,係使用流動床噴霧造粒製程將該功能性成分與該載劑或該賦形劑混合,以達到快速且均勻混合之目的。 In one specific embodiment of the present disclosure, the functional ingredient is mixed with the carrier or the excipient using a fluidized bed spray granulation process to achieve rapid and uniform mixing.

以下係藉由具體的製備例及實施例進一步說明本揭露之特點及其功效,但非用於限制本揭露之範圍。 The following is a detailed description of the features and effects of the present disclosure through specific preparation examples and implementation examples, but is not intended to limit the scope of the present disclosure.

製備例Preparation example

圖1顯示製備本揭露之顆粒結構的方法,其包含下列步驟: 步驟(a):將玉米來源可溶性纖維、即溶紅茶粉、菊苣纖維等功能性成分進行過篩;步驟(b):將過篩後之成分以流動床乾燥設備進行57℃至63℃混合及乾燥;步驟(c):將混合及乾燥後之成分進行噴霧造粒程序以形成核心,其過程中可視需要加入水、食用香料、甜味劑、酸味劑、膠體或其中兩者以上之組合;步驟(d):加入水、食用香料、甜味劑、酸味劑、膠體或其中兩者以上之組合,以形成包覆核心之調味殼層;步驟(e):依序添加紅茶菌發酵液成分、香氣之微膠囊及抗吸濕之膠體組合成分針對顆粒結構進行乾燥;步驟(f):針對顆粒結構進行整粒,以達到所需之平均粒徑及形狀。 FIG1 shows a method for preparing the granular structure disclosed herein, which comprises the following steps: Step (a): Screening the functional ingredients such as corn-derived soluble fiber, instant black tea powder, chicory fiber, etc.; Step (b): Mixing and drying the screened ingredients at 57°C to 63°C using a fluidized bed drying device; Step (c): Performing a spray granulation process on the mixed and dried ingredients to form a core, during which water, edible flavorings, Sweetener, acidulant, colloid or a combination of two or more thereof; Step (d): adding water, edible flavor, sweetener, acidulant, colloid or a combination of two or more thereof to form a seasoning shell layer covering the core; Step (e): sequentially adding kombucha fermentation liquid component, aroma microcapsule and anti-hygroscopic colloid component to dry the particle structure; Step (f): performing particle size adjustment on the particle structure to achieve the required average particle size and shape.

實施例1:顆粒結構之剖面Example 1: Cross-section of particle structure

如圖2所示,本揭露之顆粒結構100包含紅茶粉11、纖維12、紅茶菌菇發酵液13、調味殼層22及保護層23,其中,該調味殼層22包含香氣微膠囊21。 As shown in FIG. 2 , the particle structure 100 disclosed herein comprises black tea powder 11, fiber 12, black tea mushroom fermentation liquid 13, a seasoning shell layer 22 and a protective layer 23, wherein the seasoning shell layer 22 comprises an aroma microcapsule 21.

實施例2:噴霧造粒溫度對有機酸保留之影響Example 2: Effect of spray granulation temperature on organic acid retention

以上述製備例所述方法,於37℃至43℃、57℃至63℃、77℃至83℃之噴霧造粒溫度範圍下,分別製備顆粒結構之實例A及實例A’、實例B及實例B’、實例C,並於製備完成時及常溫儲藏1個月後測定每克實例中的醋酸含量(毫克),結果如下表1及表2所示:

Figure 111150976-A0305-12-0014-1
By the method described in the above preparation example, at the spray granulation temperature range of 37°C to 43°C, 57°C to 63°C, and 77°C to 83°C, Example A and Example A', Example B and Example B', and Example C of the granule structure were prepared respectively, and the acetic acid content (mg) per gram of the example was measured after the preparation was completed and after 1 month of storage at room temperature. The results are shown in Tables 1 and 2 below:
Figure 111150976-A0305-12-0014-1

Figure 111150976-A0305-12-0014-2
Figure 111150976-A0305-12-0014-2

上表1顯示於顆粒結構製備完成時,實例B之醋酸含量高於實例A及實例C。上表2則顯示經常溫儲藏1個月後,實例B’之醋酸耗損率低於實例A’。上述數據表示使用57℃至63℃之噴霧造粒溫度所形成的顆粒結構具有較佳的醋酸保留效果。 Table 1 above shows that when the granular structure is prepared, the acetic acid content of Example B is higher than that of Example A and Example C. Table 2 above shows that after being stored at room temperature for one month, the acetic acid consumption rate of Example B' is lower than that of Example A'. The above data indicate that the granular structure formed using a spray granulation temperature of 57°C to 63°C has a better acetic acid retention effect.

實施例3:流動性測試 Example 3: Fluidity test

測定實施例2中的實例B與市售品之總體密度(bulk density)及振實密度(tapped density),再進一步計算其卡爾指數(Carr’s index)及豪斯納比(Hausner ratio),結果如下表3所示:

Figure 111150976-A0305-12-0015-3
The bulk density and tapped density of Example B in Example 2 and the commercial product were measured, and the Carr's index and Hausner ratio were further calculated. The results are shown in Table 3 below:
Figure 111150976-A0305-12-0015-3

總體密度係指未經振實之顆粒樣品的質量與其總體積(包括顆粒間的空隙體積)之比值,一般而言,其值越低的產品,其顆粒粒徑較大,相對利於包裝、運輸和儲存。振實密度則是指對裝有顆粒樣品的容器振動以使顆粒處於緊密填充狀態後的密度。卡爾指數及豪斯納比為流動性指標,其值越低,表示顆粒樣品之流動性越高。由上表可知,實例B之總體密度、卡爾指數及豪斯納比皆小於市售品,表示本揭露之成品相較於其它市售品具有較佳的流動性與充填適性,且更有利於包裝、運輸和儲存。 The overall density refers to the ratio of the mass of the uncompacted particle sample to its total volume (including the volume of the voids between the particles). Generally speaking, the lower the value, the larger the particle size of the product, which is relatively convenient for packaging, transportation and storage. The tapped density refers to the density after the container containing the particle sample is vibrated to make the particles in a densely packed state. The Karl index and Hausner ratio are flowability indicators. The lower the value, the higher the flowability of the particle sample. As can be seen from the above table, the overall density, Karl index and Hausner ratio of Example B are all lower than those of commercial products, indicating that the finished product disclosed herein has better flowability and filling suitability than other commercial products, and is more convenient for packaging, transportation and storage.

上述製備例或實施例僅為例示性說明,而非用於限制本揭露。本領域之通常知識者均可在不違背本揭露之精神及範疇下,對上述實施例進行修飾與改變。因此,本揭露之權利保護範圍係由所附之申請專利範圍所定義,只要不影響本揭露之效果及實施目的,應涵蓋於此公開技術內容中。 The above preparation examples or implementation examples are only illustrative and are not intended to limit the present disclosure. People with ordinary knowledge in this field can modify and change the above implementation examples without violating the spirit and scope of the present disclosure. Therefore, the scope of protection of the present disclosure is defined by the scope of the attached patent application. As long as it does not affect the effect and implementation purpose of the present disclosure, it should be included in the content of this public technology.

100:顆粒結構 100: Particle structure

11:紅茶粉 11: Black tea powder

12:纖維 12: Fiber

13:紅茶菌菇發酵液 13: Kombucha mushroom fermented liquid

21:香氣微膠囊 21: Aroma microcapsule

22:調味殼層 22: Seasoning the crust

23:保護層 23: Protective layer

Claims (8)

一種製備顆粒結構的方法,包含:將功能性成分過篩,其中,該功能性成分包含纖維;將過篩後之成分在57℃至63℃下進行混合及乾燥;將混合及乾燥後之成分在57℃至63℃下進行噴霧造粒程序,其中,該噴霧造粒程序包含添加紅茶菌菇發酵液以形成核心;形成包覆該核心之調味殼層;以及形成包覆該調味殼層之保護層。 A method for preparing a granular structure, comprising: screening a functional ingredient, wherein the functional ingredient comprises fiber; mixing and drying the screened ingredients at 57°C to 63°C; performing a spray granulation process on the mixed and dried ingredients at 57°C to 63°C, wherein the spray granulation process comprises adding a fermented liquid of kombucha mushrooms to form a core; forming a seasoning shell layer covering the core; and forming a protective layer covering the seasoning shell layer. 如請求項1所述之顆粒結構,其中,該功能性成分進一步包含紅茶粉。 The particle structure as described in claim 1, wherein the functional ingredient further comprises black tea powder. 如請求項1所述之顆粒結構,其中,該顆粒結構之平均粒徑為0.2mm至0.5mm。 The particle structure as described in claim 1, wherein the average particle size of the particle structure is 0.2 mm to 0.5 mm. 如請求項1所述之顆粒結構,其中,該纖維係可溶性纖維、果寡糖或其組合。 The particle structure as described in claim 1, wherein the fiber is soluble fiber, fructooligosaccharide or a combination thereof. 如請求項1所述之顆粒結構,其中,該紅茶菌菇發酵液包含有機酸或益生菌。 The granular structure as described in claim 1, wherein the kombucha mushroom fermentation liquid contains organic acid or probiotics. 如請求項5所述之顆粒結構,其中,該有機酸係選自由醋酸、檸檬酸、琥珀酸、草酸、葡萄糖醛酸及葡萄糖酸所組成群組之其中之一或其組合,且該益生菌為乳酸菌。 The particle structure as described in claim 5, wherein the organic acid is selected from one or a combination of the group consisting of acetic acid, citric acid, succinic acid, oxalic acid, glucuronic acid and gluconic acid, and the probiotic is lactic acid bacteria. 如申請專利範圍第1項所述之顆粒結構,其中,該調味殼層包含香氣微膠囊及調味成分。 The particle structure as described in item 1 of the patent application scope, wherein the flavoring shell contains aroma microcapsules and flavoring ingredients. 一種由請求項1所述方法製備之顆粒結構,包含: 該核心,其包含該功能性成分及該紅茶菌菇發酵液,其中,該紅茶菌菇發酵液在該核心外層且包含有機酸;該調味殼層,其包覆該核心;以及該保護層,其包覆該調味殼層;其中,該顆粒結構之平均粒徑為至少0.2mm。 A particle structure prepared by the method described in claim 1, comprising: The core, which comprises the functional ingredient and the fermented tea mushroom liquid, wherein the fermented tea mushroom liquid is on the outer layer of the core and comprises an organic acid; the seasoning shell layer, which covers the core; and the protective layer, which covers the seasoning shell layer; wherein the average particle size of the particle structure is at least 0.2 mm.
TW111150976A 2022-12-30 2022-12-30 Granular structure with active compound of organic acids and method for preparing the same TWI868553B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
TW111150976A TWI868553B (en) 2022-12-30 2022-12-30 Granular structure with active compound of organic acids and method for preparing the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
TW111150976A TWI868553B (en) 2022-12-30 2022-12-30 Granular structure with active compound of organic acids and method for preparing the same

Publications (2)

Publication Number Publication Date
TW202425955A TW202425955A (en) 2024-07-01
TWI868553B true TWI868553B (en) 2025-01-01

Family

ID=92929084

Family Applications (1)

Application Number Title Priority Date Filing Date
TW111150976A TWI868553B (en) 2022-12-30 2022-12-30 Granular structure with active compound of organic acids and method for preparing the same

Country Status (1)

Country Link
TW (1) TWI868553B (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105747061B (en) * 2016-02-29 2019-02-12 丽水学院 A kind of method for preparing kombucha solid beverage
TWM605965U (en) * 2020-06-17 2021-01-01 葡萄王生技股份有限公司 Granular structure for encapsulating probiotics
TWM605957U (en) * 2020-06-11 2021-01-01 葡萄王生技股份有限公司 Calcium-containing granular structure

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105747061B (en) * 2016-02-29 2019-02-12 丽水学院 A kind of method for preparing kombucha solid beverage
TWM605957U (en) * 2020-06-11 2021-01-01 葡萄王生技股份有限公司 Calcium-containing granular structure
TWM605965U (en) * 2020-06-17 2021-01-01 葡萄王生技股份有限公司 Granular structure for encapsulating probiotics

Also Published As

Publication number Publication date
TW202425955A (en) 2024-07-01

Similar Documents

Publication Publication Date Title
Sarao et al. Probiotics, prebiotics, and microencapsulation: A review
CN101541194B (en) Probiotic oral dosage forms
US20120015075A1 (en) Chewable supplement with live microorganisms
CN114698849A (en) A kind of probiotic composition and its preparation method and application
JP2012175977A (en) Composition for administering microorganism into intestine
CN116634889A (en) Improved protein digestion and amino acid bioavailability by probiotic strains
CN103347398A (en) Soluble milk-based tablet surface-treated with carbohydrate
TWM605965U (en) Granular structure for encapsulating probiotics
CN107835641A (en) Glyceryl rubber candy and foam confectionary products with probiotics
JP6945888B1 (en) Composition for improving immune function
TWI868553B (en) Granular structure with active compound of organic acids and method for preparing the same
KR20250152039A (en) Food composition with snow melt texture and preparing method thereof
KR102535339B1 (en) Glycerin-based and protein-based foamed candy products with probiotic bacteria
TWM641394U (en) Granular structure with active compound of organic acids
CN103997900A (en) Soluble non-dairy creamer tablet surface-treated with carbohydrate
CN109259245A (en) A kind of the probiotics Intestine-lubricatinhealth-care health-care food and preparation method stable by fiber
Kandur et al. Oral pharmabiotic tablet formulations
JP2612001B2 (en) Granules containing useful intestinal bacteria and method for producing the same
CN105724571B (en) Isotonic probiotics preparation and preparation method thereof
JP7440144B1 (en) Oral composition
TWM602905U (en) Probiotic particles with core-shell structure
Şenöztop et al. A comprehensive review on the development of probiotic supplemented confectioneries
KR102907346B1 (en) Food composition with snow melt texture
CN118383445A (en) Composition containing probiotics and probiotic tablet candy prepared by using same
JP2020129986A (en) Oral composition