RU2008118478A - Способ получения полиизоциануратного полиуретанового материала - Google Patents
Способ получения полиизоциануратного полиуретанового материала Download PDFInfo
- Publication number
- RU2008118478A RU2008118478A RU2008118478/04A RU2008118478A RU2008118478A RU 2008118478 A RU2008118478 A RU 2008118478A RU 2008118478/04 A RU2008118478/04 A RU 2008118478/04A RU 2008118478 A RU2008118478 A RU 2008118478A RU 2008118478 A RU2008118478 A RU 2008118478A
- Authority
- RU
- Russia
- Prior art keywords
- polyisocyanate
- isocyanate
- weight
- amount
- polyol
- Prior art date
Links
- 239000000463 material Substances 0.000 title claims abstract 7
- 229920000582 polyisocyanurate Polymers 0.000 title claims abstract 3
- 239000011495 polyisocyanurate Substances 0.000 title claims abstract 3
- 239000004814 polyurethane Substances 0.000 title claims abstract 3
- 229920002635 polyurethane Polymers 0.000 title claims abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 229920001228 polyisocyanate Polymers 0.000 claims abstract 18
- 239000005056 polyisocyanate Substances 0.000 claims abstract 18
- 238000000034 method Methods 0.000 claims abstract 8
- 150000001875 compounds Chemical class 0.000 claims abstract 7
- 229920005862 polyol Polymers 0.000 claims abstract 7
- 150000003077 polyols Chemical class 0.000 claims abstract 7
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 claims abstract 6
- 125000006353 oxyethylene group Chemical group 0.000 claims abstract 3
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract 2
- 239000003054 catalyst Substances 0.000 claims abstract 2
- 238000006243 chemical reaction Methods 0.000 claims abstract 2
- 239000012948 isocyanate Substances 0.000 claims abstract 2
- 150000002513 isocyanates Chemical class 0.000 claims abstract 2
- 239000007788 liquid Substances 0.000 claims abstract 2
- 229920000570 polyether Polymers 0.000 claims abstract 2
- 238000005829 trimerization reaction Methods 0.000 claims abstract 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/09—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/09—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture
- C08G18/092—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture oligomerisation to isocyanurate groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4833—Polyethers containing oxyethylene units
- C08G18/4837—Polyethers containing oxyethylene units and other oxyalkylene units
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7657—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
- C08G18/7664—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups
- C08G18/7671—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups containing only one alkylene bisphenyl group
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyurethanes Or Polyureas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1. Способ получения полиизоциануратного полиуретанового материала, включающий взаимодействие полиизоцианата и реакционно-способной по отношению к изоцианату композиции, где взаимодействие проводят при изоцианатном индексе от 1600 до 100000 и в присутствии катализатора тримеризации, где полиизоцианат содержит а) 75-100 мас.% дифенилметандиизоцианата, содержащего по меньшей мере 40 мас.%, 4,4'-дифенилметандиизоцианата и/или варианта указанного дифенилметандиизоцианата, каковой вариант является жидким при 25оС и имеет величину NCO по меньшей мере 20 мас.% (полиизоцианат а), и b) 25-0 мас.% другого полиизоцианата (полиизоцианат b), причем количество полиизоцианата а) и полиизоцианата b) рассчитано на суммарное количество этого полиизоцианата а) и полиизоцианата b), и где реакционно-способная по отношению к изоцианату композиция содержит а) 80-100 мас.% полиэфирполиола, имеющего среднюю номинальную функциональность 2-6, среднюю эквивалентную массу 1100-5000 и содержание оксиэтилена (ЕО) 65-100 мас.%, и b) 20-0 мас.% одного или нескольких других реакционно-способных по отношению к изоцианату соединений, где количество полиола а) и соединения b) рассчитано на суммарное количество этого полиола а) и соединения b) и где содержание жестких блоков составляет по меньшей мере 50%. ! 2. Способ по п.1, где эквивалентный вес составляет 1100-4000 и индекс составляет 1700-50000. ! 3. Способ по п.1 или 2, где содержание оксиэтилена составляет 65-90 мас.%, количество полиола а) составляет 90-100% и количество соединения b) составляет 0-10 мас.%. ! 4. Способ по п.1 или 2, в котором материал имеет плотность более 100 кг/м3. ! 5. Способ по п.3, в котором материал имеет плотность более 100 кг/м3. ! 6. Материал, изг�
Claims (7)
1. Способ получения полиизоциануратного полиуретанового материала, включающий взаимодействие полиизоцианата и реакционно-способной по отношению к изоцианату композиции, где взаимодействие проводят при изоцианатном индексе от 1600 до 100000 и в присутствии катализатора тримеризации, где полиизоцианат содержит а) 75-100 мас.% дифенилметандиизоцианата, содержащего по меньшей мере 40 мас.%, 4,4'-дифенилметандиизоцианата и/или варианта указанного дифенилметандиизоцианата, каковой вариант является жидким при 25оС и имеет величину NCO по меньшей мере 20 мас.% (полиизоцианат а), и b) 25-0 мас.% другого полиизоцианата (полиизоцианат b), причем количество полиизоцианата а) и полиизоцианата b) рассчитано на суммарное количество этого полиизоцианата а) и полиизоцианата b), и где реакционно-способная по отношению к изоцианату композиция содержит а) 80-100 мас.% полиэфирполиола, имеющего среднюю номинальную функциональность 2-6, среднюю эквивалентную массу 1100-5000 и содержание оксиэтилена (ЕО) 65-100 мас.%, и b) 20-0 мас.% одного или нескольких других реакционно-способных по отношению к изоцианату соединений, где количество полиола а) и соединения b) рассчитано на суммарное количество этого полиола а) и соединения b) и где содержание жестких блоков составляет по меньшей мере 50%.
2. Способ по п.1, где эквивалентный вес составляет 1100-4000 и индекс составляет 1700-50000.
3. Способ по п.1 или 2, где содержание оксиэтилена составляет 65-90 мас.%, количество полиола а) составляет 90-100% и количество соединения b) составляет 0-10 мас.%.
4. Способ по п.1 или 2, в котором материал имеет плотность более 100 кг/м3.
5. Способ по п.3, в котором материал имеет плотность более 100 кг/м3.
6. Материал, изготовленный согласно способу по пп.1-5.
7. Материал, получаемый согласно способу по пп.1-5.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP05109530 | 2005-10-13 | ||
| EP05109530.5 | 2005-10-13 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2008118478A true RU2008118478A (ru) | 2009-11-20 |
| RU2415877C2 RU2415877C2 (ru) | 2011-04-10 |
Family
ID=35788185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2008118478/04A RU2415877C2 (ru) | 2005-10-13 | 2006-09-29 | Способ получения полиизоциануратного полиуретанового материала |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US8785570B2 (ru) |
| EP (1) | EP1940899B1 (ru) |
| JP (1) | JP5044561B2 (ru) |
| KR (1) | KR20080057271A (ru) |
| CN (1) | CN101283012B (ru) |
| AT (1) | ATE438669T1 (ru) |
| AU (1) | AU2006301367B2 (ru) |
| BR (1) | BRPI0616662B1 (ru) |
| CA (1) | CA2625689C (ru) |
| DE (1) | DE602006008337D1 (ru) |
| ES (1) | ES2327569T3 (ru) |
| RU (1) | RU2415877C2 (ru) |
| WO (1) | WO2007042411A1 (ru) |
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| CA2523481C (en) * | 2003-06-12 | 2012-05-01 | Huntsman International Llc | Process for preparing a polyisocyanurate polyurethane material |
| EP1940899B1 (en) | 2005-10-13 | 2009-08-05 | Huntsman International Llc | Process for preparing polyisocyanurate polyurethane material |
| DE602007007903D1 (de) * | 2006-02-21 | 2010-09-02 | Huntsman Int Llc | Herstellungsverfahren für einen polyisocyanuratverbund |
| ES2332955T3 (es) | 2006-06-14 | 2010-02-15 | Huntsman International Llc | Panel de material compuesto. |
| CN101945910B (zh) * | 2008-02-14 | 2013-09-18 | 亨茨曼国际有限公司 | 具有高的硬嵌段含量的弹性体材料和制备它们的方法 |
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| EP2182017A1 (en) * | 2008-07-10 | 2010-05-05 | Huntsman International Llc | A polyisocyanurate-based syntactic coating for offshore applications |
| CN102131840B (zh) * | 2008-08-28 | 2014-01-29 | 亨茨曼国际有限公司 | 通过多元醇和酸酐的反应获得的混合物及其在聚异氰酸酯中用来制备聚异氰脲酸酯的用途 |
| CN102482489B (zh) * | 2009-06-09 | 2014-02-19 | 亨茨曼国际有限公司 | 包含基质的材料及其制备方法 |
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| DE19918726C2 (de) | 1999-04-24 | 2002-04-11 | Bayer Ag | Offenzellige Polyurethanhartschaumstoffe |
| US6509392B1 (en) * | 2000-01-25 | 2003-01-21 | H.A. International Llc | Foundry binder and process |
| EP1167414A1 (en) | 2000-06-29 | 2002-01-02 | Huntsman International Llc | Process for making rigid polyurethane foams having high adhesion |
| EP1172387A1 (en) | 2000-07-14 | 2002-01-16 | Huntsman International Llc | Process for preparing an elastomer |
| EP1178063A1 (en) * | 2000-08-01 | 2002-02-06 | Huntsman International Llc | Process for preparing a polyurethane material |
| FR2812653A1 (fr) * | 2000-08-03 | 2002-02-08 | Michelin Soc Tech | Colle pour compositions de caoutchouc, son procede de preparation et articles comportant cette colle |
| JP4472856B2 (ja) * | 2000-09-19 | 2010-06-02 | 有限会社サン・イースト・リサーチ | 親水性連続微細気泡ポリイソシアヌレートフォームの製造方法並びに親水性連続微細気泡ポリイソシアヌレートフォーム |
| IT1319215B1 (it) * | 2000-10-16 | 2003-09-26 | Industrialesud Spa | Prodotto multistrato, suo uso per la realizzazione di articolileggeri, fonoassorbenti, autoportanti e articoli ottenibili con detto |
| DE10145458B4 (de) | 2001-09-14 | 2014-03-20 | Basf Se | Verfahren zur Herstellung von Urethan- und überwiegend Isocyanuratgruppen aufweisenden Polyurethanhartschaumstoffen |
| US6773756B2 (en) | 2002-03-20 | 2004-08-10 | Bayer Polymers Llc | Process to manufacture three dimensionally shaped substrate for sound abatement |
| US6729045B2 (en) * | 2002-10-02 | 2004-05-04 | Dale F. Isackson | Tap device for clogging shoes |
| US20040069971A1 (en) | 2002-10-15 | 2004-04-15 | Witteveen Martijn M. | Polyol compositions and rigid polyisocyanurate foams prepared therefrom |
| DE10257633A1 (de) | 2002-12-09 | 2004-06-24 | Basf Ag | Verbundelemente, insbesondere gedämmte Rohre |
| US20040249078A1 (en) * | 2003-06-04 | 2004-12-09 | Honeywell International, Inc. | Foam catalyst systems |
| CA2523481C (en) * | 2003-06-12 | 2012-05-01 | Huntsman International Llc | Process for preparing a polyisocyanurate polyurethane material |
| DE10359024A1 (de) | 2003-12-15 | 2005-07-21 | Basf Ag | Zinnfreie Polyurethanschaumstoffe |
| US7763341B2 (en) * | 2004-01-23 | 2010-07-27 | Century-Board Usa, Llc | Filled polymer composite and synthetic building material compositions |
| ITRM20040375A1 (it) * | 2004-07-23 | 2004-10-23 | Tekno Garden S R L | Materiali compositi a base di resine leganti, procedimenti per la loro preparazione e usi. |
| EP1940899B1 (en) | 2005-10-13 | 2009-08-05 | Huntsman International Llc | Process for preparing polyisocyanurate polyurethane material |
| CN101283011B (zh) * | 2005-10-13 | 2013-04-10 | 亨茨曼国际有限公司 | 聚异氰脲酸酯聚氨酯材料的制备方法 |
| DE602007007903D1 (de) * | 2006-02-21 | 2010-09-02 | Huntsman Int Llc | Herstellungsverfahren für einen polyisocyanuratverbund |
-
2006
- 2006-09-29 EP EP06793910A patent/EP1940899B1/en active Active
- 2006-09-29 CA CA2625689A patent/CA2625689C/en active Active
- 2006-09-29 JP JP2008534979A patent/JP5044561B2/ja not_active Expired - Fee Related
- 2006-09-29 KR KR1020087008753A patent/KR20080057271A/ko not_active Ceased
- 2006-09-29 WO PCT/EP2006/066889 patent/WO2007042411A1/en not_active Ceased
- 2006-09-29 BR BRPI0616662-8A patent/BRPI0616662B1/pt not_active IP Right Cessation
- 2006-09-29 AU AU2006301367A patent/AU2006301367B2/en not_active Ceased
- 2006-09-29 ES ES06793910T patent/ES2327569T3/es active Active
- 2006-09-29 US US12/089,831 patent/US8785570B2/en active Active
- 2006-09-29 DE DE602006008337T patent/DE602006008337D1/de active Active
- 2006-09-29 RU RU2008118478/04A patent/RU2415877C2/ru active
- 2006-09-29 CN CN2006800377177A patent/CN101283012B/zh not_active Expired - Fee Related
- 2006-09-29 AT AT06793910T patent/ATE438669T1/de not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| EP1940899A1 (en) | 2008-07-09 |
| WO2007042411A1 (en) | 2007-04-19 |
| CN101283012B (zh) | 2011-07-06 |
| RU2415877C2 (ru) | 2011-04-10 |
| ATE438669T1 (de) | 2009-08-15 |
| CN101283012A (zh) | 2008-10-08 |
| AU2006301367B2 (en) | 2012-02-02 |
| CA2625689A1 (en) | 2007-04-19 |
| US20080262168A1 (en) | 2008-10-23 |
| ES2327569T3 (es) | 2009-10-30 |
| JP2009511685A (ja) | 2009-03-19 |
| US8785570B2 (en) | 2014-07-22 |
| AU2006301367A1 (en) | 2007-04-19 |
| BRPI0616662B1 (pt) | 2017-06-13 |
| DE602006008337D1 (de) | 2009-09-17 |
| EP1940899B1 (en) | 2009-08-05 |
| JP5044561B2 (ja) | 2012-10-10 |
| KR20080057271A (ko) | 2008-06-24 |
| CA2625689C (en) | 2013-07-09 |
| BRPI0616662A2 (pt) | 2012-12-25 |
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