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RU2007112912A - Композиция катализатора гидрокрекинга - Google Patents

Композиция катализатора гидрокрекинга Download PDF

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Publication number
RU2007112912A
RU2007112912A RU2007112912/04A RU2007112912A RU2007112912A RU 2007112912 A RU2007112912 A RU 2007112912A RU 2007112912/04 A RU2007112912/04 A RU 2007112912/04A RU 2007112912 A RU2007112912 A RU 2007112912A RU 2007112912 A RU2007112912 A RU 2007112912A
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Russia
Prior art keywords
catalyst composition
compounds
metals
composition according
zeolite
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RU2007112912/04A
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English (en)
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RU2387480C2 (ru
Inventor
Виллем Хартман Юрриан СТОРК (NL)
Виллем Хартман Юрриан СТОРК
Ласло ДОМОКОС (NL)
Ласло ДОМОКОС
Херманус ЙОНГКИНД (NL)
Херманус ЙОНГКИНД
Марчелло Стефано РИГУТТО (NL)
Марчелло Стефано РИГУТТО
ДЕН ВОРТ Эстер Хиллегарда Карола ВАН (NL)
ДЕН ВОРТ Эстер Хиллегарда Карола ВАН
Original Assignee
Шелл Интернэшнл Рисерч Маатсхаппий Б.В. (NL)
Шелл Интернэшнл Рисерч Маатсхаппий Б.В.
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Publication of RU2007112912A publication Critical patent/RU2007112912A/ru
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/08—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y
    • B01J29/16—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/02—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils characterised by the catalyst used
    • C10G11/06—Sulfides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/076—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/08—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y
    • B01J29/16—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J29/166—Y-type faujasite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/02—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/06—Sulfides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/16—Crystalline alumino-silicate carriers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Claims (15)

1. Композиция катализатора без носителя, которая включает в себя один или несколько металлов группы VIb, один или несколько неблагородных металлов группы VIII, один или несколько цеолитов и, необязательно, тугоплавкий оксидный материал.
2. Композиция катализатора по п.1, в которой цеолит представляет собой ультрастабильный или весьма ультрастабильный цеолит Y, который присутствует в количестве от 1 до 85 мас.%, предпочтительно от 15 до 75 мас.%, в расчете на всю композицию.
3. Композиция катализатора по п.1, в которой тугоплавкий оксид представляет собой диоксид кремния, который присутствует в количестве от 0 до 40 мас.%, предпочтительно от 0 до 15 мас.%, в расчете на всю композицию.
4. Композиция катализатора по п.1, в которой тугоплавкий оксид представляет собой диоксид титана, который присутствует в количестве от 0 до 40 мас.%, предпочтительно от 0 до 15 мас.%, в расчете на всю композицию.
5. Композиция катализатора по любому из пп.1-4, в которой присутствующие металлы представляют собой никель и молибден в молярном соотношении никеля к молибдену от 0,5:1 до 2,5:1.
6. Композиция катализатора по п.5, в которой количество молибдена, расположенного в порах цеолита, находится в диапазоне от 4, предпочтительно от 5 до 25 мас.%, в расчете на оксидную форму композиции.
7. Способ получения композиции катализатора по любому из пп.1-6, в котором одно или несколько соединений металлов группы VIb объединяют с одним или несколькими соединениями неблагородных металлов группы VIII, и с цеолитом, в присутствии протоносодержащей жидкости и необязательно щелочного соединения, и после осаждения извлекают композицию катализатора.
8. Способ по п.7, в котором в ходе осаждения смесь компонентов имеет значение рН, по меньшей мере, 6,0.
9. Способ по п.7, в котором, по меньшей мере, одно из соединений металла частично находится в твердом состоянии и частично в растворенном состоянии.
10. Способ по п.9, который включает в себя нагревание предшественника композиции, который находится в виде суспензии, или извлечен из суспензии необязательно после старения при температуре в диапазоне от 20 до 95°С, минимум в течение 10 мин, причем указанную суспензию получают путем (со)осаждения, при соответствующей температуре и в течение достаточного времени, одного или нескольких соединений металлов группы VIb, одного или нескольких соединений неблагородных металлов группы VIII, одного или нескольких цеолитов, необязательно одного или нескольких тугоплавких оксидных материалов и щелочного соединения, в протоносодержащей жидкости.
11. Способ по любому из пп.7-10, в котором композицию катализатора выделяют с помощью распылительной сушки.
12. Композиция катализатора, полученная способом по п.7.
13. Способ превращения углеводородного сырья в материалы с меньшей температурой кипения, который включает в себя контактирование сырья при повышенной температуре в присутствии композиции катализатора по любому из пп.1-6, 12, или композиции катализатора, полученной способом по любому из пп.7-11.
14. Применение композиции катализатора по любому из пп.1-6 и 12 в способе гидрокрекинга.
15. Способ по п.13, или применение по п.14, в котором композицию катализатора подвергают сульфидированию, используя реагент сульфидирования в жидкой фазе.
RU2007112912/04A 2004-09-08 2005-09-06 Композиция катализатора гидрокрекинга RU2387480C2 (ru)

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EP04255442.8 2004-09-08
EP04255442 2004-09-08

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US (1) US7648939B2 (ru)
EP (1) EP1794264B1 (ru)
JP (1) JP2008512223A (ru)
KR (1) KR20070104517A (ru)
CN (1) CN101035881B (ru)
BR (1) BRPI0514960A (ru)
CA (1) CA2579445A1 (ru)
DK (1) DK1794264T3 (ru)
RU (1) RU2387480C2 (ru)
UA (1) UA92156C2 (ru)
WO (1) WO2006027359A1 (ru)
ZA (1) ZA200701613B (ru)

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US7648939B2 (en) 2010-01-19
UA92156C2 (ru) 2010-10-11
EP1794264A1 (en) 2007-06-13
JP2008512223A (ja) 2008-04-24
EP1794264B1 (en) 2020-05-27
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BRPI0514960A (pt) 2008-07-01
WO2006027359A1 (en) 2006-03-16
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