RS58401B1 - Sastav fungicida koji sadrži derivat tetrazoliloksima i derivat tiazolilpiperidina - Google Patents
Sastav fungicida koji sadrži derivat tetrazoliloksima i derivat tiazolilpiperidinaInfo
- Publication number
- RS58401B1 RS58401B1 RS20190239A RSP20190239A RS58401B1 RS 58401 B1 RS58401 B1 RS 58401B1 RS 20190239 A RS20190239 A RS 20190239A RS P20190239 A RSP20190239 A RS P20190239A RS 58401 B1 RS58401 B1 RS 58401B1
- Authority
- RS
- Serbia
- Prior art keywords
- procedure according
- copper
- hydroxide
- requirements
- indicated
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/18—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with sulfur as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/713—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with four or more nitrogen atoms as the only ring hetero atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/18—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, directly attached to a heterocyclic or cycloaliphatic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N2300/00—Combinations or mixtures of active ingredients covered by classes A01N27/00 - A01N65/48 with other active or formulation relevant ingredients, e.g. specific carrier materials or surfactants, covered by classes A01N25/00 - A01N65/48
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- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pretreatment Of Seeds And Plants (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
Description
POSTUPAK ZA DOBIJANJE FUNGICIDNO AKTIVNOG BAKAR
HIDROKSIDA
OBLAST TEHNIKE NA KOJU SE PRONALAZAK ODNOSI
Pronalazak pripada oblasti hernije, poljoprivrede, odnosno oblasti zaštite bilja u poljoprivredi i šumarstvu.
Prema međunarodnoj klasifikaciji patenta (MKP) predmet pronalaska je razvrstan, odnosno klasiran i označen simbolima: A 01 N 59/20, C 01 G 3/02
TEHNIČKI PROBLEM
Tehnički problem koji se rešava predmetnim pronalaskom sastoji se
u tome kako proizvesti na efikasan način fungicidno aktivan bakar hidroksid i način da se nus proizvodi koji nastaju mogu da prevedu u proizvode, čime bi se dobio znatno bolji i kvalitetniji postupak i omogućilo smanjenje ispuštanja nus produkata u otpadne vode.
STANJE TEHNIKE
Za sada je poznato da se problem proizvodnje bakar hidroksida opšte formule Cu(OH)2-xH20, dobija jednim od sledećih postupaka:
1. tretiranjem rastvora soli bakra hidroksilnim jonima, taloženjem pomoću rastvora natrijum ili kalijum hidroksida, ili pomoću amonijaka:
2. Elektrolizom u alkalnim rastvorima.
Najvažniji od ovih postupaka jeste taloženje soli bakra bazama koje se nalaze u obliku rastvora u velikim razblaženjima, pri čemu se dobija bakarni hidroksid u obliku gela i razblaženi rastvori alkainih soli. Bakar hidroksid dobijen na ovaj način ima oblik gela koji uvek zadržava jone sredstava za taloženje i treba ga ispirati velikom količinom vode što dalje povećava količine rastvarane alkalne soli. Rastvori alkainih soli natrijum, kalijum, amonijum sulfata nisu pogodni za dalju preradu zbog male koncentracije i najčešće se javljaju kao otpadne vode iz ovih proizvodnji. Bakar hidroksid koji se dobija postupcima koji se danas primenjuju u početku je svetio plav, ali polako u vodi ili na vazduhu menja boju u crnu, čak i na običnim temperaturama.
Prelaz je utoliko brži ukoliko je temperatura viša. Ove promene potiču od pretvaranja bakar hidroksida u bakar oksid.
Takođe je poznato da se stabilni bakar hidroksid stvara ako se sveže staloženi bakar hidroksid dobro opere, a zatim tretira alkalijama.
Čist bakar hidroksid bez alkalija nije stabilan.
Bakar hidroksid dobijen postupcima koji su poznati od ranije usled svoje nestabilnosti na poznati način transformiše u crni bakarni oksid usled čega dolazi do potpunog gubitka fungicidnog dejstva. Bakar hidroksid dobijen i stabilisan dodatkom alkalija ima nedostatak da oštećuje biljke koje se njime prskaju. Ove mane i nestabilnost ograničavaju uspešnu primenu na polju fitopatologije. Sušenje bakar hidroksida u cilju dobijanja praškastih proizvoda vezano je za značajan utrošak energije, a prate ga poznate promene koje se događaju na povišenim temperaturama, odnosno pretvaranje u crni oksid.
IZLAGANJE SUŠTINE PRONALASKA
Ovaj pronalazak se odnosi na postupak za dobijanje fungicidno aktivnog bakar hidroksida.Postupak se sastoji u tome da se obavlja u dve faze: U prvoj fazi se taloži jedna bazna so koja se odvoji od alkalne soli, a u sledećoj fazi prevodi u hidroksid.
Postupak je da se pomešaju rastvori kupri soli i hidroksidi ili karbonati natrijuma, kalijuma ili amonijaka usled čega dolazi do taloženja stabilne bazne bakarne soli, u zavisnosti od polazne soli sulfata, hlorida, nitrata ili dr.
n = 2 + 3, tako da je molski odnos 4:3 do 4:2.
Reakcija se izvodi u količini vode koja omogućuje da se dobije koncentrovani rastvor alkalne soli koja se filtracijom ili taloženjem odvoji od bazne soli i koristi se za dobijanje kristalne alkalne soli natrijum sulfata, kalijum sulfata ili amonijum sulfata koji su komercijalni proizvodi. Nastala bazna so odvojena kao filtraciona pogača, ili kao talog sedimentacije se suspenduje u vodi uz dodatak nekog od viševalentnih alkohola kao što su: etilenglikol, propilenglikol, glicerin, ili si.
U tako dobijenu suspenziju dodaje se koncentrovani rastvor alkalije na primer kalijum hidroksid i bakar prevodi u bakarni hidroksid:
Hidroksid se dodaje u višku tako da je na kraju taloženja
pH = 11-12,7.
Suspenzija bakar hidroksida dobija intenzivno plavu boju i kada se proverom utvrdi da je pH suspenzije stabilan, odnosno da se ne menja vrši se neutralizacija viška alkalija. Višak alkalija se neutrališe: sirćetnom kiselinom, fosfornom kiselinom, lignosulfonskom kiselinom, salicilnom kiselinom, ili si. Da se postigne pH < 8.Dobijeni bakar hidroksid u suspenziji je stabilan, pokazuje dobre fungicidne osobine i ne pokazuje u primeni fitotoksične efekte.
KRATAK OPIS
U cilju lakšeg razumevanja pronalaska, kao i zbog prikazivanja kako se on može ostvariii u praksi, autor se poziva na: 1. Neutralizacija bakarne soli: CuS04, CuCC>2, Cu(NC>3)2 i dobijanje bazne soli: (3) 2. Prevođenje bazne soli u hidroksid bakra alkalijama kao što su: KOH, NaOH, ili njihovim mešavinama. (4) 3. Neutralizacija viška alkalija sa kiselinama kao što su: sirćetna kiselina (CH3—COOH), fosforna (H3P04), lignosulfonska, salicilna ili slično.
DETALJAN OPIS PRONALASKA
Pripremi se rastvor gram mola CuS04-5H20 u 500 ml vode. Ovome se doda u malim delovima 1/2 do 1/3 gram mola, odnosno 75 gr natrijum karbonata (Na2C03) za vreme taloženja koje usled ovoga nastaje. Potrebno je dobro mešanje da bi se izbeglo stvaranje grudvi i jako alkainih zona. Dobro umešana suspenzija nastale bazne soli pokazuje pH 7+8; talog se ocedi i dobijeni rastvor natrijum sulfata Na2S04nekom od poznatih metoda kristališe u kristalni proizvod. Talog se suspenduje dodatkom vode u koju se doda mešavina 10 gr propilenglikola i 2 gr glicerina tako da se dobije 200 ml suspenzije bazne soli.
U suspenziju bazne soli doda se 1/2 gram mola kalijum hidroksida KOH rastvorena u 50 ml vode i 2 gr glicerina uz dobro mešanje, pri čemu nastaje stabilan bakar hidroksid, a pH ovako nastale suspenzije je 11+12,7.
Neutralizacija viška alkalija vrši se dodatkom 1/20 gram mola fosforne kiseline u kapima uz intenzivno mešanje dok se proverom ne utvrdi da je pH < 8. Dobijena suspenzija bakar hidroksida se meša sa dodacima za bolje kvašenje - etoksilovani alkilfenilfosfat 5 gr; stabilnost suspenzije - kondenzovani alkilnaftalinsulfonat 5 gr, natriumlignosulfonat 5 gr i bentonitska glina 5 gr; korekciju viskoziteta - xantan guma 0,25 gr i antipenušavcem - silikonsko ulje 1 gr, melje, pri čemu veličina čestice mora biti da na situ od 44 p.m masa ostatka ne srne biti veća od 1% i na taj način dobije preparat koji sadrži:
Dobijeni preparat ima viskozitet > 100 mPa-s i stabilan je tokom skladištenja.
Preparat se koristi za suzbijanje prouzrokovača u:
1. zasadu jabuke i kruške, pegavosti lista i krastavosti plodovaVenturia inequalisiVenturia purina 2.zasadima breskve, kasije, višnje, trešnje i badema, šupljikavosti lišća,Stigmina carpophilia,sušenje grančica
Monilinia laxa
3. zasadima vinove loze, plamenjačePlasmopara viticola
4. zasadima hmelja,Pseudoperonospora hum uli
5. usevu krastavaca, plamenjačaPseudoperonospora cubensis.
Ako se želi može se dobiti praškasti proizvod sušenjem nekim od poznatih postupaka.
Claims (7)
1. Postupak za dobijanje fungicidnog bakar hidroksida,naznačen time,što se reakcija između rastvora jedne soli bakra i jedne alkalije natrijum hidroksida i/ili kalijum hidroksida, ili karbonata u molarnoj srazmeri 4:3 do 4:2, pri čemu se dobija talog stabilne bazne soli bakra pri pH 7+8 posle čega se talog izdvaja i neutrališe viškom alkalija kalijum hidroksida i/ili natrijum hidroksida pri čemu nastaje nerastvorni hidroksid bakra.
2. Postupak prema zahtevu jenaznačen timešto pH vrednost na kraju reakcije može biti 11+12,7.
3. Postupak prema zahtevima 1 i 2 jenaznačen timešto se alkalni rastvor dodaje u malim količinama uz intenzivno mešanje. u količini od 1/2 gram mola po gram molu bakar sulfata.
4. Postupak prema zahtevima od 1 do 3naznačen timešto se u suspenziju bazne soli dodaje etilenglikol i/ili propilenglikol i/ili glicerin u količini 50+60 gr/l.
5. Postupak prema ma kom od zahteva od 1 do 6,naznačen timešto se višak alkalija neutrališe sirćetnom i/lii fosfornom i/ili lignosulfonskom i/ili salicilnom kiselinom dok pH ne dostigne vrednost < 8.
6. Postupak prema ma kom od zahteva od 1 do 7 što se dobijena suspenzija melje, pri čemu veličina čestice mora biti da na situ od 44 (im masa ostatka ne srne biti veća od 1% i koristi kao sredstvo za zaštitu jabuke, kruške, breskve, kajsije, višnje, trešnje, badema, vinove loze, hmelja i krastavaca od bolesti.
7. Postupak prema ma kom od zahteva od 1 do 8 što se dobijena suspenzija suši i time dobija praškasti proizvod namenjen za korišćenje u poljoprivredi i šumarstvu.
NAČIN INDUSTRIJSKEIDRUGE PRIMENE PRONALASKANačin primene pronalaska proističe na očigledan način iz prethodnog teksta, te ga nije potrebno posebno opisivati. Sve karakteriatike pronalaska pronalazač je proverio u opitnoj proizvodnji i praktičnoj proveri u zaštiti bilja.
Svakako da se, zadržavajući isti princip pronalaska, detalji i oblici izvodjenja mogu menjati u širokim granicama u odnosu na opisane i prikazane, a da se ne odstupi od opsega prikazanog pronalaska.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10356026 | 2010-10-07 | ||
| US41461710P | 2010-11-17 | 2010-11-17 | |
| EP11769834.0A EP2624699B1 (en) | 2010-10-07 | 2011-10-06 | Fungicide composition comprising a tetrazolyloxime derivative and a thiazolylpiperidine derivative |
| PCT/EP2011/067424 WO2012045798A1 (en) | 2010-10-07 | 2011-10-06 | Fungicide composition comprising a tetrazolyloxime derivative and a thiazolylpiperidine derivative |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RS58401B1 true RS58401B1 (sr) | 2019-04-30 |
Family
ID=43608026
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RS20190239A RS58401B1 (sr) | 2010-10-07 | 2011-10-06 | Sastav fungicida koji sadrži derivat tetrazoliloksima i derivat tiazolilpiperidina |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US9408391B2 (sr) |
| EP (1) | EP2624699B1 (sr) |
| JP (2) | JP5977242B2 (sr) |
| KR (1) | KR101871525B1 (sr) |
| CN (1) | CN103338638B (sr) |
| BR (1) | BR112013008446B1 (sr) |
| CO (1) | CO6700870A2 (sr) |
| MX (1) | MX346667B (sr) |
| PE (1) | PE20131399A1 (sr) |
| PL (1) | PL2624699T3 (sr) |
| RS (1) | RS58401B1 (sr) |
| WO (1) | WO2012045798A1 (sr) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012045798A1 (en) * | 2010-10-07 | 2012-04-12 | Bayer Cropscience Ag | Fungicide composition comprising a tetrazolyloxime derivative and a thiazolylpiperidine derivative |
| EP2630135B1 (en) * | 2010-10-21 | 2020-03-04 | Bayer Intellectual Property GmbH | 1-(heterocyclic carbonyl) piperidines |
| EP2965628B1 (en) * | 2013-03-05 | 2019-06-26 | Nippon Soda Co., Ltd. | Method for controlling rhizopus genus fungus in rice |
| EP2865267A1 (en) | 2014-02-13 | 2015-04-29 | Bayer CropScience AG | Active compound combinations comprising phenylamidine compounds and biological control agents |
| EP2865265A1 (en) | 2014-02-13 | 2015-04-29 | Bayer CropScience AG | Active compound combinations comprising phenylamidine compounds and biological control agents |
| WO2016024350A1 (ja) | 2014-08-13 | 2016-02-18 | 株式会社エス・ディー・エス バイオテック | 縮合１１員環化合物及びそれらを含有する農園芸用殺菌剤 |
| JP6290064B2 (ja) * | 2014-10-20 | 2018-03-07 | 日本曹達株式会社 | 農園芸用殺菌剤 |
| KR102605762B1 (ko) | 2016-02-08 | 2023-11-27 | 고완 크롭 프로텍션 리미티드 | 살균성 조성물 |
| CN108602765B (zh) | 2016-02-08 | 2022-05-03 | 高文有限公司 | 1,2-苯二甲醇化合物的制造方法 |
| BR122022025232B1 (pt) | 2016-10-10 | 2023-10-31 | Basf Se | Mistura pesticida, composição pesticida, métodos para controlar pragas fitopatogênicas, para melhorar a saúde de plantas e para a proteção do material de propagação vegetal contra pragas e material de propagação vegetal |
| US20190307127A1 (en) | 2016-10-10 | 2019-10-10 | Basf Se | Pesticidal Mixtures |
| CN106689161A (zh) * | 2016-12-20 | 2017-05-24 | 东莞市瑞德丰生物科技有限公司 | 含有picarbutrazox的杀菌组合物 |
| KR20210131350A (ko) | 2019-02-20 | 2021-11-02 | 바스프 에스이 | 피라졸 화합물을 포함하는 살충 혼합물 |
| WO2025238213A1 (en) | 2024-05-17 | 2025-11-20 | Syngenta Crop Protection Ag | Method for treatment of root rot disease caused by plant pathogens in legume crops |
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-
2011
- 2011-10-06 WO PCT/EP2011/067424 patent/WO2012045798A1/en not_active Ceased
- 2011-10-06 RS RS20190239A patent/RS58401B1/sr unknown
- 2011-10-06 MX MX2013003750A patent/MX346667B/es active IP Right Grant
- 2011-10-06 PL PL11769834T patent/PL2624699T3/pl unknown
- 2011-10-06 KR KR1020137011757A patent/KR101871525B1/ko active Active
- 2011-10-06 US US13/877,737 patent/US9408391B2/en active Active
- 2011-10-06 EP EP11769834.0A patent/EP2624699B1/en active Active
- 2011-10-06 CN CN201180048152.3A patent/CN103338638B/zh active Active
- 2011-10-06 JP JP2013532189A patent/JP5977242B2/ja active Active
- 2011-10-06 BR BR112013008446-4A patent/BR112013008446B1/pt active IP Right Grant
- 2011-10-06 PE PE2013000798A patent/PE20131399A1/es active IP Right Grant
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2013
- 2013-05-03 CO CO13111895A patent/CO6700870A2/es unknown
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2016
- 2016-05-25 JP JP2016104015A patent/JP6342447B2/ja active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2624699A1 (en) | 2013-08-14 |
| US20130190353A1 (en) | 2013-07-25 |
| JP2016188221A (ja) | 2016-11-04 |
| JP2013542934A (ja) | 2013-11-28 |
| US9408391B2 (en) | 2016-08-09 |
| BR112013008446A2 (pt) | 2016-06-28 |
| CN103338638B (zh) | 2016-04-06 |
| JP6342447B2 (ja) | 2018-06-13 |
| MX346667B (es) | 2017-03-28 |
| JP5977242B2 (ja) | 2016-08-24 |
| BR112013008446B1 (pt) | 2018-06-12 |
| PL2624699T3 (pl) | 2019-05-31 |
| WO2012045798A1 (en) | 2012-04-12 |
| CN103338638A (zh) | 2013-10-02 |
| PE20131399A1 (es) | 2013-12-16 |
| KR101871525B1 (ko) | 2018-06-26 |
| EP2624699B1 (en) | 2018-11-21 |
| CO6700870A2 (es) | 2013-06-28 |
| KR20130117788A (ko) | 2013-10-28 |
| MX2013003750A (es) | 2013-05-20 |
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