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PE20142016A1 - Proceso en lecho movil simulado (smb) - Google Patents

Proceso en lecho movil simulado (smb)

Info

Publication number
PE20142016A1
PE20142016A1 PE2014000008A PE2014000008A PE20142016A1 PE 20142016 A1 PE20142016 A1 PE 20142016A1 PE 2014000008 A PE2014000008 A PE 2014000008A PE 2014000008 A PE2014000008 A PE 2014000008A PE 20142016 A1 PE20142016 A1 PE 20142016A1
Authority
PE
Peru
Prior art keywords
zone
pufa
column
product
collected
Prior art date
Application number
PE2014000008A
Other languages
English (en)
Inventor
Adam Kelliher
Angus Morrison
Anil Oroskar
Rema Rakesh Vikraman Nair
Abhilesh Agarwal
Original Assignee
Basf Pharma Callanish Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Pharma Callanish Ltd filed Critical Basf Pharma Callanish Ltd
Publication of PE20142016A1 publication Critical patent/PE20142016A1/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/185—Simulated moving beds characterised by the components to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1892—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns the sorbent material moving as a whole, e.g. continuous annular chromatography, true moving beds or centrifugal chromatography
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/10—Refining fats or fatty oils by adsorption
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • C11B7/0033—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents in solvents containing other heteroatoms in their molecule
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/005—Splitting up mixtures of fatty acids into their constituents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/007—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids using organic solvents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Sustainable Development (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)

Abstract

REFERIDA A UN PROCESO DE SEPARACION CROMATOGRAFICO, CON EL FIN DE RECUPERAR UN PRODUCTO DEL ACIDO POLIINSATURADO (PUFA) A PARTIR DE UNA MEZCLA DE ALIMENTACION, EL CUAL COMPRENDE LA INTRODUCCION DE LA MEZCLA DE ALIMENTACION A UN APARATO DE CROMATOGRAFIA EN LECHO MOVIL REAL O SIMULADO, QUE TIENE UNA PLURALIDAD DE COLUMNAS DE CROMATOGRAFIA ENLAZADAS CONTENIENDO, COMO ELUYENTE, UN SOLVENTE ORGANICO ACUOSO, DONDE EL APARATO TIENE UNA PLURALIDAD DE ZONAS COMPRENDIENDO UNA PRIMERA Y SEGUNDA ZONA, TENIENDO CADA ZONA UNA CORRIENTE DEL EXTRACTO Y UNA CORRIENTE DEL REFINADO, A PARTIR DE LA CUAL PUEDE SER RECOLECTADO LIQUIDO DESDE DICHA PLURALIDAD DE COLUMNAS DE CROMATOGRAFIA ENLAZADAS, DONDE a) UNA CORRIENTE DEL REFINADO CONTENIENDO EL RPODUCTO PUFA JUNTO CON LOS COMPONENTES MAS POLARES SE RECOLECTA DESDE UNA COLUMNA EN LA PRIMERA ZONA E INTRODUCIDA A UNA COLUMNA NO ADYACENTE EN LA SEGUNDA ZONA Y/O b) UNA CORRIENTE DEL EXTRACTO CONTENIENDO EL PRODUCTO PUFA JUNTO CON LOS COMPONENTES MENOS POLARES SE RECOLECTA DESDE UNA COLUMNA EN LA SEGUNDA ZONA E INTRODUCIDA A UNA COLUMNA NO ADYACENTE EN LA PRIMERA ZONA, SIENDO DICHO PRODUCTO PUFA SEPARADO DESDE DIFERENTES COMPONENTES DE LA MEZCLA DE ALIMENTACION EN CADA ZONA Y DONDE EL SOLVENTE ORGANICO ACUOSO ES DISTINTO AL ALCOHOL ACUOSO. EL PRODUCTO PUFA COMPRENDE UN PUFA OMEGA-3 TALES COMO EL ACIDO EICOSAPENTAENOICO (EPA) Y EL ACIDO DOCOSAHEXAENOICO (DHA)
PE2014000008A 2011-07-06 2012-07-06 Proceso en lecho movil simulado (smb) PE20142016A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB1111601.9A GB201111601D0 (en) 2011-07-06 2011-07-06 New process

Publications (1)

Publication Number Publication Date
PE20142016A1 true PE20142016A1 (es) 2014-12-30

Family

ID=44544346

Family Applications (1)

Application Number Title Priority Date Filing Date
PE2014000008A PE20142016A1 (es) 2011-07-06 2012-07-06 Proceso en lecho movil simulado (smb)

Country Status (13)

Country Link
US (1) US9370730B2 (es)
EP (1) EP2613858B1 (es)
JP (2) JP6153519B2 (es)
KR (1) KR101594722B1 (es)
CN (1) CN103764242B (es)
AU (1) AU2012280065B2 (es)
BR (1) BR112014000163A2 (es)
CA (1) CA2815296C (es)
CL (1) CL2013003796A1 (es)
ES (1) ES2536911T3 (es)
GB (1) GB201111601D0 (es)
PE (1) PE20142016A1 (es)
WO (1) WO2013005046A1 (es)

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RU2014146265A (ru) 2009-12-30 2015-07-10 Басф Фарма (Калланиш) Лимитед Способ хроматографического разделения с псевдодвижущимся слоем
GB201111591D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Further new process
GB201111601D0 (en) * 2011-07-06 2011-08-24 Equateq Ltd New process
GB201111594D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New improved process
GB201111589D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New modified process
GB201111595D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Improved process
GB201300354D0 (en) * 2013-01-09 2013-02-20 Basf Pharma Callanish Ltd Multi-step separation process
JP6546911B2 (ja) * 2013-05-07 2019-07-17 グループ ノヴァセップＧｒｏｕｐｅ Ｎｏｖａｓｅｐ 高度に精製したポリ不飽和脂肪酸を生成するクロマトグラフプロセス
US8802880B1 (en) 2013-05-07 2014-08-12 Group Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
US9428711B2 (en) 2013-05-07 2016-08-30 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
EP3118186B1 (fr) 2013-12-11 2022-02-09 Novasep Process Installation chromatographique de production d acides gras polyinsatures
JP6303017B2 (ja) 2014-01-07 2018-03-28 ノヴァセプ プロセスＮｏｖａｓｅｐ Ｐｒｏｃｅｓｓ 芳香族アミノ酸を精製する方法
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EP3586640A1 (en) 2018-06-21 2020-01-01 Nuseed Pty Ltd Dha enriched polyunsaturated fatty acid compositions
EP3586642A1 (en) 2018-06-21 2020-01-01 Nuseed Pty Ltd Ala enriched polyunsaturated fatty acid compositions
CN113015578B (zh) 2018-09-18 2023-11-21 英威达纺织（英国）有限公司 用于从水性混合物中回收胺及其衍生物的系统和方法
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CN112169373B (zh) * 2019-07-05 2022-03-11 中国石油化工股份有限公司 一种模拟移动床吸附分离目标产物的方法
CN113831244A (zh) * 2020-06-24 2021-12-24 北京创新通恒科技有限公司 一种提纯高纯EPA-ee分离设备及工艺方法
CA3238072A1 (en) 2021-12-17 2023-06-22 Basf Se Chromatographic separation process for efficient purification of polyunsaturated fatty acids
CN115073292B (zh) * 2022-07-01 2023-10-03 江苏汉邦科技股份有限公司 一种二十碳五烯酸乙酯的制备方法

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CA2815296C (en) 2015-02-10
JP6153519B2 (ja) 2017-06-28
EP2613858B1 (en) 2015-03-18
GB201111601D0 (en) 2011-08-24
CA2815296A1 (en) 2013-01-10
KR20140034920A (ko) 2014-03-20
CN103764242B (zh) 2015-07-15
US20140194636A1 (en) 2014-07-10
EP2613858A1 (en) 2013-07-17
ES2536911T3 (es) 2015-05-29
BR112014000163A2 (pt) 2017-02-07
CN103764242A (zh) 2014-04-30
AU2012280065A1 (en) 2013-05-09
WO2013005046A1 (en) 2013-01-10
JP2017020031A (ja) 2017-01-26
AU2012280065B2 (en) 2015-07-09
CL2013003796A1 (es) 2014-07-04
KR101594722B1 (ko) 2016-02-16
JP2014518312A (ja) 2014-07-28

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