PE20142014A1 - Proceso nuevo en smb - Google Patents
Proceso nuevo en smbInfo
- Publication number
- PE20142014A1 PE20142014A1 PE2014000007A PE2014000007A PE20142014A1 PE 20142014 A1 PE20142014 A1 PE 20142014A1 PE 2014000007 A PE2014000007 A PE 2014000007A PE 2014000007 A PE2014000007 A PE 2014000007A PE 20142014 A1 PE20142014 A1 PE 20142014A1
- Authority
- PE
- Peru
- Prior art keywords
- product
- pufa
- separation step
- chromatography
- separation
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- 239000000047 product Substances 0.000 abstract 6
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 abstract 5
- 238000004587 chromatography analysis Methods 0.000 abstract 4
- 239000000203 mixture Substances 0.000 abstract 4
- 238000000926 separation method Methods 0.000 abstract 4
- 235000013305 food Nutrition 0.000 abstract 3
- JAZBEHYOTPTENJ-JLNKQSITSA-N all-cis-5,8,11,14,17-icosapentaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O JAZBEHYOTPTENJ-JLNKQSITSA-N 0.000 abstract 2
- 235000020673 eicosapentaenoic acid Nutrition 0.000 abstract 2
- 229960005135 eicosapentaenoic acid Drugs 0.000 abstract 2
- JAZBEHYOTPTENJ-UHFFFAOYSA-N eicosapentaenoic acid Natural products CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O JAZBEHYOTPTENJ-UHFFFAOYSA-N 0.000 abstract 2
- VJYFKVYYMZPMAB-UHFFFAOYSA-N ethoprophos Chemical compound CCCSP(=O)(OCC)SCCC VJYFKVYYMZPMAB-UHFFFAOYSA-N 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 238000000746 purification Methods 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- DVSZKTAMJJTWFG-SKCDLICFSA-N (2e,4e,6e,8e,10e,12e)-docosa-2,4,6,8,10,12-hexaenoic acid Chemical compound CCCCCCCCC\C=C\C=C\C=C\C=C\C=C\C=C\C(O)=O DVSZKTAMJJTWFG-SKCDLICFSA-N 0.000 abstract 1
- GZJLLYHBALOKEX-UHFFFAOYSA-N 6-Ketone, O18-Me-Ussuriedine Natural products CC=CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O GZJLLYHBALOKEX-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 238000013375 chromatographic separation Methods 0.000 abstract 1
- 235000020669 docosahexaenoic acid Nutrition 0.000 abstract 1
- KAUVQQXNCKESLC-UHFFFAOYSA-N docosahexaenoic acid (DHA) Natural products COC(=O)C(C)NOCC1=CC=CC=C1 KAUVQQXNCKESLC-UHFFFAOYSA-N 0.000 abstract 1
- 239000013067 intermediate product Substances 0.000 abstract 1
- 235000013336 milk Nutrition 0.000 abstract 1
- 239000008267 milk Substances 0.000 abstract 1
- 210000004080 milk Anatomy 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
- B01D15/185—Simulated moving beds characterised by the components to be separated
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1892—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns the sorbent material moving as a whole, e.g. continuous annular chromatography, true moving beds or centrifugal chromatography
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
- C11B7/0025—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents in solvents containing oxygen in their molecule
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
- C11C1/005—Splitting up mixtures of fatty acids into their constituents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
- C11C1/007—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids using organic solvents
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Sustainable Development (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
REFERIDA A UN PROCESO DE SEPARACION CROMATOGRAFICA PARA LA RECUPERACION DE UN PRODUCTO DEL ACIDO POLIINSATURADO (PUFA) A PARTIR DE UNA MEZCLA DE ALIMENTACION, EL CUAL COMPRENDE i) LA PURIFICACION DE LA MEZCLA DE ALIMENTACION EN UN PRIMER PASO DE SEPARACION EN UN APARATO DE CROMATOGRAFIA EN LECHO MOVIL, REAL O SIMULADO, TENIENDO UNA PLURALIDAD DE COLUMNAS CROMATOGRAFICAS ENLAZADAS CONTENIENDO COMO ELUYENTE, UN SOLVENTE ORGANICO ACUOSO, CON EL FIN DE OBTENER UN PRODUCTO INTERMEDIARIO Y ii) LA PURIFICACION DEL PRODUCTO INTERMEDIARIO OBTENIDO EN i) EN UN SEGUNDO PASO DE SEPARACION, USANDO UN APARATO DE CROMATOGRAFIA EN LECHO MOVIL, REAL O SIMULADO, TENIENDO UNA PLURALIDAD DE COLUMNAS DE CROMATOGRAFIA ENLAZADAS CONTENIENDO, COMO ELUYENTE, UN SOLVENTE ORGANICO ACUOSO, CON EL FIN DE OBTENER UN PRODUCTO DEL PUFA, DONDE a) EL PRIMER Y SEGUNDO PASO DE SEPARACION SE REALIZAN EN FORMA SECUENCIAL EN EL MISMO APARATO DE CROMATOGRAFIA, DE MANERA QUE EL PRODUCTO DEL PUFA ES SEPARADO DE LOS DIFERENTES COMPONENTES DE LA MEZCLA DE ALIMENTACION O b) EL PRIMER Y SEGUNDO PASO DE SEPARACION SE REALIZAN EN APARATOS DE CROMATOGRAFIA SEPARADOS, SIENDO EL PRODUCTO INTERMEDIARIO OBTENIDO A PARTIR DEL PRIMER PASO DE SEPARACION INTRODUCIDO DENTRO DEL SEGUNDO APARATO DE CROMATOGRAFIA Y SIENDO EL PRODUCTO DEL PUFA SEPARADO DE LOS DIFERENTES COMPONENTES DE LA MEZCLA DE ALIMENTACION. EL PRODUCTO DEL PUFA COMPRENDE UN PUFA OMEGA-3 TALES COMO EL ACIDO EICOSAPENTAENOICO (EPA) Y EL ACIDO DOCOSAHEXAENOICO (DHA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GBGB1111589.6A GB201111589D0 (en) | 2011-07-06 | 2011-07-06 | New modified process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PE20142014A1 true PE20142014A1 (es) | 2014-12-24 |
Family
ID=44544336
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PE2014000007A PE20142014A1 (es) | 2011-07-06 | 2012-07-06 | Proceso nuevo en smb |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US9260677B2 (es) |
| EP (1) | EP2613862B1 (es) |
| JP (1) | JP5990580B2 (es) |
| KR (1) | KR101603448B1 (es) |
| CN (1) | CN103796724B (es) |
| AU (1) | AU2012279993B2 (es) |
| BR (1) | BR112014000152B1 (es) |
| CA (1) | CA2815301C (es) |
| CL (1) | CL2013003799A1 (es) |
| DK (1) | DK2613862T3 (es) |
| ES (1) | ES2710652T3 (es) |
| GB (1) | GB201111589D0 (es) |
| HU (1) | HUE043139T2 (es) |
| PE (1) | PE20142014A1 (es) |
| PL (1) | PL2613862T3 (es) |
| TR (1) | TR201819866T4 (es) |
| WO (1) | WO2013005051A1 (es) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2014146265A (ru) | 2009-12-30 | 2015-07-10 | Басф Фарма (Калланиш) Лимитед | Способ хроматографического разделения с псевдодвижущимся слоем |
| GB201111601D0 (en) | 2011-07-06 | 2011-08-24 | Equateq Ltd | New process |
| GB201111594D0 (en) | 2011-07-06 | 2011-08-24 | Equateq Ltd | New improved process |
| GB201111591D0 (en) | 2011-07-06 | 2011-08-24 | Equateq Ltd | Further new process |
| GB201111589D0 (en) | 2011-07-06 | 2011-08-24 | Equateq Ltd | New modified process |
| GB201111595D0 (en) | 2011-07-06 | 2011-08-24 | Equateq Ltd | Improved process |
| GB201300354D0 (en) * | 2013-01-09 | 2013-02-20 | Basf Pharma Callanish Ltd | Multi-step separation process |
| JP6546911B2 (ja) * | 2013-05-07 | 2019-07-17 | グループ ノヴァセップGroupe Novasep | 高度に精製したポリ不飽和脂肪酸を生成するクロマトグラフプロセス |
| US9428711B2 (en) | 2013-05-07 | 2016-08-30 | Groupe Novasep | Chromatographic process for the production of highly purified polyunsaturated fatty acids |
| EP2801604B1 (en) | 2013-05-07 | 2017-04-12 | Groupe Novasep | Chromatographic process for the production of highly purified polyunsaturated fatty acids |
| FR3014435B1 (fr) | 2013-12-11 | 2016-10-21 | Novasep Process | Purification d'acides gras par un procede chromatographique |
| EP3118186B1 (fr) | 2013-12-11 | 2022-02-09 | Novasep Process | Installation chromatographique de production d acides gras polyinsatures |
| FR3014436B1 (fr) | 2013-12-11 | 2016-10-21 | Novasep Process | Procede de purification chromatographique d'un acide gras |
| JP6303017B2 (ja) | 2014-01-07 | 2018-03-28 | ノヴァセプ プロセスNovasep Process | 芳香族アミノ酸を精製する方法 |
| US9163198B2 (en) * | 2014-01-17 | 2015-10-20 | Orochem Technologies, Inc. | Process for purification of EPA (eicosapentanoic acid) ethyl ester from fish oil |
| US9546125B2 (en) * | 2015-02-11 | 2017-01-17 | Orochem Technologies, Inc. | Continuous process for extraction of unsaturated triglycerides from fish oil |
| TWI648258B (zh) * | 2017-07-10 | 2019-01-21 | 喬璞科技有限公司 | 純化不飽和脂肪酸以及二十碳五烯酸的方法 |
| CN111411019A (zh) * | 2020-04-20 | 2020-07-14 | 福建师范大学 | 一种高epa含量的深海鱼油及其加工工艺 |
| CA3238072A1 (en) | 2021-12-17 | 2023-06-22 | Basf Se | Chromatographic separation process for efficient purification of polyunsaturated fatty acids |
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-
2011
- 2011-07-06 GB GBGB1111589.6A patent/GB201111589D0/en not_active Ceased
-
2012
- 2012-07-06 US US13/880,145 patent/US9260677B2/en active Active
- 2012-07-06 EP EP12738160.6A patent/EP2613862B1/en active Active
- 2012-07-06 CA CA2815301A patent/CA2815301C/en active Active
- 2012-07-06 PE PE2014000007A patent/PE20142014A1/es active IP Right Grant
- 2012-07-06 AU AU2012279993A patent/AU2012279993B2/en not_active Ceased
- 2012-07-06 KR KR1020147003083A patent/KR101603448B1/ko active Active
- 2012-07-06 DK DK12738160.6T patent/DK2613862T3/en active
- 2012-07-06 HU HUE12738160A patent/HUE043139T2/hu unknown
- 2012-07-06 CN CN201280033630.8A patent/CN103796724B/zh active Active
- 2012-07-06 BR BR112014000152-9A patent/BR112014000152B1/pt not_active IP Right Cessation
- 2012-07-06 WO PCT/GB2012/051596 patent/WO2013005051A1/en not_active Ceased
- 2012-07-06 ES ES12738160T patent/ES2710652T3/es active Active
- 2012-07-06 JP JP2014517956A patent/JP5990580B2/ja active Active
- 2012-07-06 PL PL12738160T patent/PL2613862T3/pl unknown
- 2012-07-06 TR TR2018/19866T patent/TR201819866T4/tr unknown
-
2013
- 2013-12-30 CL CL2013003799A patent/CL2013003799A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA2815301C (en) | 2015-09-29 |
| US20140128627A1 (en) | 2014-05-08 |
| DK2613862T3 (en) | 2019-03-11 |
| HUE043139T2 (hu) | 2019-07-29 |
| PL2613862T3 (pl) | 2019-05-31 |
| CN103796724B (zh) | 2015-07-15 |
| JP5990580B2 (ja) | 2016-09-14 |
| AU2012279993B2 (en) | 2015-07-23 |
| KR20140034923A (ko) | 2014-03-20 |
| AU2012279993A1 (en) | 2013-05-02 |
| GB201111589D0 (en) | 2011-08-24 |
| BR112014000152B1 (pt) | 2020-10-27 |
| ES2710652T3 (es) | 2019-04-26 |
| EP2613862A1 (en) | 2013-07-17 |
| JP2014523944A (ja) | 2014-09-18 |
| EP2613862B1 (en) | 2018-12-19 |
| KR101603448B1 (ko) | 2016-03-14 |
| US9260677B2 (en) | 2016-02-16 |
| TR201819866T4 (tr) | 2019-01-21 |
| CA2815301A1 (en) | 2013-01-10 |
| BR112014000152A2 (pt) | 2017-02-14 |
| CL2013003799A1 (es) | 2014-07-04 |
| CN103796724A (zh) | 2014-05-14 |
| WO2013005051A1 (en) | 2013-01-10 |
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