PE20121824A1 - Proceso para preparar y purificar acidos grasos - Google Patents
Proceso para preparar y purificar acidos grasosInfo
- Publication number
- PE20121824A1 PE20121824A1 PE2012001069A PE2012001069A PE20121824A1 PE 20121824 A1 PE20121824 A1 PE 20121824A1 PE 2012001069 A PE2012001069 A PE 2012001069A PE 2012001069 A PE2012001069 A PE 2012001069A PE 20121824 A1 PE20121824 A1 PE 20121824A1
- Authority
- PE
- Peru
- Prior art keywords
- acid
- fatty acid
- precipitate
- fatty acids
- preparing
- Prior art date
Links
- 235000014113 dietary fatty acids Nutrition 0.000 title abstract 7
- 229930195729 fatty acid Natural products 0.000 title abstract 7
- 239000000194 fatty acid Substances 0.000 title abstract 7
- 150000004665 fatty acids Chemical class 0.000 title abstract 7
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 3
- 239000002244 precipitate Substances 0.000 abstract 3
- HOBAELRKJCKHQD-UHFFFAOYSA-N (8Z,11Z,14Z)-8,11,14-eicosatrienoic acid Natural products CCCCCC=CCC=CCC=CCCCCCCC(O)=O HOBAELRKJCKHQD-UHFFFAOYSA-N 0.000 abstract 2
- 235000021298 Dihomo-γ-linolenic acid Nutrition 0.000 abstract 2
- HOBAELRKJCKHQD-QNEBEIHSSA-N dihomo-γ-linolenic acid Chemical compound CCCCC\C=C/C\C=C/C\C=C/CCCCCCC(O)=O HOBAELRKJCKHQD-QNEBEIHSSA-N 0.000 abstract 2
- 239000010410 layer Substances 0.000 abstract 2
- 229910003002 lithium salt Inorganic materials 0.000 abstract 2
- 159000000002 lithium salts Chemical class 0.000 abstract 2
- LNAVIIOBBICBIS-NBRVCOCJSA-N CCCCCCCCCCCCCCC\C=C\C=C\C(O)=O Chemical compound CCCCCCCCCCCCCCC\C=C\C=C\C(O)=O LNAVIIOBBICBIS-NBRVCOCJSA-N 0.000 abstract 1
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000012044 organic layer Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
- C07C51/377—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups
- C07C51/38—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups by decarboxylation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Abstract
SE REFIERE A UN PROCESO DE PURIFICACION DE ACIDOS GRASOS QUE COMPRENDE: A) HACER REACCIONAR UN ACIDO GRASO TAL COMO ACIDO DIHOMO-GAMMA-LINOLENICO (DGLA), ACIDO EICOSADIENOICO, ACIDO DOCOSAPENTAENOICO (DPA), ACIDO EICOSATETRAENOICO (ETA) Y ACIDO EICOSATRIENOICO, CON UNA SAL DE LITIO TAL COMO HIDROXIDO DE LITIO EN UNA SOLUCION PARA FORMAR UN PRECIPITADO DE SAL DE LITIO DEL ACIDO GRASO; B) AISLAR EL PRECIPITADO; C) DISOLVER EL PRECIPITADO EN UNA SEGUNDA SOLUCION FORMANDOSE DOS CAPAS INMISCIBLES UNA ORGANICA Y UNA ACUOSA; D) SEPARAR LAS DOS CAPAS INMISCIBLES; E) EVAPORAR LA CAPA ORGANICA PARA AISLAR EL ACIDO GRASO PURIFICADO. TAMBIEN SE REFIERE A UN PROCESO DE PRODUCCION DE ACIDOS GRASOS. DICHO PROCESO PERMITE REMOVER LAS IMPUREZAS NO ACIDAS DE LOS ACIDOS GRASOS
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GBGB1001345.6A GB201001345D0 (en) | 2010-01-27 | 2010-01-27 | Process for preparing and purifying fatty acids |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PE20121824A1 true PE20121824A1 (es) | 2013-01-28 |
Family
ID=42084065
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PE2012001069A PE20121824A1 (es) | 2010-01-27 | 2011-01-27 | Proceso para preparar y purificar acidos grasos |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US9079847B2 (es) |
| EP (1) | EP2528889B1 (es) |
| JP (1) | JP5706446B2 (es) |
| KR (1) | KR101782187B1 (es) |
| CN (1) | CN102844289B (es) |
| AU (1) | AU2011209584B2 (es) |
| BR (1) | BR112012018681B1 (es) |
| CA (1) | CA2787875C (es) |
| DK (1) | DK2528889T3 (es) |
| ES (1) | ES2703280T3 (es) |
| GB (1) | GB201001345D0 (es) |
| HU (1) | HUE041867T2 (es) |
| PE (1) | PE20121824A1 (es) |
| PL (1) | PL2528889T3 (es) |
| PT (1) | PT2528889T (es) |
| RU (1) | RU2553473C2 (es) |
| TR (1) | TR201816300T4 (es) |
| WO (1) | WO2011092467A1 (es) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2916208A1 (en) | 2012-06-17 | 2013-12-27 | Matinas Biopharma, Inc. | Omega-3 pentaenoic acid compositions and methods of use |
| CN103012100B (zh) * | 2012-12-28 | 2016-05-25 | 李赛荣 | 十四酸的纯化方法 |
| CN104098461B (zh) * | 2013-04-12 | 2017-06-16 | 江阴技源药业有限公司 | 一种β‑羟基‑β‑甲基丁酸的纯化方法 |
| FR3014436B1 (fr) * | 2013-12-11 | 2016-10-21 | Novasep Process | Procede de purification chromatographique d'un acide gras |
| JP6825810B2 (ja) * | 2014-02-03 | 2021-02-03 | 備前化成株式会社 | 炭素鎖延長反応による不飽和脂肪酸の化学変換方法 |
| PE20170265A1 (es) * | 2014-04-07 | 2017-03-26 | Epax Norway As | Composicion de acidos grasos monoinsaturados de cadena larga y metodo para la produccion de la misma |
| JP6162646B2 (ja) * | 2014-05-27 | 2017-07-12 | 信越化学工業株式会社 | 3,5−ジメチルドデカン酸の製造方法 |
| US9682055B2 (en) | 2014-06-04 | 2017-06-20 | Dignity Sciences Limted | Pharmaceutical compositions comprising DGLA and use of same |
| JPWO2017002353A1 (ja) * | 2015-06-30 | 2018-04-12 | 備前化成株式会社 | 化学的炭素鎖延長反応による長鎖不飽和脂肪酸の合成 |
| AU2016317523B2 (en) * | 2015-08-31 | 2019-12-12 | Nippon Suisan Kaisha, Ltd. | Free polyunsaturated fatty acid-containing composition and manufacturing method therefor |
| KR102052708B1 (ko) | 2015-12-22 | 2019-12-09 | 주식회사 엘지화학 | 글리세린 탈수 반응용 촉매, 이의 제조 방법 및 상기 촉매를 이용한 아크롤레인의 제조 방법 |
| CN108281637B (zh) * | 2018-01-29 | 2020-07-14 | 蒋央芳 | 一种镍钴锰酸锂的制备方法 |
| WO2020018581A1 (en) | 2018-07-16 | 2020-01-23 | Provivi, Inc. | Synthesis of straight-chain lepidopteran pheromones through one- or two- carbon homologation of fatty alkenes |
| US20210315851A1 (en) | 2020-04-03 | 2021-10-14 | Afimmune Limited | Compositions comprising 15-hepe and methods of treating or preventing hematologic disorders, and/or related diseases |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2228925A (en) * | 1937-11-27 | 1941-01-14 | Jasco Inc | Recovery of fatty acids and alkali salts from soaps |
| GB942452A (en) * | 1959-12-10 | 1963-11-20 | Gernot Grimmer | Unsaturated fatty acids and salts thereof and a process for their preparation |
| FR1552860A (es) | 1967-08-01 | 1969-01-10 | ||
| DE2355856A1 (de) | 1972-11-21 | 1974-05-22 | Akzona Inc | Verfahren zur reinigung neutralisierter fettsaeureamide |
| FR2338327A1 (fr) | 1976-01-13 | 1977-08-12 | Ugine Kuhlmann | Procede de separation des savons a chaines lineaires, des savons a chaines ramifiees et de leurs acides |
| SU739058A1 (ru) * | 1978-01-30 | 1980-06-05 | Предприятие П/Я А-1785 | Способ выделени синтетических жирных кислот |
| US4452994A (en) * | 1981-03-02 | 1984-06-05 | G. D. Searle & Co. | Process for isolating organic compounds and lithium salt complexes useful in said process |
| FI67229C (fi) | 1982-08-17 | 1985-02-11 | Oulu Oy | Foerfarande foer att foerbaettra faergen och faergstabilitetenhos en karboxylsyra eller dess blandning |
| JPS60142940A (ja) * | 1983-12-28 | 1985-07-29 | Otsuka Pharmaceut Co Ltd | Ζ−及びe−9−ヘキサデセン酸の分離法 |
| ES2040847T3 (es) * | 1987-04-27 | 1996-07-16 | Efamol Holdings | Un procedimiento para preparar una composicion farmaceutica que contiene una sal de litio. |
| US5252333A (en) | 1987-04-27 | 1993-10-12 | Scotia Holdings Plc | Lithium salt-containing pharmaceutical compositions |
| SU1766904A1 (ru) * | 1990-06-07 | 1992-10-07 | Matushkin Karp M | Способ выделени синтетических жирных кислот |
| DE4215478A1 (de) * | 1992-05-11 | 1993-11-18 | Solvay Deutschland | Lactobionsäureamidzusammensetzungen und deren Verwenndung |
| DE4304468A1 (de) | 1993-02-15 | 1994-08-18 | Henkel Kgaa | Verfahren zur Herstellung hellfarbiger Polyolester |
| US6310227B1 (en) | 1997-01-31 | 2001-10-30 | The Procter & Gamble Co. | Reduced calorie cooking and frying oils having improved hydrolytic stability, and process for preparing |
| JP4079516B2 (ja) | 1998-06-19 | 2008-04-23 | サントリー株式会社 | トリグリセリドの製造方法 |
| CA2273570A1 (en) | 1999-05-31 | 2000-11-30 | Jfs Envirohealth Ltd. | Concentration and purification of polyunsaturated fatty acid esters by distillation-enzymatic transesterification coupling |
| US20090093648A1 (en) | 2004-03-29 | 2009-04-09 | Purtle Ian C | Soapstock treatment |
| CN100358987C (zh) | 2005-08-05 | 2008-01-02 | 鞍山海华油脂化学有限公司 | 高极压锂基润滑脂 |
| WO2007081269A1 (en) | 2006-01-12 | 2007-07-19 | Ageratec Ab | Process for purification of fatty acid alkyl esters and use of agents to facilitate such purification |
| US7524621B2 (en) | 2007-09-21 | 2009-04-28 | Carestream Health, Inc. | Method of preparing silver carboxylate soaps |
| CN101481637B (zh) | 2008-01-09 | 2012-09-05 | 中国石油化工股份有限公司 | 复合锂基润滑脂的制备方法 |
| GB0800875D0 (en) | 2008-01-17 | 2008-02-27 | Pharma Marine As | Process |
| EP2100910A1 (en) | 2008-03-14 | 2009-09-16 | Solvay Solexis S.p.A. | Process for the purification of polyol PFPE derivative |
| CL2009001343A1 (es) * | 2009-06-02 | 2009-07-10 | Golden Omega S A | Proceso de obtencion concentrado de esteres de epa y dha a partir de aceite marino, que comprende agregar al aceite alcali y agua a menos de 100 grados celsius, agregar solvente, separar fase de refinado, agregar acido, separar la fase no acuosa y agregar alcohol y un catalizador a menos de 150 grados celsius, desolventilizar y destilar. |
-
2010
- 2010-01-27 GB GBGB1001345.6A patent/GB201001345D0/en not_active Ceased
-
2011
- 2011-01-27 PE PE2012001069A patent/PE20121824A1/es not_active Application Discontinuation
- 2011-01-27 WO PCT/GB2011/000104 patent/WO2011092467A1/en not_active Ceased
- 2011-01-27 KR KR1020127022269A patent/KR101782187B1/ko not_active Expired - Fee Related
- 2011-01-27 EP EP11702490.1A patent/EP2528889B1/en not_active Not-in-force
- 2011-01-27 AU AU2011209584A patent/AU2011209584B2/en not_active Ceased
- 2011-01-27 RU RU2012136070/04A patent/RU2553473C2/ru not_active IP Right Cessation
- 2011-01-27 TR TR2018/16300T patent/TR201816300T4/tr unknown
- 2011-01-27 HU HUE11702490A patent/HUE041867T2/hu unknown
- 2011-01-27 DK DK11702490.1T patent/DK2528889T3/en active
- 2011-01-27 ES ES11702490T patent/ES2703280T3/es active Active
- 2011-01-27 PL PL11702490T patent/PL2528889T3/pl unknown
- 2011-01-27 CN CN201180007253.6A patent/CN102844289B/zh not_active Expired - Fee Related
- 2011-01-27 US US13/574,634 patent/US9079847B2/en not_active Expired - Fee Related
- 2011-01-27 CA CA2787875A patent/CA2787875C/en active Active
- 2011-01-27 JP JP2012550509A patent/JP5706446B2/ja not_active Expired - Fee Related
- 2011-01-27 BR BR112012018681A patent/BR112012018681B1/pt not_active IP Right Cessation
- 2011-01-27 PT PT11702490T patent/PT2528889T/pt unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN102844289B (zh) | 2016-01-20 |
| BR112012018681B1 (pt) | 2018-10-16 |
| WO2011092467A1 (en) | 2011-08-04 |
| AU2011209584B2 (en) | 2014-02-06 |
| JP5706446B2 (ja) | 2015-04-22 |
| EP2528889B1 (en) | 2018-10-31 |
| KR101782187B1 (ko) | 2017-09-26 |
| US9079847B2 (en) | 2015-07-14 |
| PT2528889T (pt) | 2019-01-28 |
| CA2787875C (en) | 2017-10-03 |
| RU2012136070A (ru) | 2014-03-10 |
| DK2528889T3 (en) | 2019-01-07 |
| ES2703280T3 (es) | 2019-03-07 |
| TR201816300T4 (tr) | 2018-11-21 |
| US20130150602A1 (en) | 2013-06-13 |
| CN102844289A (zh) | 2012-12-26 |
| EP2528889A1 (en) | 2012-12-05 |
| KR20120132627A (ko) | 2012-12-06 |
| AU2011209584A1 (en) | 2012-08-16 |
| CA2787875A1 (en) | 2011-08-04 |
| HUE041867T2 (hu) | 2019-06-28 |
| PL2528889T3 (pl) | 2019-06-28 |
| GB201001345D0 (en) | 2010-03-17 |
| BR112012018681A2 (pt) | 2016-05-03 |
| JP2013518088A (ja) | 2013-05-20 |
| RU2553473C2 (ru) | 2015-06-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| PE20121824A1 (es) | Proceso para preparar y purificar acidos grasos | |
| AR128483A2 (es) | Formas sólidas de ácido {[5-(3-clorofenil)-3-hidroxipiridin-2-carbonil]amino}acético, sus composiciones y usos | |
| MX374703B (es) | Proceso para purificar una composicion acida que comprende acido 2-formil-furan-5-carboxilico y acido 2,5-furandicarboxilico. | |
| MX2020004603A (es) | Metodos de purificacion de arn mensajero. | |
| CL2014000919A1 (es) | Compuestos derivados de acido 2-tert-butoxi-2-(5-metilbenzo[d]tiazol-6-il) acetico; composicion farmaceutica que los comprende; metodo para tratar una infeccion por vih; y su uso para tratar una infeccion por vih. | |
| CL2013000792A1 (es) | Proceso para concentrar acidos grasos de omega-3 de una mezcla de aceites grasos, que comprende combinar dicha mezcla de aceites con una solucion de sal de plata para formar una fase organica y una acuosa, donde la solucion acuosa de la sal de plata forma un complejo con el acido graso omega-3. | |
| FR2987830B1 (fr) | Procede de purification d'acide phosphorique par nanofiltration | |
| BR112015014895A2 (pt) | processo para produção de produtos de biomassa | |
| AR102365A1 (es) | Purificación de salmuera que contiene litio | |
| AR093986A1 (es) | Cuerpos de carbono ferromagneticos y proceso de produccion | |
| BR112015023313A2 (pt) | métodos para purificação de 5-(halometil)furfural | |
| UY33325A (es) | Purificación mediante adsorción de colorante caramelo | |
| PL2537840T3 (pl) | Sposób wytwarzania walerolaktonu z kwasu lewulinowego | |
| CL2013001560A1 (es) | Procedimiento para la separacion y recuperacion de una sal de metal alcalino purificada que comprende tratamiento de eliminacion de una sustancia inhibidora de la purificacion de una solucion acuosa de sal de metal alcalino con membrana de separacion. | |
| ES2539787T3 (es) | Procedimiento y dispositivo para la purificación de productos de nitración | |
| TR201901100T4 (tr) | Saponinlerin saflaştırılması için işlem. | |
| AR078916A1 (es) | Procedimiento para la purificacion de paliperidona | |
| MX380544B (es) | Purificación de ácido acrílico de origen biológico a ácido acrílico crudo y glacial. | |
| AR086547A1 (es) | Procedimiento de produccion de una solucion de litio a partir de una salmuera | |
| EP2985275A4 (en) | METHOD FOR PURIFYING BETA-HYDROXY-BETA-METHYLBUTYLIC ACID | |
| CL2016001133A1 (es) | Proceso para obtener alginatos o derivados de alginatos a partir de alga marina que comprende la remoción de la superficie externa del estípite, la división del estípite en porciones y la extracción de alginatos o sus derivados | |
| MX2017007191A (es) | Procedimiento de produccion de cristales de derivado de diazabiciclooctano y preparacion liofilizada estable. | |
| BR112013009359A2 (pt) | ácidos cetocarboxílicos, ésteres cetocarboxílicos, métodos de fabricação e usos dos mesmos. | |
| CL2017002290A1 (es) | Proceso para la fabricación de productos de propionato | |
| MX2015011381A (es) | Metodo para purificar acido ferulico y/o sales del mismo. |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FA | Abandonment or withdrawal |