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KR940004005A - 경화가능한 수성 조성물 및 유리섬유 부직물 결합제로서의 용도 - Google Patents

경화가능한 수성 조성물 및 유리섬유 부직물 결합제로서의 용도 Download PDF

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KR940004005A
KR940004005A KR1019930015260A KR930015260A KR940004005A KR 940004005 A KR940004005 A KR 940004005A KR 1019930015260 A KR1019930015260 A KR 1019930015260A KR 930015260 A KR930015260 A KR 930015260A KR 940004005 A KR940004005 A KR 940004005A
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carboxylic acid
salts
aqueous composition
curable aqueous
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토마스 아켄즈 찰스
데이비드 글라임 로버트
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윌리엄 이. 탬버트3세
롬 앤드 하스 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F8/00—Chemical modification by after-treatment
    • C08F8/14—Esterification
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/58—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives
    • D04H1/587—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives characterised by the bonding agents used
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/58—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives
    • D04H1/64—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives the bonding agent being applied in wet state, e.g. chemical agents in dispersions or solutions

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Nonwoven Fabrics (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Reinforced Plastic Materials (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Woven Fabrics (AREA)
  • Artificial Filaments (AREA)
  • Paper (AREA)
  • Surface Treatment Of Glass Fibres Or Filaments (AREA)

Abstract

본 발명은 최소한 둘의 카르복시산기들, 산무수물기들, 또는 그 염들을 포항하는 다중산(polyacid) : 최소한 둘의 히드록시기를 포함하는 다가 알코올(polyol) ; 및 인-함유 촉진제 (phosporous-containing accerator)률 포함하는, 포름알데히드-비함유 경화가능한 수성 조성물에 관한 것 이다. 본 발명의 조성물은 유리섬유로 구성된 부직물 같은 내열성 부직물들에 대한 결합제로서 사용될 수 있다.

Description

경화가능한 수성 조성물 및 유리섬유 부직물 결합제로서의 용도
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (27)

  1. (a)최소한 둘의 카르복시산기들, 산무수물기들, 또는 그 염들을 포함하는 다중산(polyacid) ; (b)최소한 둘의 히드록시기를 포함하는 다가 알코올 (Polyol) ; 및 (c) 인 -함유 촉진제 (phosporous-containing accerator) 를 함유하며, 상기 카르복시산기들, 산무수물기들 또는 그 염까지 당량수/상기 히드록시기들의 당량수의 비는 1/0.01내지 1/3이고, 상기 카르복시산기들, 산무수물기들, 또는 그 염들은 비휘발성 염기와 함께 35%이하 수준까지 중화된 것인, 경화가능한 수성 조성물.
  2. 제1항에 있어서, 상기 다중산이 중합체 다중산인 경화가능한 수성 조성물.
  3. 제2항에 있어서, 상기 중합체 다중산이 최소한 하나의 공중합성 에틸렌계 불포화 카르복시산-함유 단량체를 포함하는 첨가 중합체인 경화가능한 수성 조성물
  4. 제1항에 있어서, 상기 다가 알코올이 최소한 둘의 히드록시기들을 함유하는 분자량 1000이하의 화합물인 경화가능한 수성 조성물.
  5. 제4항에 있어서, 상기 다가 알코올이 히드록시아민인 경화간능한 수성 조성물.
  6. 제5항에 있어서, 상기 히드록시아민이 디이소프로판올아민, 2- (2-아미노에틸아미노)에탄올, 트리에탄올 아민, 트리스(히드록시메틸)아미노메탄, 및 디에탄올아민으로 구성된 군으로부터 선택된 것인 경화가능한 수성 조성물.
  7. 제1항에 있어서, 상기 카르복시산기들, 산무수물기들, 또는 그 염들의 당량수/상기 히드록시기들의 당량수 비가 1/0.2 내지 1/1인 경화가능한 수성 조성물.
  8. (a)최소한 둘의 카르복시산기들, 산무수물기들, 또는 그 염들을 포함하는 다중산 및 (b)최소한 둘의 히드록시기들을 포함하는 매우 반응성인 다가 알코올(highlyreactive polyol)을 함유하며, 상기 카르복시산기들, 산 무수물기들 또는 그 염들의 당량수/상기 히드록시기들의 당량수의 비는 1/0.01 내지 1/3이고, 상기 카르복시산기들, 산무수물기들, 또는 그 염들은 비휘발성 염기와 함께 35%이하 수중까지 중화된 것인, 경화가능한 수성 조성물.
  9. 제8항에 있어서, 상기 매우 반응성인 다가 알코올이 다음 일반식을 갖는 것인 경화가능한 수성 조성물
    (HO-CH(R3)CH2)2N-C(0)(CH2)m-C(0)-N(CH2CH(R3)OH)2
    상기 식에서, R3는 둘다 H이거나 또는 둘다 -CH3이다.
  10. 다음 단계들을 포함하는, 다중산들의 경화방법.
    (a) (1)최소한 둘의 카르복시산기들, 산무수물기들, 또는 그 염들을 포함하는 다중산; (2)최소한 둘의 히드록시기를 포함하는 다가 알코올; 및 (3)인-함유 촉진제를 혼합시켜 경화가능한 수성 조성물을 형성함(여기서, 상기 카르복시산기들. 산무수물기들, 또는 그 염들외 당량수/상기 히드록시기들의 당량수의 비는 1/0.01 내지 1/3이고, 상기 카르복시산기들, 산무수물기들, 또는 그 염들은 비휘발성염기와 함께 35%이하의 수준까지 중화된 것임) ; 및 (b)상기 경화가능한 수성조성물을 120-400℃의 온도에서 가열시킴.
  11. 제10항에 있어서, 상기 다중산이 중합체 다중산인 것인 방법.
  12. 제11항에 있어서, 상기 중합체 다중산이 최소한 하나의 공중합성 에틸렌 불포화 카르복시산-함유 단량체를 포함하는 첨가 중함체인 것인 방법.
  13. 제10항에 있어서, 상기 다가 알코올이 최소한 둘의 히드록시기들을 함유하는 분자량 1000이항의 화합물인것 인 방법.
  14. 제13항에 있어서, 상기 다가 알코올이 히드록시아민인 것인 방법
  15. 제14항에 있어서, 상기 히드록시아민이 디이소프로판올아민. 2- (2-아미노에틸아미노)에탄올, 트리에탄올아민, 트리스(히드록시메틸)아미노메탄, 및 디에탄올아민으로 구서어된 군으로부터 선택된 것인 방법.
  16. 제10항에 있어서, 상기 카르복시산기들, 산무수물기들, 또는 그 염들의 당량수/상기 히드록시기들의 당량수 비가 1/0.2내지 1/1인 경화가능한 것인 방법.
  17. 제10항에 있어서, 상기 경화가능한 수성 조성물이 상기 청구범위 제8항의 경화가능한 수성 조성물인 것인 방법.
  18. 제17항에 있어서, 매우 반응성인 다가 알코올이 다음 일반식을 갖는 것인 방법
    (HO-CH(R3)CH2)2N-C(0)(CH2)m-C(0)-N(CH2CH(R3)OH)2
    상기 식에서, R3는 둘다 H이거나 또는 둘다 -CH3이다.
  19. 다음 단계들을 포함하는, 다중산들의 경화방법.
    (a) (1)최소한 둘의 카르복시산기들, 산무수물기들, 또는 그 염들을 포함하는 다중산: (2)최소한 둘의 히드록시기를 포함하는 다가 알코올; 및 (3)인-함유 촉진제를 혼합시켜 경화가능한 수성 조성물을 형성함(여기서, 상기 카르복시산기들, 산무수물기들, 또는 그 염들의 당량수/상기 히드록시기들의 당량수의 비는 1/0.01 내지 1/3이고, 상기 카르복시산기들, 산무수물기들, 또는 그 염들은 비휘발성염기와 함께 35%이하의 수준까지 중화된 것임) ; 및 (b) 내 열성 부직물 또는 그외 섬우들을 상기 경화가능한 수성 조성물과 함께 접촉시킴 : 및 (c)상기 경화가능한 수성조성물을 120-400℃의 온도에서 가열시킴.
  20. 제19항에 있어서, 상기 다중산이 중합체 다중산인 것인 방법.
  21. 제19항에 있어서, 상기 중합체 다중산이 최소한 하나의 공중합성 에틸렌계 불포화 카르복시산-함유 단량체를 포함하는 첨가 중합체인 것인 방법.
  22. 제17항에 있어서, 상기 다가 알코올이 최소한 둘의 히드록시들을 함유하는 분자량 1000이하의 화합물인 것인 방법.
  23. 제22항에 있어서, 상기 다가 알코올이 히드록시아민인 것인 방법
  24. 제23항에 있어서, 상기 히드록시아민이 디이소프로판올아민, 2-(2-아미노에틸아미노)에탄올, 트리에탄올아민, 트리스(히드록시메틸)아미노메탄, 및 디에탄올아민으로 구성된 군으로부터 선택된 것인 방법.
  25. 제19항에 있어서, 상기 카르복시산기들, 산무수물기들, 또는 그 염들의 당량수/상기 히드록시기들의 당량수 비가 1/0.2내지 1/1인 경화가능한 것인 방법,
  26. 제19항에 있어서, 상기 경화가능한 수성 조성물이 상기 청구범위 제8항의 경화가능한 수성 조성물인 것인 방법.
  27. 제19항에 있어서, 매우 반응성인 다가 알코올이 다음 일반식을 갖는 것인 방법.
    (HO-CH(R3)CH2)2N-C(0)(CH2)m-C(0)-N(CH2CH(R3)OH)2
    상기 식에서, R3는 둘다 H이거나 또는 둘다 -CH3이다
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019930015260A 1992-08-06 1993-08-06 경화가능한 수성 조성물 및 유리섬유 부직물 결합제로서의 용도 Ceased KR940004005A (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US92626292A 1992-08-06 1992-08-06
US926,262 1992-08-06
US08/075,715 US5661213A (en) 1992-08-06 1993-06-11 Curable aqueous composition and use as fiberglass nonwoven binder
US075,715 1993-06-11

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KR940004005A true KR940004005A (ko) 1994-03-14

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US (4) US5661213A (ko)
EP (1) EP0583086B2 (ko)
JP (1) JP3215233B2 (ko)
KR (1) KR940004005A (ko)
CN (1) CN1060793C (ko)
AT (1) ATE160597T1 (ko)
AU (1) AU667921B2 (ko)
BR (1) BR9303315A (ko)
CA (1) CA2101450A1 (ko)
CZ (1) CZ159293A3 (ko)
DE (1) DE69315393T3 (ko)
DK (1) DK0583086T3 (ko)
ES (1) ES2109441T5 (ko)
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GR (1) GR3026182T3 (ko)
HU (1) HUT66516A (ko)
IL (1) IL106446A (ko)
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MY (1) MY110113A (ko)
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MX9304685A (es) 1994-03-31
EP0583086A1 (en) 1994-02-16
EP0583086B2 (en) 2002-08-28
AU667921B2 (en) 1996-04-18
MY110113A (en) 1998-01-27
US5763524A (en) 1998-06-09
CZ159293A3 (en) 1994-03-16
DE69315393T3 (de) 2003-01-30
JPH06184285A (ja) 1994-07-05
ZA935397B (en) 1994-02-07
US6221973B1 (en) 2001-04-24
DK0583086T3 (da) 1998-02-02
US6136916A (en) 2000-10-24
ES2109441T5 (es) 2003-03-16
IL106446A (en) 1997-09-30
NZ248215A (en) 1995-09-26
ATE160597T1 (de) 1997-12-15
DE69315393T2 (de) 1998-04-30
IL106446A0 (en) 1993-11-15
HUT66516A (en) 1994-12-28
AU4212793A (en) 1994-04-28
CN1083844A (zh) 1994-03-16
ES2109441T3 (es) 1998-01-16
US5661213A (en) 1997-08-26
GR3026182T3 (en) 1998-05-29
HK1001096A1 (en) 1998-05-22
SK82993A3 (en) 1994-04-06
HU9302275D0 (en) 1993-11-29
FI933473L (fi) 1994-02-07
CN1060793C (zh) 2001-01-17
FI933473A0 (fi) 1993-08-05
TW265349B (en) 1995-12-11
BR9303315A (pt) 1994-03-22
DE69315393D1 (de) 1998-01-08
JP3215233B2 (ja) 2001-10-02
EP0583086B1 (en) 1997-11-26
CA2101450A1 (en) 1994-02-07
FI933473A7 (fi) 1994-02-07

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