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KR900701988A - 계면활성제-함유 과립의 제조방법 - Google Patents

계면활성제-함유 과립의 제조방법

Info

Publication number
KR900701988A
KR900701988A KR1019900701333A KR900701333A KR900701988A KR 900701988 A KR900701988 A KR 900701988A KR 1019900701333 A KR1019900701333 A KR 1019900701333A KR 900701333 A KR900701333 A KR 900701333A KR 900701988 A KR900701988 A KR 900701988A
Authority
KR
South Korea
Prior art keywords
water
weight
granules
nonionic surfactant
insoluble solids
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
KR1019900701333A
Other languages
English (en)
Other versions
KR970001224B1 (en
Inventor
윌름즈 엘마르
Original Assignee
게오르그 챠이트, 호르스트 헤를레
헨켈 코만디트 게젤샤프트 아우프 아크티엔
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 게오르그 챠이트, 호르스트 헤를레, 헨켈 코만디트 게젤샤프트 아우프 아크티엔 filed Critical 게오르그 챠이트, 호르스트 헤를레
Publication of KR900701988A publication Critical patent/KR900701988A/ko
Application granted granted Critical
Publication of KR970001224B1 publication Critical patent/KR970001224B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/72Ethers of polyoxyalkylene glycols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets
    • C11D17/065High-density particulate detergent compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/124Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246Silicates, e.g. diatomaceous earth
    • C11D3/1253Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/126Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/124Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246Silicates, e.g. diatomaceous earth
    • C11D3/128Aluminium silicates, e.g. zeolites

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Medicinal Preparation (AREA)
  • Colloid Chemistry (AREA)
  • Cosmetics (AREA)
  • Glanulating (AREA)
  • Superconductors And Manufacturing Methods Therefor (AREA)

Abstract

내용 없음

Description

계면활성제-함유 과립의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. (A)임의로 수용성 또는 수불용성 고형분 총량의 일부(50중량%미만)을 용해된 또는 분산된 형태로 함유할 수 있는 비이온성 계면활성제를 물과 혼합하여 점성 겔상을 형성한후, (B)남은 대부분의 양의 수용성 또는 수불용성 고형분을 분말형으로 가하고, 생성되는 혼합물을 기계적으로 처리하여, 무수물로 표시되는 총 고형분 존재량에 대한 겔 상에서의 비이온성 계면활성제 및 물의 중량비가 25:75~65:35인 과립을 형성시킴을 특징으로 하는, 폴리글리콜 에테르 유도체계 유래의 비이온성 계면활성제, 미분쇄된 수용성 및/또는 수불용성 고형분 및 물을 함유하는 고 외견상 밀도를 갖는 자유-유동성 과립의 제조방법.
  2. 제1항에 있어서, 총 고형분 존재량에 대한 겔 상(A)에서의 비이온성 계면활성제 및 물의 비가 30 : 70∼60 : 40인 방법.
  3. 제1항 또는 2항에 있어서, 총 고형분 존재량의 0∼40중량%, 바람직하게는 0∼30중량%, 보다 바람직하게는 5∼25중량%가 젤상(A)의 형성시 사용되고, 남은 대부분의 양이 건조분말로 과립상(B)에서 첨가되는 방법.
  4. 제3항에 있어서, 100㎛미만, 바람직하게는 50㎛미만인 그레인 크기를 갖는 수불용성 고형분이 사용되는 방법.
  5. 제4항에 있어서, 미세 결정성 제올라이트, 벤토나이트 또는 그의 혼합물이 수불용성 고형분으로 사용되는 방법.
  6. 제1항 내지 4항중 어느 한 항에 있어서, 형성되는 과립의 외견상 밀도가 최대치에 이를때까지만 겔상을 분말형 고형분과 혼합하는 방법.
  7. 제1항 내지 4항중 어느 한 항에 있어서, 비이온성 계면활성제가, 무수불을 기준으로 제올라이트 35∼55중량%, 분산안정화제로 작용하는 비이온성 계면활성제 0.5∼5중량%및 물 64.5∼40중량%를 함유하는 미세결정성 제올라이트의 수성 분산액과 혼합되어 겔이 형성되는 방법.
  8. 제1항 내지 6항중 어느 한 항에 기재된 방법에 의해 제조된 과립.
  9. 제8항에 있어서, 외견상 밀도가 600∼1,000 g/l, 바람직하게는 650∼900 g/l인 과립.
  10. 제8항 내지 9항에 기재된 과립을 함유하는 과립상 세제 및 청정제제.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR90701333A 1988-10-21 1990-06-21 Process for the production of surfactant-containing granulates Expired - Fee Related KR970001224B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DEP3835918.9 1988-10-21
DE3835918A DE3835918A1 (de) 1988-10-21 1988-10-21 Verfahren zur herstellung von tensidhaltigen granulaten
PCT/EP1989/001206 WO1990004629A2 (de) 1988-10-21 1989-10-12 Verfahren zur herstellung von tensidhaltigen granulaten

Publications (2)

Publication Number Publication Date
KR900701988A true KR900701988A (ko) 1990-12-05
KR970001224B1 KR970001224B1 (en) 1997-02-04

Family

ID=6365638

Family Applications (1)

Application Number Title Priority Date Filing Date
KR90701333A Expired - Fee Related KR970001224B1 (en) 1988-10-21 1990-06-21 Process for the production of surfactant-containing granulates

Country Status (11)

Country Link
US (1) US5354493A (ko)
EP (2) EP0364881A3 (ko)
JP (1) JP2704020B2 (ko)
KR (1) KR970001224B1 (ko)
AT (1) ATE117718T1 (ko)
DE (2) DE3835918A1 (ko)
DK (1) DK71791D0 (ko)
ES (1) ES2067569T3 (ko)
PT (1) PT92060A (ko)
TR (1) TR24142A (ko)
WO (1) WO1990004629A2 (ko)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3943019A1 (de) * 1989-12-27 1991-07-04 Henkel Kgaa Granulares, avivierend wirkendes waschmitteladditiv und verfahren zu seiner herstellung
KR0170424B1 (ko) * 1990-07-05 1999-01-15 호르스트 헤를레,요한 글라슬 세제 및 청정제용 표면 활성제 과립의 제조방법
US5108646A (en) * 1990-10-26 1992-04-28 The Procter & Gamble Company Process for agglomerating aluminosilicate or layered silicate detergent builders
DE4110510A1 (de) * 1991-03-30 1992-10-01 Henkel Kgaa Niederalkalische, chlor- und phosphatfreie maschinengeschirrspuelmittel in form von schwerpulvern und -granulaten
DE4127323A1 (de) * 1991-08-20 1993-02-25 Henkel Kgaa Verfahren zur herstellung von tensidgranulaten
DE4137470A1 (de) * 1991-11-14 1993-05-19 Henkel Kgaa Verfahren zur herstellung niederalkalischer, aktivchlor- und phosphatfreier maschinengeschirrspuelmittel in form von schwergranulaten
CA2083331C (en) * 1991-11-26 1998-08-11 Johannes H. M. Akkermans Detergent compositions
DE4203789A1 (de) * 1992-02-10 1993-08-12 Henkel Kgaa Verfahren zur stabilisierung von waessrigen zeolith-suspensionen
DE4216629A1 (de) * 1992-05-20 1993-11-25 Henkel Kgaa Verfahren zur Herstellung aniontensidhaltiger Wasch- und Reinigungsmittel
EP0622454A1 (en) * 1993-04-30 1994-11-02 The Procter & Gamble Company Structuring liquid nonionic surfactants prior to granulation process
ATE188991T1 (de) * 1993-09-13 2000-02-15 Procter & Gamble Granulare waschmittelzusammensetzungen mit nichtionischem tensid und verfahren zu ihrer herstellung
GB9324129D0 (en) * 1993-11-24 1994-01-12 Unilever Plc Detergent compositions and process for preparing them
US5496486A (en) * 1994-06-30 1996-03-05 Amway Corporation Process for increasing liquid surfactant loading in free flowing powder detergents
EP0694608A1 (en) * 1994-07-28 1996-01-31 The Procter & Gamble Company Process for making granular detergents and detergent compositions comprising nonionic surfactant
TW326472B (en) * 1994-08-12 1998-02-11 Kao Corp Method for producing nonionic detergent granules
WO1996025482A1 (en) * 1995-02-13 1996-08-22 The Procter & Gamble Company Process for producing detergent agglomerates in which particle size is controlled
US5574005A (en) * 1995-03-07 1996-11-12 The Procter & Gamble Company Process for producing detergent agglomerates from high active surfactant pastes having non-linear viscoelastic properties
US5888419A (en) * 1995-06-07 1999-03-30 The Clorox Company Granular N-alkyl ammonium acetontrile compositions
GB9513327D0 (en) * 1995-06-30 1995-09-06 Uniliver Plc Process for the production of a detergent composition
DE19603760A1 (de) * 1996-02-02 1997-08-07 Henkel Kgaa Feste Reinigungsmittelzubereitungen
GB9605534D0 (en) * 1996-03-15 1996-05-15 Unilever Plc Detergent compositions
GB9711356D0 (en) 1997-05-30 1997-07-30 Unilever Plc Particulate detergent composition
US7625855B2 (en) * 1999-08-11 2009-12-01 Gonzalez Gustavo M Cleaning compositions for removing organic deposits in hard to reach surfaces
US6057280A (en) 1998-11-19 2000-05-02 Huish Detergents, Inc. Compositions containing α-sulfofatty acid esters and methods of making and using the same
DE19913995A1 (de) 1999-03-29 2000-10-05 Basf Ag Verfahren zur Herstellung von körnigen N-Alkylamoniumacetonitril-Salzen
DE10008815A1 (de) * 2000-02-25 2001-08-30 Sued Chemie Ag Schichtmineralhaltige Agglomerate mit nichtionischen Tensiden
CN108837784A (zh) * 2018-06-07 2018-11-20 曾婧 一种改进的用于生产洗涤剂组合物颗粒的方法

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2874123A (en) * 1954-09-07 1959-02-17 Colgate Palmolive Co Process for the preparation of granular compositions
US3769222A (en) * 1971-02-09 1973-10-30 Colgate Palmolive Co Free flowing nonionic surfactants
ZA734721B (en) 1972-07-14 1974-03-27 Procter & Gamble Detergent compositions
AT330930B (de) 1973-04-13 1976-07-26 Henkel & Cie Gmbh Verfahren zur herstellung von festen, schuttfahigen wasch- oder reinigungsmitteln mit einem gehalt an calcium bindenden substanzen
US4166039A (en) * 1973-10-15 1979-08-28 The Proctor & Gamble Company Detergent composition and process
AT335035B (de) * 1974-10-10 1977-02-25 Henkel & Cie Gmbh Stabile suspensionen wasserunloslicher, zum binden von calciumionen befahigter silikate und deren verwendung zur herstellung von wasch- und reinigungsmitteln
US4169075A (en) * 1974-10-10 1979-09-25 Henkel Kommanditgesellschaft Auf Aktien Process for the production of powdery washing agents by spray-drying
GB1545810A (en) * 1976-11-02 1979-05-16 Albright & Wilson Manufacture of detergents
DE2837504C2 (de) * 1978-08-28 1983-07-07 Henkel KGaA, 4000 Düsseldorf Verfahren zur Herstellung eines schüttfähigen, nichtionische Tenside enthaltenden Wasch- und Reinigungsmittelgranulates
EP0026529B2 (en) 1979-09-29 1992-08-19 THE PROCTER & GAMBLE COMPANY Detergent compositions
ATE5896T1 (de) * 1979-11-03 1984-02-15 The Procter & Gamble Company Granulare waschmittelzusammensetzungen.
AU549000B2 (en) 1981-02-26 1986-01-09 Colgate-Palmolive Pty. Ltd. Base beads for detergent compositions
GB8329880D0 (en) * 1983-11-09 1983-12-14 Unilever Plc Particulate adjuncts
DE3444311A1 (de) * 1984-12-05 1986-06-05 Degussa Ag, 6000 Frankfurt Waessrige stabile suspension wasserunloeslicher, zum binden von calciumionen befaehigter silikate und deren verwendung zur herstellung von wasch- und reinigungsmitteln
DE3444960A1 (de) * 1984-12-10 1986-06-12 Henkel KGaA, 4000 Düsseldorf Koerniges adsorptionsmittel
US4970017A (en) * 1985-04-25 1990-11-13 Lion Corporation Process for production of granular detergent composition having high bulk density
DE3526405A1 (de) * 1985-07-24 1987-02-05 Henkel Kgaa Schichtsilikate mit beschraenktem quellvermoegen, verfahren zu ihrer herstellung und ihre verwendung in wasch- und reinigungsmitteln
US4894117A (en) * 1988-04-28 1990-01-16 Colgate-Palmolive Company Process for manufacturing high bulk density particulate fabric softening synthetic anionic organic detergent compositions
US4925585A (en) * 1988-06-29 1990-05-15 The Procter & Gamble Company Detergent granules from cold dough using fine dispersion granulation

Also Published As

Publication number Publication date
WO1990004629A2 (de) 1990-05-03
DE3835918A1 (de) 1990-04-26
US5354493A (en) 1994-10-11
TR24142A (tr) 1991-04-09
JP2704020B2 (ja) 1998-01-26
DK71791A (da) 1991-04-19
ES2067569T3 (es) 1995-04-01
EP0536110B1 (de) 1995-01-25
KR970001224B1 (en) 1997-02-04
WO1990004629A3 (de) 1991-05-30
ATE117718T1 (de) 1995-02-15
EP0364881A2 (de) 1990-04-25
PT92060A (pt) 1990-04-30
JPH04501129A (ja) 1992-02-27
EP0536110A1 (de) 1993-04-14
DK71791D0 (da) 1991-04-19
EP0364881A3 (de) 1990-06-06
DE58908952D1 (de) 1995-03-09

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