JPH0583534B2 - - Google Patents
Info
- Publication number
- JPH0583534B2 JPH0583534B2 JP5203985A JP5203985A JPH0583534B2 JP H0583534 B2 JPH0583534 B2 JP H0583534B2 JP 5203985 A JP5203985 A JP 5203985A JP 5203985 A JP5203985 A JP 5203985A JP H0583534 B2 JPH0583534 B2 JP H0583534B2
- Authority
- JP
- Japan
- Prior art keywords
- cellulose
- optical resolution
- formula
- chloropropionic
- chloropropionic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- GAWAYYRQGQZKCR-UHFFFAOYSA-N 2-chloropropionic acid Chemical class CC(Cl)C(O)=O GAWAYYRQGQZKCR-UHFFFAOYSA-N 0.000 claims description 9
- 229920002678 cellulose Polymers 0.000 claims description 6
- 239000001913 cellulose Substances 0.000 claims description 6
- 230000003287 optical effect Effects 0.000 claims description 6
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 229920002284 Cellulose triacetate Polymers 0.000 claims description 2
- NNLVGZFZQQXQNW-ADJNRHBOSA-N [(2r,3r,4s,5r,6s)-4,5-diacetyloxy-3-[(2s,3r,4s,5r,6r)-3,4,5-triacetyloxy-6-(acetyloxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6s)-4,5,6-triacetyloxy-2-(acetyloxymethyl)oxan-3-yl]oxyoxan-2-yl]methyl acetate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](OC(C)=O)[C@H]1OC(C)=O)O[C@H]1[C@@H]([C@@H](OC(C)=O)[C@H](OC(C)=O)[C@@H](COC(C)=O)O1)OC(C)=O)COC(=O)C)[C@@H]1[C@@H](COC(C)=O)O[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]1OC(C)=O NNLVGZFZQQXQNW-ADJNRHBOSA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 150000004676 glycans Chemical class 0.000 claims description 2
- 229920001282 polysaccharide Polymers 0.000 claims description 2
- 239000005017 polysaccharide Substances 0.000 claims description 2
- 239000004480 active ingredient Substances 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- -1 2-isopropylphenyl α-chloropropionate Chemical compound 0.000 description 4
- BWWXKHHVIAJJFM-UHFFFAOYSA-N 2-chloro-n-phenylpropanamide Chemical compound CC(Cl)C(=O)NC1=CC=CC=C1 BWWXKHHVIAJJFM-UHFFFAOYSA-N 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 238000004811 liquid chromatography Methods 0.000 description 2
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 2
- HBAQYPYDRFILMT-UHFFFAOYSA-N 8-[3-(1-cyclopropylpyrazol-4-yl)-1H-pyrazolo[4,3-d]pyrimidin-5-yl]-3-methyl-3,8-diazabicyclo[3.2.1]octan-2-one Chemical class C1(CC1)N1N=CC(=C1)C1=NNC2=C1N=C(N=C2)N1C2C(N(CC1CC2)C)=O HBAQYPYDRFILMT-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 230000005526 G1 to G0 transition Effects 0.000 description 1
- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 235000004279 alanine Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- VDCSGNNYCFPWFK-UHFFFAOYSA-N diphenylsilane Chemical compound C=1C=CC=CC=1[SiH2]C1=CC=CC=C1 VDCSGNNYCFPWFK-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000002363 herbicidal effect Effects 0.000 description 1
- 239000004009 herbicide Substances 0.000 description 1
- QKGYJVXSKCDGOK-UHFFFAOYSA-N hexane;propan-2-ol Chemical compound CC(C)O.CCCCCC QKGYJVXSKCDGOK-UHFFFAOYSA-N 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5203985A JPS61212539A (ja) | 1985-03-15 | 1985-03-15 | α−クロロプロピオン酸類の光学分割方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5203985A JPS61212539A (ja) | 1985-03-15 | 1985-03-15 | α−クロロプロピオン酸類の光学分割方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61212539A JPS61212539A (ja) | 1986-09-20 |
| JPH0583534B2 true JPH0583534B2 (es) | 1993-11-26 |
Family
ID=12903672
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5203985A Granted JPS61212539A (ja) | 1985-03-15 | 1985-03-15 | α−クロロプロピオン酸類の光学分割方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61212539A (es) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| USRE43573E1 (en) | 1997-02-24 | 2012-08-14 | Genesis Microchip (Delaware) Inc. | Method and system for displaying an analog image by a digital display device |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0796503B2 (ja) * | 1986-07-04 | 1995-10-18 | ダイセル化学工業株式会社 | α−置換酢酸エステル類の光学分割方法 |
| CN113607840B (zh) * | 2021-07-29 | 2023-06-30 | 山东京博农化科技股份有限公司 | 一种2-氯丙酸手性异构体的分离检测方法 |
-
1985
- 1985-03-15 JP JP5203985A patent/JPS61212539A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| USRE43573E1 (en) | 1997-02-24 | 2012-08-14 | Genesis Microchip (Delaware) Inc. | Method and system for displaying an analog image by a digital display device |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS61212539A (ja) | 1986-09-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Wang et al. | Enantiomeric separation of some pharmaceutical intermediates and reversal of elution orders by high-performance liquid chromatography using cellulose and amylose tris (3, 5-dimethylphenylcarbamate) derivatives as stationary phases | |
| DE122005000045I1 (de) | R-Enantiomer von N-Propargyl-1-aminoindan, dessen Herstellung und dieses enthaltende pharmazeutischeZusammensetzungen. | |
| FR2623498B1 (fr) | Nouveaux composes enantiomeres derives d'amino-acides, leur procede de preparation et leurs applications therapeutiques | |
| FR2395263A1 (fr) | Derives d'acides thiadiazole-1, 2, 3 carboxyliques-5 utilisables comme matieres actives de produits herbicides | |
| HU202180B (en) | Process for producing 3,6-dichloro-2-methoxybenzoic acid salt | |
| RU94019417A (ru) | Способ получения фармацевтической композиции, фармацевтическая композиция, фармацевтический препарат, способы получения фармацевтического препарата | |
| JPH0583534B2 (es) | ||
| TNSN97060A1 (fr) | Procede pour preparer des acides cycloalcano - indole - et azaindole- et pyrimido (1,2-a) indole-carboxylique purs d'un point de vue enantiomere, et leurs derives actives | |
| Vashistha | Enantioselective analysis of mexiletine using chromatographic techniques: A review | |
| Hyun et al. | Resolution of tocainide and its analogues on liquid chromatographic chiral stationary phases based on (+)-(18-crown-6)-2, 3, 11, 12-tetracarboxylic acid | |
| EP0040991B1 (en) | Preparation of insecticidal mixture of stereoisomers of alpha-cyano-3-phenoxybenzyl isovalerates | |
| Ackermann et al. | The optical isomers of α‐cyano‐3‐phenoxybenzyl 3‐(1, 2‐dibromo‐2, 2‐dichloroethyl)‐2, 2‐dimethylcyclo‐propanecarboxylate and their insecticidal activities | |
| Hyun et al. | Enantiomeric separation of tocainide and its analogues on an optically active crown ether-based stationary phase by liquid chromatography | |
| SU1241989A3 (ru) | Способ получени (-)-2- @ 1-(2,6-дихлорфенокси)этил @ -1,3-диазациклопентена-2 или его гидрохлорида | |
| Török et al. | High-performance liquid chromatographic enantioseparation of bicalutamide and its related compounds | |
| JPH0215531B2 (es) | ||
| JPH0780793B2 (ja) | クロマト分離法 | |
| Hamper et al. | Analytical and preparative separation of the enantiomers of pyrazole phenyl ether herbicides on three chiral stationary phases | |
| Akanya et al. | Direct resolution of isomeric and diastereoisomeric mixtures of amides, lactones, alcohols, carbazones and pyrethenoid derivatives | |
| JPH06343857A (ja) | 固定相 | |
| KR100949758B1 (ko) | 항생제인 세파클러를 기저로 하는 키랄 고정상 및 이들로충진된 키랄컬럼 | |
| JP2912075B2 (ja) | ガスクロマトグラフィー用充填剤 | |
| JPS62135450A (ja) | 光学活性なベ−タ遮断薬の製造方法 | |
| FR2447373A1 (fr) | Produits derives de l'aniline ayant une activite antifongique ainsi que leur procede de preparation | |
| JPH05246950A (ja) | ジャスモン酸メチルおよびその関連物質の光学異性体分離法 |