ES2033117T3 - Nuevo procedimiento de fabricacion industrial del parahidroximandelato sodico. - Google Patents
Nuevo procedimiento de fabricacion industrial del parahidroximandelato sodico.Info
- Publication number
- ES2033117T3 ES2033117T3 ES198989402790T ES89402790T ES2033117T3 ES 2033117 T3 ES2033117 T3 ES 2033117T3 ES 198989402790 T ES198989402790 T ES 198989402790T ES 89402790 T ES89402790 T ES 89402790T ES 2033117 T3 ES2033117 T3 ES 2033117T3
- Authority
- ES
- Spain
- Prior art keywords
- parhydroximandelate
- sodium
- manufacturing procedure
- industrial manufacturing
- new industrial
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 229910052708 sodium Inorganic materials 0.000 title 1
- 239000011734 sodium Substances 0.000 title 1
- HHLFWLYXYJOTON-UHFFFAOYSA-N glyoxylic acid Chemical compound OC(=O)C=O HHLFWLYXYJOTON-UHFFFAOYSA-N 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 2
- YHXHKYRQLYQUIH-UHFFFAOYSA-N 4-hydroxymandelic acid Chemical compound OC(=O)C(O)C1=CC=C(O)C=C1 YHXHKYRQLYQUIH-UHFFFAOYSA-N 0.000 abstract 1
- YKGBNAGNNUEZQC-UHFFFAOYSA-N 6-methyl-n,n-bis(6-methylheptyl)heptan-1-amine Chemical compound CC(C)CCCCCN(CCCCCC(C)C)CCCCCC(C)C YKGBNAGNNUEZQC-UHFFFAOYSA-N 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
- IMFACGCPASFAPR-UHFFFAOYSA-N tributylamine Chemical compound CCCCN(CCCC)CCCC IMFACGCPASFAPR-UHFFFAOYSA-N 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
- C07C51/367—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of functional groups containing oxygen only in singly bound form
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
ESTE PROCEDIMIENTO SE CARACTERIZA POR EL HECHO DE QUE SE HACE REACCIONAR EL ACIDO GLIOXILICO EN DISOLUCION ACUOSA CON UN EXCESO DE FENOL, EN PRESENCIA DE UNA AMINA TERCIARIA INSOLUBLE O POCO SOLUBLE EN AGUA, Y LIQUIDA A LA TEMPERATURA AMBIENTE, ESPECIALMENTE TRIBUTILAMINA O TRIISOOCTILAMINA, Y PORQUE DESPUES SE SALIFICA EL ACIDO PARAHIDROXIMANDELICO ASI OBTENIDO CON HIDROXIDO SODICO EN DISOLUCION ACUOSA. LA REACCION DEL ACIDO GLIOXILICO CON EL FENOL SE EFECTUA A UNA TEMPERATURA COMPRENDIDA ENTRE 15 Y 80 (GRADOS) C.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8814575A FR2638740B1 (fr) | 1988-11-08 | 1988-11-08 | Nouveau procede de fabrication industrielle du parahydroxymandelate de sodium |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2033117T3 true ES2033117T3 (es) | 1993-03-01 |
Family
ID=9371685
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES198989402790T Expired - Lifetime ES2033117T3 (es) | 1988-11-08 | 1989-10-10 | Nuevo procedimiento de fabricacion industrial del parahidroximandelato sodico. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4978784A (es) |
| EP (1) | EP0368696B1 (es) |
| JP (1) | JP2789045B2 (es) |
| AT (1) | ATE77618T1 (es) |
| CA (1) | CA2002139A1 (es) |
| DE (1) | DE68901913T2 (es) |
| ES (1) | ES2033117T3 (es) |
| FR (1) | FR2638740B1 (es) |
| GR (1) | GR3005026T3 (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2687143B1 (fr) * | 1992-02-12 | 1995-06-23 | Hoechst France | Procede d'obtention de l'acide orthohydroxymandelique et de ses sels. |
| FR2705669B1 (fr) * | 1993-05-28 | 1995-08-25 | Hoechst France | Procédé de préparation d'acides hydroxyphénylacétiques. |
| FR2760745B1 (fr) * | 1997-03-11 | 1999-05-28 | Hoechst France | Procede industriel de preparation en continu de l'orthohydroxymandelate de sodium |
| NL1010090C2 (nl) * | 1998-09-15 | 2000-03-17 | Gerard Kessels Sociedad Anonim | Werkwijze voor de bereiding van 2- en 4-hydroxyamandelzuur. |
| FR2901553B1 (fr) | 2006-05-24 | 2011-08-26 | Clariant Specialty Fine Chem F | Complexes metalliques comprenant un ligand derive d'acide 2-aryl-2-hydroxyacetique et un cation metallique divalent ou trivalent, et leur utilisation |
| FR3013351B1 (fr) * | 2013-11-15 | 2016-01-01 | Rhodia Operations | Procede de preparation de compose aromatique mandelique et de compose aldehyde aromatique |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6023659B2 (ja) * | 1977-10-20 | 1985-06-08 | 宇部興産株式会社 | ヒドロキシモノマンデル酸化合物の製造法 |
| FR2427322A1 (fr) * | 1979-06-15 | 1979-12-28 | Hoechst France | Parahydroxymandelate de sodium racemique cristallise, son procede de preparation et son application a la preparation du paraformylphenolate de sodium cristallise |
| ATE3408T1 (de) * | 1979-08-09 | 1983-06-15 | Beecham Group Plc | Verfahren zur abscheidung eines festen salzes der p-hydroxymandelsaeure; einige salze der phydroxymandels[ure. |
| JPS5668641A (en) * | 1979-11-07 | 1981-06-09 | Nippon Synthetic Chem Ind Co Ltd:The | Preparation of hydroxymandelic acids |
| JPS55102537A (en) * | 1980-01-16 | 1980-08-05 | Nippon Synthetic Chem Ind Co Ltd:The | Preparation of 4-hydroxymandelic acid |
-
1988
- 1988-11-08 FR FR8814575A patent/FR2638740B1/fr not_active Expired - Lifetime
-
1989
- 1989-10-10 AT AT89402790T patent/ATE77618T1/de not_active IP Right Cessation
- 1989-10-10 EP EP89402790A patent/EP0368696B1/fr not_active Expired - Lifetime
- 1989-10-10 ES ES198989402790T patent/ES2033117T3/es not_active Expired - Lifetime
- 1989-10-10 DE DE8989402790T patent/DE68901913T2/de not_active Expired - Lifetime
- 1989-10-25 US US07/426,352 patent/US4978784A/en not_active Expired - Lifetime
- 1989-11-01 JP JP1286017A patent/JP2789045B2/ja not_active Expired - Lifetime
- 1989-11-02 CA CA002002139A patent/CA2002139A1/en not_active Abandoned
-
1992
- 1992-06-25 GR GR920401220T patent/GR3005026T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0368696B1 (fr) | 1992-06-24 |
| US4978784A (en) | 1990-12-18 |
| FR2638740B1 (fr) | 1991-07-12 |
| JP2789045B2 (ja) | 1998-08-20 |
| EP0368696A1 (fr) | 1990-05-16 |
| CA2002139A1 (en) | 1990-05-08 |
| JPH02178251A (ja) | 1990-07-11 |
| DE68901913T2 (de) | 1992-12-17 |
| DE68901913D1 (de) | 1992-07-30 |
| GR3005026T3 (es) | 1993-05-24 |
| ATE77618T1 (de) | 1992-07-15 |
| FR2638740A1 (fr) | 1990-05-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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