[go: up one dir, main page]

AR083111A1 - Proceso para producir carbonato de litio a partir de salmuera de litio concentrada - Google Patents

Proceso para producir carbonato de litio a partir de salmuera de litio concentrada

Info

Publication number
AR083111A1
AR083111A1 ARP110103514A ARP110103514A AR083111A1 AR 083111 A1 AR083111 A1 AR 083111A1 AR P110103514 A ARP110103514 A AR P110103514A AR P110103514 A ARP110103514 A AR P110103514A AR 083111 A1 AR083111 A1 AR 083111A1
Authority
AR
Argentina
Prior art keywords
lithium
concentrated
lithium carbonate
carbonate
precipitated
Prior art date
Application number
ARP110103514A
Other languages
English (en)
Original Assignee
Orocobre Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Orocobre Ltd filed Critical Orocobre Ltd
Publication of AR083111A1 publication Critical patent/AR083111A1/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/08—Carbonates; Bicarbonates
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

Se revelan métodos para un proceso simplificado para preparar carbonato de litio a partir de salmuera de litio concentrada que puede utilizarse para aplicaciones de calidad para baterías, usos farmacéuticos y otras aplicaciones que requieren una calidad de gran pureza. Se precipita carbonato de litio a partir de salmuera concentrada en litio, mediante la adición de cenizas de soda, preferentemente con un contenido reducido en magnesio, subsiguientemente se suspende en solución acuosa y se hace reaccionar con dióxido de carbono de manera de formar bicarbonato de litio disuelto. Se filtran las impurezas insolubles, y el boro y las impurezas metálicas disueltas tales como calcio, magnesio y hierro son separados físicamente de la solución de bicarbonato de litio mediante medios selectivos de iones o mediante otros procesos selectivos. Subsiguientemente, se precipita el carbonato de litio.
ARP110103514A 2011-09-15 2011-09-26 Proceso para producir carbonato de litio a partir de salmuera de litio concentrada AR083111A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/AU2011/001189 WO2013036983A1 (en) 2011-09-15 2011-09-15 Process for producing lithium carbonate from concentrated lithium brine

Publications (1)

Publication Number Publication Date
AR083111A1 true AR083111A1 (es) 2013-01-30

Family

ID=47882433

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP110103514A AR083111A1 (es) 2011-09-15 2011-09-26 Proceso para producir carbonato de litio a partir de salmuera de litio concentrada

Country Status (6)

Country Link
US (2) US9994930B2 (es)
CN (1) CN103958412A (es)
AR (1) AR083111A1 (es)
AU (1) AU2011376865A1 (es)
HK (1) HK1200158A1 (es)
WO (1) WO2013036983A1 (es)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114538482A (zh) * 2022-03-10 2022-05-27 中国科学院过程工程研究所 一种吸附-加压脱附法提纯含锂溶液制备碳酸锂的方法

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI124088B (fi) * 2012-06-05 2014-03-14 Outotec Oyj Menetelmä ja laitteisto puhtaan litiumpitoisen liuoksen valmistamiseksi
BR102013023697B1 (pt) * 2013-09-16 2019-09-10 Vale Sa processo utilizado para a produção de carbonato de lítio, a partir de uma salmoura rica em ca e mg
FI127782B (en) * 2014-12-02 2019-02-15 Keliber Oy Process for the production of lithium metal phosphate
CN105836766A (zh) * 2016-03-18 2016-08-10 中国科学院青海盐湖研究所 一种脱除高锂溶液中的硼离子的方法
JP6970368B2 (ja) * 2016-06-07 2021-11-24 住友金属鉱山株式会社 リチウム化合物粉体、このリチウム化合物粉体の製造方法、および非水系電解質二次電池用正極活物質の製造方法
CN109715288B (zh) * 2016-08-18 2022-06-17 爱克斯司博申公司 从盐水中提取金属离子
US10315926B2 (en) * 2017-02-09 2019-06-11 U.S. Department Of Energy Selective lithium recovery as lithium carbonate from natural brines
CN110997568A (zh) * 2017-08-02 2020-04-10 捷客斯金属株式会社 锂化合物的溶解方法及碳酸锂的制造方法、以及由锂离子二次电池废料回收锂的方法
CN107445181B (zh) * 2017-08-16 2022-12-23 中国恩菲工程技术有限公司 碳酸锂连续碳酸氢化反应的系统
US11229880B2 (en) * 2017-10-26 2022-01-25 International Battery Metals, Ltd. Modular extraction apparatus
HRP20241474T1 (hr) * 2017-11-09 2025-01-03 U.S. Borax, Inc. Postupak dobivanja minerala
EP3759257A4 (en) * 2018-02-28 2021-11-24 Lilac Solutions, Inc. ION EXCHANGE REACTOR WITH PARTICLE TRAPS FOR LITHIUM EXTRACTION
AU2019352457B2 (en) * 2018-10-01 2025-04-17 Reed Advanced Materials Pty Ltd Processing of lithium containing brines
FR3087356B1 (fr) * 2018-10-18 2021-04-23 Geolith Installation et procede de separation d’au moins une espece ionique a partir d’une solution comprenant au moins ladite espece ionique et du lithium
CN109244588B (zh) * 2018-11-22 2022-08-23 湖南天泰天润新能源科技有限公司 一种废三元锂电池生产三元前驱体和高纯碳酸锂的方法
FI3898517T3 (fi) * 2018-12-20 2023-09-05 Lanxess Deutschland Gmbh Erittäin puhtaan litiumkarbonaatin valmistus suolaliuoksista
CA3124281C (en) 2018-12-21 2023-08-22 Mangrove Water Technologies Ltd. Li recovery processes and onsite chemical production for li recovery processes
EP3670686A1 (en) * 2018-12-21 2020-06-24 A.C.N. 630 589 507 Pty Ltd Battery recycling process
US11708279B2 (en) 2019-08-12 2023-07-25 Energy, United States Department Of Selective material recovery from solution
US11634789B2 (en) 2019-09-16 2023-04-25 InCoR Lithium Selective lithium extraction from brines
CN110550643A (zh) * 2019-09-30 2019-12-10 山东瑞福锂业有限公司 从析钠母液中回收制备电池级锂盐的工艺
TR201915707A2 (tr) 2019-10-11 2021-04-21 Eti Maden Isletmeleri Genel Mueduerluegue Boraks zayif çözelti̇leri̇nden li̇tyum geri̇ kazanimi
CN111122548A (zh) * 2020-01-06 2020-05-08 江苏容汇通用锂业股份有限公司 一种碳酸锂中微量金属铜、锌的检测方法
CN111589278B (zh) * 2020-04-27 2022-03-22 湖南凯地众能科技有限公司 一种回收废旧锂离子电池水循环利用系统及其方法
CN113924375B (zh) * 2020-05-12 2023-04-04 能源探索技术有限公司 用于从盐水中回收锂的系统和方法
CN111960445B (zh) * 2020-08-31 2023-04-07 长沙有色冶金设计研究院有限公司 一种采用硫酸锂粗矿制备电池级碳酸锂并回收副产物的方法
CN111943237B (zh) * 2020-08-31 2023-05-02 长沙有色冶金设计研究院有限公司 一种采用硫酸锂粗矿制备电池级碳酸锂的方法
US20240101438A1 (en) * 2020-10-27 2024-03-28 Galaxy Resources Limited Recovery of lithium from aqueous solutions
CN112151903B (zh) * 2020-11-26 2021-03-09 清华四川能源互联网研究院 一种锂电池报废正极材料回收过程中的除杂和处理方法
CA3200159A1 (en) * 2020-12-02 2022-06-09 Amit PATWARDHAN A lithium carbonate production process and apparatus
CN112717468A (zh) * 2020-12-09 2021-04-30 西安蓝晓科技新材料股份有限公司 一种用于沉锂母液中锂回收的方法
US11931701B2 (en) 2021-08-06 2024-03-19 Lithium Ark Holding B.V. Production of lithium hydroxide and lithium carbonate
CN113636577A (zh) * 2021-08-25 2021-11-12 金川集团股份有限公司 一种低磁性球形高纯碳酸锂制备方法
CN115159549A (zh) * 2022-06-20 2022-10-11 广东邦普循环科技有限公司 一种苛化法制备氢氧化锂的工艺及其应用
US20240068070A1 (en) * 2022-08-23 2024-02-29 Clean Energy Systems, Inc. Lithium extraction with an oxy-fuel combustor
GB202216132D0 (en) * 2022-10-31 2022-12-14 Mexichem Uk Ltd Process
CN116183325A (zh) * 2022-12-30 2023-05-30 南通瑞翔新材料有限公司 一种溶解碳酸锂固体测试可磁化颗粒数的装置
US20240293779A1 (en) * 2023-03-03 2024-09-05 Board Of Regents, The University Of Texas System Chlor-alkali electrodialysis for lithium extration from geothermal fluids
CN116395720B (zh) * 2023-03-24 2025-08-05 浙江工业大学 一种碳化法提纯工业Li2CO3过程中连续流碳化反应制备纯Li2CO3的工艺及装置
WO2025181142A1 (de) 2024-02-29 2025-09-04 Lanxess Deutschland Gmbh Herstellung von calciumreduziertem lithiumcarbonat
US12258830B1 (en) 2024-06-02 2025-03-25 National Energy Services Reunited Corporation Degradable delivery devices to facilitate dissolution of degradable downhole tools

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1065179B (de) * 1955-02-07 1959-09-10 Rohm &. Haas Company, Philadelphia, Pa. (V. St. A.) Verfahren zur Herstellung harzartiger Produkte
GB876580A (en) * 1958-08-11 1961-09-06 Dept Of Mines Improvements in or relating to the treatment of spodumene
GB1576130A (en) * 1976-08-10 1980-10-01 Quebec Ministere Des Richesses Continuous production of lithium carbonate
US5219550A (en) 1989-03-31 1993-06-15 Cyprus Foote Mineral Company Production of low boron lithium carbonate from lithium-containing brine
SE506154C2 (sv) 1995-10-13 1997-11-17 Asea Brown Boveri Förfarande och anordning för induktiv mätning av mått och läge hos objekt av elektriskt ledande material
AR001917A1 (es) 1996-03-28 1997-12-10 Minera Salar De Atacama S A So Producción de carbonato de litio de alta pureza desde salmueras naturales o industriales
US6048507A (en) * 1997-12-09 2000-04-11 Limtech Process for the purification of lithium carbonate
US6143260A (en) 1998-07-16 2000-11-07 Chemetall Foote Corporation Method for removing magnesium from brine to yield lithium carbonate
US7157065B2 (en) 1998-07-16 2007-01-02 Chemetall Foote Corporation Production of lithium compounds directly from lithium containing brines
AU2006235251B2 (en) 2005-04-08 2010-08-19 Dow Global Technologies Inc. Alkaline regeneration of N-Methyl-D-glucamine functional resins
CN101177288B (zh) * 2007-10-30 2010-08-11 中国科学院青海盐湖研究所 一种利用盐湖锂资源制取高纯碳酸锂的工艺方法
US8641992B2 (en) 2008-07-18 2014-02-04 Ady Resources Limited Process for recovering lithium from a brine
FI121785B (fi) 2009-03-11 2011-04-15 Outotec Oyj Menetelmä litiumbikarbonaatin puhdistamiseksi
AU2010341402B2 (en) * 2010-01-07 2014-01-30 Tianqi Lithium Corporation Process for the production of lithium carbonate
ES3048283T3 (en) 2010-02-17 2025-12-09 Terralithium Llc Processes for preparing highly pure lithium carbonate
CN101948124B (zh) * 2010-09-09 2012-09-19 江西赣锋锂业股份有限公司 一种从锂辉石中提取锂盐的方法
US20120263637A1 (en) * 2011-04-15 2012-10-18 Emc Metals Corporation System and Method For Recovering Boron Values From Plant Tailings

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114538482A (zh) * 2022-03-10 2022-05-27 中国科学院过程工程研究所 一种吸附-加压脱附法提纯含锂溶液制备碳酸锂的方法
CN114538482B (zh) * 2022-03-10 2023-08-01 中国科学院过程工程研究所 一种吸附-加压脱附法提纯含锂溶液制备碳酸锂的方法

Also Published As

Publication number Publication date
HK1200158A1 (en) 2015-07-31
AU2011376865A1 (en) 2013-05-02
US9994930B2 (en) 2018-06-12
CN103958412A (zh) 2014-07-30
US20140334997A1 (en) 2014-11-13
WO2013036983A1 (en) 2013-03-21
US20180320247A1 (en) 2018-11-08

Similar Documents

Publication Publication Date Title
AR083111A1 (es) Proceso para producir carbonato de litio a partir de salmuera de litio concentrada
CL2020002454A1 (es) Método para producir hidróxido de litio monohidratado a partir de salmueras
CL2015003511A1 (es) Proceso para preparar carbonato de litio, con las etapas de preparar una salmuera al 6 de litio, agregar kcl, eliminar boro, agregar licor madre, agregar cao y na2co3, precipitar carbonato de litio, filtrar, introducir co2 a una suspensión para producir bicarbonato litio, filtrar y precipitar litio divisional 2012-79.
EA201491632A1 (ru) Способ извлечения карбоната лития
MX390629B (es) Procesamiento de material que contiene litio que incluye aspersión de ácido clorhídrico.
AR089026A1 (es) Metodo para la produccion de carbonato de litio
AR108604A1 (es) Método para preparar hidróxido de litio y carbonato de litio directamente a partir de salmuera de salar con alta proporción de magnesio-litio
MX2017005919A (es) Produccion de hidroxido de litio.
MY163075A (en) Processing of lithium containing ore
CL2012002274A1 (es) Metodo de produccion de carbonato de litio de elevada pureza que comprende hacer reaccionar carbonato de litio grado tecnico con co2; metodo para producir hexafluorofosfato de litio muy puro; metodo para producir fluoruro de litio muy puro; metodo para producir dioxido de manganeso litio; y otros metodos.
GB2572295A (en) A process for the production of potassium sulphate and magnesium sulphate from carnallite and sodium sulphate
PH12015500642A1 (en) Process and system for producing sodium chloride brine
MY160811A (en) Device and method for extracting and separating sodium and potassium
PH12014501373A1 (en) Operating method in hydrometallurgy of nickel oxide ore
AR086547A1 (es) Procedimiento de produccion de una solucion de litio a partir de una salmuera
UA113204C2 (xx) Селективна екстракція хлориду калію з відхідного шенітового розчину з використанням тартратної кислоти як безпечного м'якого екстрагента, придатного до рециркуляції
PE20140395A1 (es) Tratamiento del agua
MX337503B (es) Proceso para la produccion conjunta de carbonato de sodio y bicarbonato de sodio.
TR201202944A2 (tr) Sodyum bikarbonat üretimi için işlem.
RU2013116667A (ru) Способ комплексной переработки природных рассолов хлоридного кальциево-магниевого типа
AU2012297573A8 (en) Method for the recovery of magnesium sulphate and production of magnesium oxide
RU2010145271A (ru) Способ получения бромистого кальция из природных бромсодержащих рассолов хлоридного кальциевого типа
RS20250281A9 (sr) Postupak i uređaj za pripremu litijum hlorida visoke čistoće na osnovu litijum-jonskog čvrstog elektrolita
UA82330U (ru) Способ получения калимагнезии и бишофита из растворов хлоридно-сульфатного типа
UA61376U (ru) Способ получения соды, гипса, соляной кислоты способ бена

Legal Events

Date Code Title Description
FG Grant, registration