AR057211A1 - Procedimiento para la preparacion de sulfonamidas - Google Patents
Procedimiento para la preparacion de sulfonamidasInfo
- Publication number
- AR057211A1 AR057211A1 ARP060105297A ARP060105297A AR057211A1 AR 057211 A1 AR057211 A1 AR 057211A1 AR P060105297 A ARP060105297 A AR P060105297A AR P060105297 A ARP060105297 A AR P060105297A AR 057211 A1 AR057211 A1 AR 057211A1
- Authority
- AR
- Argentina
- Prior art keywords
- equivalents
- base
- aminosulfone
- variables
- preparation
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- NVBFHJWHLNUMCV-UHFFFAOYSA-N sulfamide Chemical class NS(N)(=O)=O NVBFHJWHLNUMCV-UHFFFAOYSA-N 0.000 abstract 7
- NXTNASSYJUXJDV-UHFFFAOYSA-N 3-nitrobenzoyl chloride Chemical class [O-][N+](=O)C1=CC=CC(C(Cl)=O)=C1 NXTNASSYJUXJDV-UHFFFAOYSA-N 0.000 abstract 3
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 abstract 1
- 125000006272 (C3-C7) cycloalkyl group Chemical group 0.000 abstract 1
- 125000003342 alkenyl group Chemical group 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000000304 alkynyl group Chemical group 0.000 abstract 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 abstract 1
- 125000004093 cyano group Chemical group *C#N 0.000 abstract 1
- 125000000392 cycloalkenyl group Chemical group 0.000 abstract 1
- 125000004438 haloalkoxy group Chemical group 0.000 abstract 1
- 125000001188 haloalkyl group Chemical group 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical class 0.000 abstract 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 abstract 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 229940124530 sulfonamide Drugs 0.000 abstract 1
- 150000003456 sulfonamides Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/38—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reaction of ammonia or amines with sulfonic acids, or with esters, anhydrides, or halides thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/16—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/13—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups
- C07C205/20—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups having nitro groups and hydroxy groups bound to carbon atoms of six-membered aromatic rings
- C07C205/21—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups having nitro groups and hydroxy groups bound to carbon atoms of six-membered aromatic rings having nitro groups and hydroxy groups bound to carbon atoms of the same non-condensed six-membered aromatic ring
- C07C205/22—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups having nitro groups and hydroxy groups bound to carbon atoms of six-membered aromatic rings having nitro groups and hydroxy groups bound to carbon atoms of the same non-condensed six-membered aromatic ring having one nitro groups bound to the ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
Abstract
Reivindicacion 1: Procedimiento para la preparacion de sulfonamidas (1) en las que las variables tienen los siguientes significados: R1, R2, R3 y 4 H, halogeno, ciano, nitro, alquilo C1-6, halogenoalquilo C1-6, alcoxi C1-6 o halogenoalcoxi C1-6; R5 y R6 H, alquilo C1-6, alquenilo C3-6, alquinilo C36, cicloalquilo C3-7, cicloalquenilo C3-7, alcoxi C1-6, fenilo o bencilo; por reaccion de cloruros de ácido m-nitrobenzoico (2) en los que las variables R1, R2, R3 y R4 tienen los significados nombrados anteriormente, con aminosulfonas (3) H2N-SO2NR5R6 en las que las variables R5 y R6 tienen los significados nombrados anteriormente; con la influencia de B equivalentes de la base IV, caracterizado porque en el paso a) se hace reaccionar la aminosulfona (3) con B1 equivalentes de la base IV, y en el paso b) se hace reaccionar la mezcla de reaccion resultante del paso a) con cloruro de ácido m-nitrobenzoico (2) y B2 equivalentes de la base IV; en el que B representa de 1,5 a 3 equivalentes de la base IV, respecto a la aminosulfona (3), B1 representa una cantidad parcial de B y se encuentra en 0,1 a 1,3 equivalentes de la base IV, respecto a la aminosulfona (3); y B2 representa una cantidad parcial de B y es la diferencia entre B y B1.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE200510057681 DE102005057681A1 (de) | 2005-12-01 | 2005-12-01 | Verfahren zur Herstellung fluorierter m-Nitro-Benzoesäurechloride |
| EP06123569 | 2006-11-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR057211A1 true AR057211A1 (es) | 2007-11-21 |
Family
ID=37697933
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP060105297A AR057211A1 (es) | 2005-12-01 | 2006-11-30 | Procedimiento para la preparacion de sulfonamidas |
Country Status (11)
| Country | Link |
|---|---|
| US (2) | US8263806B2 (es) |
| EP (1) | EP1957443A2 (es) |
| JP (1) | JP5555426B2 (es) |
| KR (3) | KR101422433B1 (es) |
| AR (1) | AR057211A1 (es) |
| AU (1) | AU2006319263B2 (es) |
| BR (1) | BRPI0619760A2 (es) |
| CA (3) | CA2821517A1 (es) |
| EA (2) | EA201100377A1 (es) |
| IL (3) | IL191503A (es) |
| WO (1) | WO2007063028A2 (es) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007063028A2 (de) * | 2005-12-01 | 2007-06-07 | Basf Se | Verfahren zur herstellung von sulfonamiden |
| BRPI0818408B1 (pt) * | 2007-10-12 | 2024-01-09 | Basf Se | Processos para preparar diamidas sulfúricas e ingredientes herbicidas ativos |
| WO2019020501A1 (en) | 2017-07-28 | 2019-01-31 | Basf Se | Preparation of substituted 3-aryl-5-trifluoromethyl-1,2,4-oxadiazoles |
| EP3587396A1 (en) * | 2018-06-27 | 2020-01-01 | Basf Se | A method of isolating a n-(3-nitrobenzoyl)sulfamide |
| CN111499506B (zh) * | 2020-03-23 | 2021-03-30 | 浙江本立科技股份有限公司 | 一种2,4-二氯-5-氟苯甲酰氯绿色生产工艺 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1240853B (de) | 1962-12-06 | 1967-05-24 | Smith Kline French Lab | Verfahren zur Herstellung von Sulfurylamiden |
| US3198785A (en) * | 1964-04-17 | 1965-08-03 | Sandoz Ag | Sulfamoyl azabicyclononanes and derivatives thereof |
| NL175521C (nl) * | 1973-04-26 | 1984-11-16 | Hoechst Ag | Werkwijze voor het bereiden van carbonzuurchloriden. |
| DE2933148A1 (de) * | 1979-08-16 | 1981-02-26 | Bayer Ag | Verfahren zur herstellung von aromatischen dicarbonsaeuredichloriden iv |
| DE3040295A1 (de) * | 1980-10-25 | 1982-06-03 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von aromatischen carbonsaeurechloriden |
| JPS61155350A (ja) * | 1984-12-28 | 1986-07-15 | Ihara Nikkei Kagaku Kogyo Kk | 脂肪酸クロライド及び芳香族酸クロライドの製造方法 |
| JPH02501309A (ja) * | 1987-06-19 | 1990-05-10 | チバ ― ガイギー アクチエンゲゼルシャフト | 複素環化合物 |
| BR8807217A (pt) | 1987-09-23 | 1989-10-17 | Hoffmann La Roche | Compostos heterocilicos |
| DE3812175A1 (de) * | 1988-04-13 | 1989-10-26 | Bayer Ag | Verfahren zur herstellung von carbonsaeurehalogeniden |
| US5238908A (en) * | 1989-08-31 | 1993-08-24 | Rohm And Haas Company | Herbicidal glutaramic acids and derivatives |
| JPH04117344A (ja) * | 1990-09-05 | 1992-04-17 | Res Assoc Util Of Light Oil | 芳香族カルボン酸塩化物の製造方法 |
| AU7782694A (en) * | 1993-09-28 | 1995-04-18 | Ciba-Geigy Ag | Acylated sulphonamides as insecticides and acaricides |
| DE19958758A1 (de) * | 1999-12-07 | 2001-07-05 | Basf Ag | Verfahren zur Herstellung von o-Chlormethylbenzoesäurechloriden |
| US7034181B1 (en) * | 1999-12-07 | 2006-04-25 | Basf Aktiengesellschaft | Method for producing o-chloromethyl benzoic acid chlorides |
| JP2001187762A (ja) * | 1999-12-28 | 2001-07-10 | Nippon Light Metal Co Ltd | 高純度芳香族酸クロライドの製造方法 |
| IL150420A0 (en) * | 1999-12-28 | 2002-12-01 | Pharmacopeia Inc | Pyrimidine and triazine kinase inhibitors |
| EP1274708A1 (en) * | 2000-04-17 | 2003-01-15 | Basf Aktiengesellschaft | Herbicidal 3-heterocyclic substituted benzisothiazole and benzisoxazole compounds |
| US6251829B1 (en) * | 2000-04-18 | 2001-06-26 | Rohm And Haas Company | Herbicidal benzoyloxy carboxylates and carboxamides |
| DK1226127T3 (da) | 2000-05-04 | 2009-10-19 | Basf Se | Substituerede phenylsulfamoylcarboxamider |
| JP2004535446A (ja) * | 2001-06-26 | 2004-11-25 | ブリストル−マイヤーズ スクイブ カンパニー | ＴＮＦ−α発現のＮ−ヘテロ環阻害剤 |
| CA2448737C (en) * | 2001-07-20 | 2010-06-01 | Boehringer Ingelheim (Canada) Ltd. | Viral polymerase inhibitors |
| JP4384028B2 (ja) * | 2002-05-16 | 2009-12-16 | ビーエーエスエフ ソシエタス・ヨーロピア | スルファミン酸ハロゲン化物の製造方法 |
| AU2003301443A1 (en) | 2002-10-18 | 2004-05-04 | E.I. Du Pont De Nemours And Company | Azolecarboxamide herbicides |
| BR0315932A (pt) * | 2002-10-30 | 2005-09-13 | Basf Ag | Processo para a preparação de iso (tio) cianatos de fenila, composto, e, processo para a preparação do mesmo |
| WO2004106324A1 (en) | 2003-05-27 | 2004-12-09 | E.I. Dupont De Nemours And Company | Azolecarboxamide herbicides |
| ES2465499T3 (es) * | 2004-07-22 | 2014-06-05 | Basf Se | Procedimiento para la preparación de 3-fenil(tio)uracilos y -ditiouracilos |
| ITMI20050275A1 (it) * | 2005-02-22 | 2006-08-23 | Miteni Spa | Procedimento per la preparazione di derivati dell'acido benzoico attraverso un nuovo intermedio di sintesi |
| WO2007063028A2 (de) | 2005-12-01 | 2007-06-07 | Basf Se | Verfahren zur herstellung von sulfonamiden |
| BRPI0818408B1 (pt) * | 2007-10-12 | 2024-01-09 | Basf Se | Processos para preparar diamidas sulfúricas e ingredientes herbicidas ativos |
-
2006
- 2006-11-23 WO PCT/EP2006/068832 patent/WO2007063028A2/de not_active Ceased
- 2006-11-23 US US12/095,582 patent/US8263806B2/en not_active Expired - Fee Related
- 2006-11-23 CA CA2821517A patent/CA2821517A1/en not_active Abandoned
- 2006-11-23 AU AU2006319263A patent/AU2006319263B2/en not_active Ceased
- 2006-11-23 KR KR1020137020659A patent/KR101422433B1/ko not_active Expired - Fee Related
- 2006-11-23 EA EA201100377A patent/EA201100377A1/ru unknown
- 2006-11-23 CA CA2821516A patent/CA2821516A1/en not_active Abandoned
- 2006-11-23 EA EA200801432A patent/EA200801432A1/ru unknown
- 2006-11-23 JP JP2008542731A patent/JP5555426B2/ja not_active Expired - Fee Related
- 2006-11-23 KR KR1020137020660A patent/KR101422434B1/ko not_active Expired - Fee Related
- 2006-11-23 EP EP06830101A patent/EP1957443A2/de not_active Withdrawn
- 2006-11-23 KR KR1020087015883A patent/KR101430949B1/ko not_active Expired - Fee Related
- 2006-11-23 BR BRPI0619760-4A patent/BRPI0619760A2/pt not_active Application Discontinuation
- 2006-11-23 CA CA002631113A patent/CA2631113A1/en not_active Abandoned
- 2006-11-30 AR ARP060105297A patent/AR057211A1/es not_active Application Discontinuation
-
2008
- 2008-05-15 IL IL191503A patent/IL191503A/en not_active IP Right Cessation
-
2011
- 2011-09-21 IL IL215279A patent/IL215279A0/en unknown
- 2011-09-21 IL IL215280A patent/IL215280A0/en unknown
-
2012
- 2012-08-13 US US13/584,213 patent/US20120310010A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| AU2006319263B2 (en) | 2012-06-28 |
| IL191503A (en) | 2014-09-30 |
| KR101422433B1 (ko) | 2014-07-22 |
| CA2821516A1 (en) | 2007-06-07 |
| BRPI0619760A2 (pt) | 2012-02-22 |
| WO2007063028A3 (de) | 2007-08-23 |
| IL215280A0 (en) | 2011-10-31 |
| KR101430949B1 (ko) | 2014-08-18 |
| CA2631113A1 (en) | 2007-06-07 |
| JP5555426B2 (ja) | 2014-07-23 |
| EA200801432A1 (ru) | 2008-12-30 |
| KR20080072093A (ko) | 2008-08-05 |
| WO2007063028A2 (de) | 2007-06-07 |
| EP1957443A2 (de) | 2008-08-20 |
| US8263806B2 (en) | 2012-09-11 |
| IL215279A0 (en) | 2011-10-31 |
| KR20130093696A (ko) | 2013-08-22 |
| US20100228054A1 (en) | 2010-09-09 |
| KR101422434B1 (ko) | 2014-07-22 |
| JP2009517440A (ja) | 2009-04-30 |
| US20120310010A1 (en) | 2012-12-06 |
| CA2821517A1 (en) | 2007-06-07 |
| AU2006319263A1 (en) | 2007-06-07 |
| KR20130093695A (ko) | 2013-08-22 |
| EA201100377A1 (ru) | 2011-08-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant, registration | ||
| FD | Application declared void or lapsed, e.g., due to non-payment of fee |