MX9301069A - Proceso para la recuperacion de 6-aminocapronitrilo. - Google Patents
Proceso para la recuperacion de 6-aminocapronitrilo.Info
- Publication number
- MX9301069A MX9301069A MX9301069A MX9301069A MX9301069A MX 9301069 A MX9301069 A MX 9301069A MX 9301069 A MX9301069 A MX 9301069A MX 9301069 A MX9301069 A MX 9301069A MX 9301069 A MX9301069 A MX 9301069A
- Authority
- MX
- Mexico
- Prior art keywords
- aminocapronitrile
- tha
- compound
- recovery
- present
- Prior art date
Links
- KBMSFJFLSXLIDJ-UHFFFAOYSA-N 6-aminohexanenitrile Chemical compound NCCCCCC#N KBMSFJFLSXLIDJ-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title 1
- 238000011084 recovery Methods 0.000 title 1
- 150000001875 compounds Chemical class 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 1
- 150000001728 carbonyl compounds Chemical class 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/32—Separation; Purification; Stabilisation; Use of additives
- C07C253/34—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La presente invención se refiere a la purificación de 6-aminocapronitrilo por calentamiento de una mezcla que contiene éste compuesto y THA, y conversión del THA a compuesto de alto punto de ebullición y posterior destilación del 6-aminocapronitrilo. El tiempo requerido para convertir el THA es reducido si un compuesto carbonil orgánico esta presente en la mezcla durante el calentamiento.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/841,351 US5162567A (en) | 1992-02-27 | 1992-02-27 | Purification of 6-aminocapronitrile |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX9301069A true MX9301069A (es) | 1993-08-01 |
Family
ID=25284651
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX9301069A MX9301069A (es) | 1992-02-27 | 1993-02-26 | Proceso para la recuperacion de 6-aminocapronitrilo. |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US5162567A (es) |
| EP (1) | EP0628025B1 (es) |
| JP (1) | JP3289903B2 (es) |
| KR (1) | KR100268689B1 (es) |
| BR (1) | BR9305994A (es) |
| CA (1) | CA2130915C (es) |
| DE (1) | DE69304514T2 (es) |
| ES (1) | ES2090982T3 (es) |
| MX (1) | MX9301069A (es) |
| WO (1) | WO1993016984A1 (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5312959A (en) * | 1993-07-12 | 1994-05-17 | E. I. Du Pont De Nemours And Company | Purification of 2-methylglutaronitrile or adiponitrile |
| DE19517823A1 (de) | 1995-05-18 | 1996-11-21 | Basf Ag | Verfahren zur Herstellung von Caprolactam |
| FR2735471B1 (fr) * | 1995-06-16 | 1997-08-22 | Rhone Poulenc Chimie | Procede de preparation de lactames |
| DE19704620A1 (de) | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronitril aus Mischungen, die 6-Aminocapronitril und ein Imin enthalten |
| DE19704614A1 (de) * | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennnung eines Imins aus einer Mischung enthaltend ein Amin und ein Imin |
| DE19704613A1 (de) | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronsäurenitril aus Mischungen, die 6-Aminocapronsäurenitril und ein Imin enthalten |
| DE19812427A1 (de) * | 1998-03-20 | 1999-09-23 | Basf Ag | Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat |
| US5961788A (en) * | 1998-10-09 | 1999-10-05 | E. I. Du Pont De Nemours And Company | Sequential distillation process for removing tetrahydroazepine from aminocapronitrile and/or hexamethylenediamine |
| DE10059716A1 (de) | 2000-11-30 | 2002-06-06 | Basf Ag | Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Amin und ein Nitril |
| US6637562B2 (en) | 2001-12-26 | 2003-10-28 | Luggage America, Inc. | Luggage with integrated cover |
| DE10223827A1 (de) * | 2002-05-28 | 2003-12-11 | Basf Ag | Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Aminonitril, ein Diamin, ein Dinitril oder deren Gemische |
| US6858728B2 (en) * | 2003-06-17 | 2005-02-22 | Invista North America S.A.R.L. | Method for making caprolactam from impure ACN in which THA is not removed until after caprolactam is produced |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA601619A (en) * | 1960-07-12 | H. Ottenheym Johannes | PROCESS FOR THE RECOVERY OF .omega.-AMINOCAPRONITRILE FROM MIXTURES OF .omega.-AMINOCAPRONITRILE,.omega.-CAPRONITRILE AND WATER | |
| US2242309A (en) * | 1938-03-23 | 1941-05-20 | Du Pont | Process for purifying nitriles |
| US3004059A (en) * | 1958-02-11 | 1961-10-10 | Degussa | Process for the recovery of omega-aminonitriles |
| NL258960A (es) * | 1959-12-15 | |||
| US4601859A (en) * | 1984-05-04 | 1986-07-22 | Allied Corporation | Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst |
-
1992
- 1992-02-27 US US07/841,351 patent/US5162567A/en not_active Expired - Lifetime
-
1993
- 1993-02-24 JP JP51495693A patent/JP3289903B2/ja not_active Expired - Fee Related
- 1993-02-24 BR BR9305994A patent/BR9305994A/pt not_active IP Right Cessation
- 1993-02-24 KR KR1019940702986A patent/KR100268689B1/ko not_active Expired - Fee Related
- 1993-02-24 DE DE69304514T patent/DE69304514T2/de not_active Expired - Fee Related
- 1993-02-24 EP EP93906065A patent/EP0628025B1/en not_active Expired - Lifetime
- 1993-02-24 CA CA002130915A patent/CA2130915C/en not_active Expired - Fee Related
- 1993-02-24 ES ES93906065T patent/ES2090982T3/es not_active Expired - Lifetime
- 1993-02-24 WO PCT/US1993/001460 patent/WO1993016984A1/en not_active Ceased
- 1993-02-26 MX MX9301069A patent/MX9301069A/es not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| US5162567A (en) | 1992-11-10 |
| KR950700238A (ko) | 1995-01-16 |
| BR9305994A (pt) | 1997-10-21 |
| EP0628025B1 (en) | 1996-09-04 |
| WO1993016984A1 (en) | 1993-09-02 |
| JP3289903B2 (ja) | 2002-06-10 |
| CA2130915A1 (en) | 1993-09-02 |
| DE69304514D1 (de) | 1996-10-10 |
| KR100268689B1 (ko) | 2000-10-16 |
| ES2090982T3 (es) | 1996-10-16 |
| EP0628025A1 (en) | 1994-12-14 |
| JPH07504415A (ja) | 1995-05-18 |
| DE69304514T2 (de) | 1997-03-27 |
| CA2130915C (en) | 2004-05-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| MX9301069A (es) | Proceso para la recuperacion de 6-aminocapronitrilo. | |
| ATE26167T1 (de) | Feuerzeug, insbesondere wegwerffeuerzeug. | |
| ES2091069T3 (es) | Procedimiento de purificacion de pentafluoroetano. | |
| ES2093494T3 (es) | Fracciones de heparina purificadas, procedimiento de obtencion y composiciones farmaceuticas que los contienen. | |
| MX166895B (es) | Procedimiento para purificar organofosfitos terciarios | |
| LU88719I2 (fr) | Nuflor solution injectable | |
| BR8804985A (pt) | Processo para recuperar trimetoxissilano a partir de uma mistura de trimetoxissilano e metanol,mistura esta capaz de formar um azeotropo | |
| ES2060428T3 (es) | Purificacion del 6-aminocapronitrilo. | |
| TW264460B (es) | ||
| ES2078657T3 (es) | Procedimiento criogenico para producir nitrogeno de pureza ultraelevada. | |
| DK0734392T3 (da) | Omdannelse af bisnoralkohol til bisnoraldehyd | |
| DK0571742T3 (da) | Fremgangmåde til fraskillelse af aminosyrer fra vandige opløsninger | |
| TW243452B (es) | ||
| MX9300017A (es) | Proceso para la recuperacion de 6-aminocapronitrilo a partir de una mezcla que contiene 6-aminocapronitrilo y tetrahidroazepina. | |
| ES2082433T3 (es) | Procedimiento para la obtencion de esteres de acidos hidroxifenilcarboxilicos. | |
| ES2139418T3 (es) | Procedimiento para la purificacion de dialdehido o-ftalico. | |
| MX9203877A (es) | Procedimiento para la amoxidacion de hidrocarburos saturados. | |
| NO960927L (no) | Fremgangsmåte ved fremstilling av 9-(2-hydroksy)-etoksymetylguanin | |
| AR246526A1 (es) | Procedimiento para preparar compuesto de macrolida y composicion que los incluye para combatir plagas excluida su aplicacion en animales y el hombre. | |
| DK0462673T3 (da) | Fremgangsmåde til fremstilling af benzinkomponenter | |
| GR3003562T3 (es) | ||
| BG104113A (en) | Method for the separation of hydroxyacetone from hydroxyaceton containing phenol | |
| DE69308934D1 (de) | Verfahren zur Herstellung von 1,1,1,2-Tetrafluorethan | |
| DE69306701D1 (de) | Verfahren zur Herstellung von Natriumhydrosulfit mit hohem Ausbringen | |
| JPS52108991A (en) | Purification of lactam |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration | ||
| MM | Annulment or lapse due to non-payment of fees |