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MX2019004519A - Sulfonacion de alcano libre de disolvente. - Google Patents

Sulfonacion de alcano libre de disolvente.

Info

Publication number
MX2019004519A
MX2019004519A MX2019004519A MX2019004519A MX2019004519A MX 2019004519 A MX2019004519 A MX 2019004519A MX 2019004519 A MX2019004519 A MX 2019004519A MX 2019004519 A MX2019004519 A MX 2019004519A MX 2019004519 A MX2019004519 A MX 2019004519A
Authority
MX
Mexico
Prior art keywords
solvent
sulfonation
alkane
free alkane
initiator
Prior art date
Application number
MX2019004519A
Other languages
English (en)
Inventor
Ott Timo
Biertümpel Ingo
Original Assignee
Grillo Werke Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Grillo Werke Ag filed Critical Grillo Werke Ag
Publication of MX2019004519A publication Critical patent/MX2019004519A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C409/00—Peroxy compounds
    • C07C409/42—Peroxy compounds containing sulfur atoms
    • C07C409/44—Peroxy compounds containing sulfur atoms with sulfur atoms directly bound to the —O—O— groups, e.g. persulfonic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C07C303/06—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/01—Sulfonic acids
    • C07C309/02—Sulfonic acids having sulfo groups bound to acyclic carbon atoms
    • C07C309/03—Sulfonic acids having sulfo groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C309/04—Sulfonic acids having sulfo groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton containing only one sulfo group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/42—Separation; Purification; Stabilisation; Use of additives
    • C07C303/44—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La presente invención se refiere a un procedimiento de sulfonación de alcano que usa alcano y trióxido de azufre, especialmente trióxido de azufre puro (100 %) en condiciones libres de disolvente en presencia de un iniciador. Se refiere además al uso de un precursor que forma "in situ" un iniciador para la fabricación de ácidos alcansulfónicos, especialmente ácidos metansulfónicos.
MX2019004519A 2016-11-28 2017-11-27 Sulfonacion de alcano libre de disolvente. MX2019004519A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16200928 2016-11-28
PCT/EP2017/080495 WO2018096138A1 (en) 2016-11-28 2017-11-27 Solvent-free alkane sulfonation

Publications (1)

Publication Number Publication Date
MX2019004519A true MX2019004519A (es) 2019-10-14

Family

ID=57442490

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019004519A MX2019004519A (es) 2016-11-28 2017-11-27 Sulfonacion de alcano libre de disolvente.

Country Status (13)

Country Link
US (1) US10961182B2 (es)
EP (1) EP3544954B1 (es)
JP (1) JP2019535774A (es)
KR (1) KR102300703B1 (es)
CN (1) CN110023281A (es)
AU (1) AU2017365556A1 (es)
BR (1) BR112019010643A2 (es)
ES (1) ES2965853T3 (es)
MX (1) MX2019004519A (es)
MY (1) MY191259A (es)
RU (1) RU2019120030A (es)
TW (1) TWI653219B (es)
WO (1) WO2018096138A1 (es)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20200115332A1 (en) * 2017-02-07 2020-04-16 Grillo-Werke Ag Method for the production of alkane sulfonic acids
CN110678444B (zh) * 2017-05-30 2023-01-10 巴斯夫欧洲公司 生产链烷磺酸的方法
CA3090041A1 (en) * 2018-02-07 2019-08-15 Basf Se Process for the manufacturing of alkanesulfonic acids
WO2020048965A1 (en) * 2018-09-04 2020-03-12 Basf Se Method for the production of alkane sulfonic acids
WO2020064573A1 (en) * 2018-09-25 2020-04-02 Basf Se Catalysts for the synthesis of alkanesulfonic acids
EP3856713B1 (en) * 2018-09-25 2022-11-09 Basf Se Cations as catalyst in the production of alkane sulfonic acids
WO2020115197A1 (en) * 2018-12-06 2020-06-11 Grillo-Werke Ag Method for the recycling or disposal of halocarbons
WO2020126855A1 (en) * 2018-12-21 2020-06-25 Basf Se Mixture comprising methanesulfonic acid and sulfuric acid
WO2020187893A1 (en) * 2019-03-21 2020-09-24 Basf Se Method for the production of alkane sulfonic acid at superacidic conditions
WO2020187902A1 (en) 2019-03-21 2020-09-24 Grillo-Werke Ag Method for the production of haloalkane sulfonic acid at non-super acidic conditions
WO2020187897A1 (en) 2019-03-21 2020-09-24 Basf Se Method for the production of alkane sulfonic acid at non-superacidic conditions
EP3712123B1 (en) * 2019-03-21 2022-05-11 Grillo-Werke AG Process for the preparation of isotope labelled alkane sulfonic acid
WO2020187894A1 (en) 2019-03-21 2020-09-24 Basf Se Method for the purification of alkanes
WO2020187901A1 (en) * 2019-03-21 2020-09-24 Grillo-Werke Ag Process for the preparation of haloalkanesulfonic acids from sulfur trioxide and a haloalkane at superacidic conditions
WO2020212299A1 (en) 2019-04-18 2020-10-22 Basf Se Process for the production of anhydrous methanesulfonic acid from methane and so3
DE112020003274T5 (de) * 2019-07-10 2022-06-23 Grillo-Werke Ag Verfahren zur Verringerung der SO3-Konzentration in einer Reaktionsmischung, die eine Sulfonsäure und SO3 enthält
MY207209A (en) 2019-08-07 2025-02-06 Basf Se Process for the production of alkanesulfonic acids
US12503429B2 (en) 2019-10-01 2025-12-23 Basf Se Process for manufacturing alkanesulfonic acids
WO2021063768A1 (en) * 2019-10-02 2021-04-08 Basf Se Process for manufacturing alkanesulfonic acids
CN111302978A (zh) * 2020-04-17 2020-06-19 凯瑞环保科技股份有限公司 一种烷基磺酸的合成装置及合成方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2493038A (en) 1946-05-31 1950-01-03 Houdry Process Corp Reaction of methane with sulfur trioxide
US2619507A (en) 1951-01-05 1952-11-25 Dow Chemical Co Di(methanesulfonyl) peroxide and its preparation
US4680095A (en) 1986-11-03 1987-07-14 Pennwalt Corporation Continuous preparation of dialkanesulfonyl peroxide
FR2610320A1 (fr) 1987-02-03 1988-08-05 Atochem Composes peroxydes renfermant l'isotope 17o
US4910335A (en) 1989-08-01 1990-03-20 Pennwalt Corporation Decolorization of alkanesulfonic and arenesulfonic acids
GB9023433D0 (en) * 1990-10-27 1990-12-12 Interox Chemicals Ltd Peroxoacid manufacture
EP1558353B1 (en) 2002-11-05 2016-06-15 Alan K. Richards Anhydrous conversion of methane and other light alkanes into methanol and other derivatives, using radical pathways and chain reactions with minimal waste products
CN1318361C (zh) * 2002-11-05 2007-05-30 艾伦·K·理查兹 使用自由基路线和链反应,在最小废物的情况下,使甲烷和其它轻质烷烃无水转化成甲醇和其它衍生物
US20080161591A1 (en) 2003-06-21 2008-07-03 Richards Alan K Anhydrous processing of methane into methane-sulfonic acid, methanol, and other compounds
US7282603B2 (en) * 2003-06-21 2007-10-16 Richards Alan K Anhydrous processing of methane into methane-sulfonic acid, methanol, and other compounds
US7119226B2 (en) 2004-04-20 2006-10-10 The Penn State Research Foundation Process for the conversion of methane
US20070282151A1 (en) 2006-05-19 2007-12-06 Richards Alan K Manufacture of higher hydrocarbons from methane, via methanesulfonic acid, sulfene, and other pathways
WO2015071365A1 (en) 2013-11-13 2015-05-21 Grillo Chemie Gmbh Process for preparing alkanesulfonic acids from sulfur trioxide and an alkane
WO2015071351A1 (en) 2013-11-13 2015-05-21 Grillo Chemie Gmbh Process for preparing bis(alkanesulfonyl peroxide)
WO2015071371A1 (en) 2013-11-13 2015-05-21 Grillo Chemie Gmbh Process for preparing bis(alkanesulfonyl) peroxide by oxidation
WO2015071455A1 (en) * 2013-11-18 2015-05-21 Grillo-Werke Ag Novel initiator for preparing alkanesulfonic acids from alkane and oleum

Also Published As

Publication number Publication date
EP3544954B1 (en) 2023-09-20
BR112019010643A2 (pt) 2019-10-01
MY191259A (en) 2022-06-11
KR102300703B1 (ko) 2021-09-09
RU2019120030A (ru) 2020-12-28
CA3041752A1 (en) 2018-05-31
EP3544954A1 (en) 2019-10-02
WO2018096138A1 (en) 2018-05-31
RU2019120030A3 (es) 2021-03-24
ES2965853T3 (es) 2024-04-17
KR20190072598A (ko) 2019-06-25
TWI653219B (zh) 2019-03-11
TW201829378A (zh) 2018-08-16
US10961182B2 (en) 2021-03-30
JP2019535774A (ja) 2019-12-12
AU2017365556A1 (en) 2019-05-02
US20190270701A1 (en) 2019-09-05
CN110023281A (zh) 2019-07-16

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