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MX2019000664A - Preparacion de 14-metil-16-oxabiciclo[10.3.1]pentadecenos de 3-metil-1,5 ciclopentadecanediona. - Google Patents

Preparacion de 14-metil-16-oxabiciclo[10.3.1]pentadecenos de 3-metil-1,5 ciclopentadecanediona.

Info

Publication number
MX2019000664A
MX2019000664A MX2019000664A MX2019000664A MX2019000664A MX 2019000664 A MX2019000664 A MX 2019000664A MX 2019000664 A MX2019000664 A MX 2019000664A MX 2019000664 A MX2019000664 A MX 2019000664A MX 2019000664 A MX2019000664 A MX 2019000664A
Authority
MX
Mexico
Prior art keywords
methyl
pentadecenos
oxabiciclo
cyclopentadecanediona
preparation
Prior art date
Application number
MX2019000664A
Other languages
English (en)
Other versions
MX385037B (es
Inventor
Bru Roig Miriam
Ruedenauer Stefan
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2019000664A publication Critical patent/MX2019000664A/es
Publication of MX385037B publication Critical patent/MX385037B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/64—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of functional groups containing oxygen only in singly bound form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/65—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups
    • C07C45/66—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups by dehydration
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/77—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D307/93—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom ortho- or peri-condensed with carbocyclic rings or ring systems condensed with a ring other than six-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Furan Compounds (AREA)
  • Fats And Perfumes (AREA)

Abstract

La presente invención se refiere a un método para preparar 14-metil-16-oxabiciclo[10.3.1]pentadecenos en una síntesis de dos etapas de 3-metil-1,5-ciclopentadecanediona como material de partida.
MX2019000664A 2016-07-15 2017-07-14 Preparacion de 14-metil-16-oxabiciclo[10.3.1]pentadecenos de 3-metil-1,5- ciclopentadecanediona. MX385037B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16179692 2016-07-15
PCT/EP2017/067811 WO2018011386A1 (en) 2016-07-15 2017-07-14 Preparation of 14-methyl-16-oxabicyclo[10.3.1]pentadecenes from 3-methyl-1,5-cyclopentadecanedione

Publications (2)

Publication Number Publication Date
MX2019000664A true MX2019000664A (es) 2019-05-20
MX385037B MX385037B (es) 2025-03-14

Family

ID=56418410

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019000664A MX385037B (es) 2016-07-15 2017-07-14 Preparacion de 14-metil-16-oxabiciclo[10.3.1]pentadecenos de 3-metil-1,5- ciclopentadecanediona.

Country Status (8)

Country Link
US (1) US10800724B2 (es)
EP (1) EP3484844B1 (es)
JP (1) JP7039551B2 (es)
CN (1) CN109476577A (es)
BR (1) BR112018077067B1 (es)
ES (1) ES2954272T3 (es)
MX (1) MX385037B (es)
WO (1) WO2018011386A1 (es)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3170828A1 (de) * 2015-11-23 2017-05-24 Basf Se Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten
JP7065825B2 (ja) 2016-07-11 2022-05-12 セージ セラピューティクス， インコーポレイテッド Ｃ７、ｃ１２、およびｃ１６置換神経刺激性ステロイドおよびそれらの使用方法
WO2019086207A1 (en) * 2017-11-01 2019-05-09 Firmenich Sa Process for preparing bicyclic enolether
EP3862356B1 (en) * 2018-09-28 2024-04-03 Kao Corporation Method for producing cyclic enol ether compound
US11753417B2 (en) * 2019-01-17 2023-09-12 International Flavors & Fragrances Inc. Synthesis of 14-methyl-16-oxabicyclo[10.3.1]hexadec-12-ene
WO2020189670A1 (ja) 2019-03-18 2020-09-24 花王株式会社 α－アリル化シクロアルカノンを製造する方法
WO2020189661A1 (ja) 2019-03-18 2020-09-24 花王株式会社 α－アリル化シクロアルカノンを製造する方法
US12037341B2 (en) 2019-04-15 2024-07-16 Firmenich Sa Process for preparing bicyclic enolether
GB202011259D0 (en) * 2020-07-21 2020-09-02 Givaudan Sa Method for the production of musk fragrance ingredient
JP7707121B2 (ja) * 2022-03-31 2025-07-14 花王株式会社 環状ジケトン化合物の製造方法
JP7738514B2 (ja) * 2022-03-31 2025-09-12 花王株式会社 環状ジケトン化合物の製造方法

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CH513791A (de) 1966-12-08 1971-10-15 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Verbindungen
CH519454A (de) 1966-02-08 1972-02-29 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Verbindungen
CH503680A (de) 1966-12-08 1971-02-28 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Ketonen
DE2916418A1 (de) 1979-04-23 1980-11-06 Basf Ag Verfahren zur herstellung von 14- methyl-bicyclo- eckige klammer auf 10.3.0. eckige klammer zu -pentadecen- eckige klammer auf 1(12) eckige klammer zu und neue zwischenprodukte dieses verfahrens
CH642373A5 (fr) * 1979-09-13 1984-04-13 Firmenich & Cie Compose pyrannique, procede pour sa preparation et son utilisation a titre d'intermediaire de synthese.
DE69314121T2 (de) * 1992-07-30 1998-02-26 Firmenich & Cie Verwendung einer Cyclopentadecenone als Parfümszutat
ATE411270T1 (de) * 2004-02-16 2008-10-15 Firmenich & Cie Verfahren zur herstellung von optisch aktiven cyclohexenonen
ES2367229T3 (es) * 2008-02-01 2011-10-31 Firmenich S.A. Ciclohexenonas sustituidas.
EP3094713B1 (en) 2014-01-14 2017-11-15 Firmenich SA Powdery, musky odorant macrocycles
US20170275225A1 (en) 2014-09-09 2017-09-28 Basf Se Method for the preparation of 2-alkoxy cyclohexanol
CN106660916A (zh) 2014-09-09 2017-05-10 巴斯夫欧洲公司 生产芳香物质的方法
MX375962B (es) 2014-09-26 2025-03-06 Basf Se Uso de cis- o trans- (2-isobutil-4-metiltetrahidropiran-4-il)acetato isomericamente puro o altamente enriquecido con isomeros.
US9920007B2 (en) 2014-11-18 2018-03-20 Basf Se Process for the preparation of 1-(2,6,6-trimethylcyclohexyl)-alkan-3-ols
CN107223120B (zh) 2014-12-19 2020-10-13 巴斯夫欧洲公司 作为新型芳香化学品的1-(7,10,10-三甲基-4-双环[6.2.0]癸基)乙酮
CN107001214B (zh) 2014-12-26 2021-03-23 花王株式会社 环状二酮化合物的制造方法
US10106517B2 (en) 2015-03-05 2018-10-23 Basf Se Method for producing tetrahydropyranyl esters
ES2775502T3 (es) 2015-05-20 2020-07-27 Basf Se Procedimiento de preparación de una dicetona macrocíclica
MX2017015395A (es) 2015-05-29 2018-03-01 Basf Se Sustancias quimicas aromaticas novedosas que tienen una porcion de 1,2,2-trimetilciclopentan-1-ilo.
WO2016193330A1 (en) 2015-06-03 2016-12-08 Basf Se Process for preparing 3-methylcyclopentadecane-1,5-dione
EP3319951B1 (de) 2015-07-10 2021-09-08 Basf Se Verfahren zur hydroformylierung von 2-substituierten butadienen und zur herstellung von folgeprodukten davon, speziell von ambrox
EP3322685A1 (en) 2015-07-15 2018-05-23 Basf Se Process for preparing an arylpropene
US10202323B2 (en) 2015-07-15 2019-02-12 Basf Se Process for preparing an arylpropene
WO2017029313A1 (en) 2015-08-18 2017-02-23 Basf Se Process for preparing alpha-damascone
CN108026007B (zh) 2015-09-22 2021-04-20 巴斯夫欧洲公司 制备3-甲基环十五烷-1,5-二醇的方法
EP3170828A1 (de) 2015-11-23 2017-05-24 Basf Se Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten

Also Published As

Publication number Publication date
BR112018077067B1 (pt) 2022-05-31
JP7039551B2 (ja) 2022-03-22
US20190300467A1 (en) 2019-10-03
JP2019521141A (ja) 2019-07-25
MX385037B (es) 2025-03-14
BR112018077067A2 (pt) 2019-04-02
EP3484844A1 (en) 2019-05-22
EP3484844B1 (en) 2023-06-14
CN109476577A (zh) 2019-03-15
ES2954272T3 (es) 2023-11-21
US10800724B2 (en) 2020-10-13
WO2018011386A1 (en) 2018-01-18

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