MX2013011688A - Proceso para producir derivados de celulosa de alta densidad aparente, buena fluidez y dispersabilidad mejorada en agua fria. - Google Patents
Proceso para producir derivados de celulosa de alta densidad aparente, buena fluidez y dispersabilidad mejorada en agua fria.Info
- Publication number
- MX2013011688A MX2013011688A MX2013011688A MX2013011688A MX2013011688A MX 2013011688 A MX2013011688 A MX 2013011688A MX 2013011688 A MX2013011688 A MX 2013011688A MX 2013011688 A MX2013011688 A MX 2013011688A MX 2013011688 A MX2013011688 A MX 2013011688A
- Authority
- MX
- Mexico
- Prior art keywords
- cellulose derivative
- bulk density
- good flowability
- cold water
- cellulose derivatives
- Prior art date
Links
- 229920002678 cellulose Polymers 0.000 title abstract 8
- 239000001913 cellulose Substances 0.000 title abstract 8
- 238000000034 method Methods 0.000 title abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title 1
- 238000001035 drying Methods 0.000 abstract 3
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/02—Alkyl or cycloalkyl ethers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
- A61K47/36—Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
- A61K47/38—Cellulose; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/28—Dragees; Coated pills or tablets, e.g. with film or compression coating
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/48—Preparations in capsules, e.g. of gelatin, of chocolate
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/48—Preparations in capsules, e.g. of gelatin, of chocolate
- A61K9/4816—Wall or shell material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/02—Alkyl or cycloalkyl ethers
- C08B11/04—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals
- C08B11/08—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals with hydroxylated hydrocarbon radicals; Esters, ethers, or acetals thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/20—Post-etherification treatments of chemical or physical type, e.g. mixed etherification in two steps, including purification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/20—Post-etherification treatments of chemical or physical type, e.g. mixed etherification in two steps, including purification
- C08B11/22—Isolation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
- C08J3/05—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media from solid polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/124—Treatment for improving the free-flowing characteristics
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2301/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives
- C08J2301/08—Cellulose derivatives
- C08J2301/26—Cellulose ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2301/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives
- C08J2301/08—Cellulose derivatives
- C08J2301/26—Cellulose ethers
- C08J2301/28—Alkyl ethers
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Biochemistry (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Wood Science & Technology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Medicinal Preparation (AREA)
- Cosmetics (AREA)
Abstract
Se describe un derivado de celulosa particulado que se obtiene en un proceso de molienda y de secado de un derivado de celulosa húmedo que comprende las etapas de A) proporcionar un derivado de celulosa que tiene un contenido de agua de 60 a 95 por ciento, con base en el peso total del derivado de celulosa húmedo, B) moler y parcialmente secar el derivado de celulosa húmedo en un molino de impacto con barrido de gas; y C) poner en contacto el derivado de celulosa molido y parcialmente secado con una cantidad adicional de un gas de secado fuera del molino de impacto con barrido de gas. El derivado de celulosa particulado obtenido tiene una alta densidad aparente no compactada y una buena fluidez.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161472227P | 2011-04-06 | 2011-04-06 | |
| PCT/US2012/031112 WO2012138533A1 (en) | 2011-04-06 | 2012-03-29 | Process for producing cellulose derivatives of high bulk density, good flowability and improved dispersibility in cold water |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2013011688A true MX2013011688A (es) | 2013-11-04 |
| MX344527B MX344527B (es) | 2016-12-19 |
Family
ID=45953273
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2013011688A MX344527B (es) | 2011-04-06 | 2012-03-29 | Proceso para producir derivados de celulosa de alta densidad aparente, buena fluidez y dispersabilidad mejorada en agua fria. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9334416B2 (es) |
| EP (1) | EP2694041B1 (es) |
| JP (1) | JP6034365B2 (es) |
| KR (1) | KR101902751B1 (es) |
| CN (2) | CN103561728B (es) |
| BR (1) | BR112013022418A2 (es) |
| MX (1) | MX344527B (es) |
| WO (1) | WO2012138533A1 (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX337827B (es) * | 2011-04-06 | 2016-03-22 | Dow Global Technologies Llc | Novedosos derivados polisacaridos y formas de administracion. |
| EP2900753B1 (en) | 2012-09-25 | 2018-07-04 | Dow Global Technologies LLC | Process for producing cellulose derivatives of high bulk density, good flowability and/or dispersibility in cold water as well as low solution color |
| KR102033179B1 (ko) * | 2012-12-28 | 2019-10-16 | 롯데정밀화학 주식회사 | 스킴코트 모르타르용 첨가제 및 이를 포함하는 스킴코트 모르타르 조성물 |
| KR20160094987A (ko) | 2013-12-04 | 2016-08-10 | 다우 글로벌 테크놀로지스 엘엘씨 | 셀룰로오스 유도체와 액체 희석제의 혼합물의 제조 방법 |
| KR101512188B1 (ko) | 2014-02-11 | 2015-04-22 | 한국전기연구원 | 모듈형 멀티레벨 컨버터의 구동방법 및 구동장치 |
| MX2017003561A (es) * | 2014-08-22 | 2017-08-28 | Medipath Inc | Composiciones y metodos para revestimientos cannabinoides para su uso en la administracion de farmacos. |
| JP6271817B1 (ja) * | 2015-01-08 | 2018-01-31 | ダウ グローバル テクノロジーズ エルエルシー | 水不溶性粒子の含有量を減少させた水溶性セルロース誘導体を生成するための方法 |
| JP6609726B1 (ja) * | 2018-02-07 | 2019-11-20 | 株式会社ダイセル | セルロースアセテート粒子、化粧品組成物及びセルロースアセテート粒子の製造方法 |
| CN109517075A (zh) * | 2018-11-22 | 2019-03-26 | 北方天普化工有限公司 | 一种羟丙基甲基纤维素制备方法及产品 |
| WO2022016248A1 (pt) * | 2020-07-21 | 2022-01-27 | Petróleo Brasileiro S.A. - Petrobras | Sistema de terceiro estágio com auto-sangria e uso |
| BR112023013931A2 (pt) * | 2021-01-13 | 2024-01-23 | Nutrition & Biosciences Usa 1 Llc | Método aprimorado para a preparação de celulose microcristalina coloidal |
| US20260027033A1 (en) | 2023-03-22 | 2026-01-29 | Eastman Chemical Company | Biodegradable cellulose ester microparticles and systems and methods for the production thereof |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2331864A (en) | 1942-03-20 | 1943-10-12 | Dow Chemical Co | Method of preparing powdered cellulose ethers quickly soluble in cold water |
| GB804306A (en) | 1956-12-13 | 1958-11-12 | Dow Chemical Co | Method of preparing cellulose ethers readily soluble in cold water |
| JPS5163927A (en) * | 1974-11-28 | 1976-06-02 | Shinetsu Chemical Co | Ketsugoseiryokonajozaihokaizaino seizohoho |
| DE10246632B4 (de) * | 2002-10-07 | 2013-05-08 | Christian Bumm | Spritzfähiges Beschichtungsmittel hergestellt mit einem Granulat, seine Herstellung und Trockenmischung und Verwendung. |
| DE3839831A1 (de) * | 1988-11-25 | 1990-05-31 | Hoechst Ag | Verfahren und vorrichtung zur produktschonenden mahlung und gleichzeitigen trocknung von feuchten celluloseethern |
| GB2262527A (en) | 1992-07-02 | 1993-06-23 | Dow Deutschland Inc | Process for grinding cellulose compounds |
| US5488104A (en) * | 1994-06-30 | 1996-01-30 | The Dow Chemical Company | Process for comminuting cellulose ethers |
| JP2959423B2 (ja) | 1994-12-01 | 1999-10-06 | シオノギクオリカプス株式会社 | カプセル用皮膜組成物 |
| EP0824107A3 (de) | 1996-08-12 | 1998-04-22 | Lenzing Aktiengesellschaft | Cellulosepartikel |
| DE19641781A1 (de) * | 1996-10-10 | 1998-04-16 | Clariant Gmbh | Verfahren und Vorrichtung zum gleichzeitigen Mahlen und Trocknen eines feuchten Celluloseether enthaltenden Mahlgutes |
| CA2278488C (en) | 1997-01-21 | 2007-03-20 | Wolff Walsrode Ag | Process for preparing fine-particle polysaccharide derivatives |
| US6680069B1 (en) * | 1999-11-09 | 2004-01-20 | Shin-Etsu Chemical Co., Ltd. | Low-substituted hydroxypropyl cellulose and process for manufacturing the same |
| JP4070402B2 (ja) * | 1999-11-09 | 2008-04-02 | 信越化学工業株式会社 | 低置換度ヒドロキシプロピルセルロース及びその製造方法 |
| DE10009411A1 (de) * | 2000-02-28 | 2001-08-30 | Wolff Walsrode Ag | Verfahren zur Herstellung pulverförmiger wasserlöslicher Cellulosederivate unter Einsatz eines Wasserdampf/Inertgas-Gemisch oder Wasserdampf/Luft-Gemisch als Transport und Wärmeträgergas |
| DE10009409A1 (de) | 2000-02-28 | 2001-08-30 | Wolff Walsrode Ag | Verfahren zur Herstellung von pulverförmigen wasserlöslichen Cellulosederivaten |
| KR100379674B1 (ko) | 2000-03-06 | 2003-04-10 | 주식회사 서흥캅셀 | 펙틴과 글리세린의 배합용액을 이용한 셀룰로오스 캅셀 및그의 제조방법 |
| DE10018155A1 (de) | 2000-04-12 | 2001-10-25 | Clariant Gmbh | Verfahren zur Herstellung von gut benetzbaren, wasserlöslichen, pulverförmigen, mindestens alkylierten, nicht-ionischen Celluloseethern |
| DE10152991A1 (de) * | 2001-10-26 | 2003-05-08 | Wolff Walsrode Ag | Verfahren und Vorrichtung zur Mahltrocknung |
| WO2006120194A1 (en) * | 2005-05-12 | 2006-11-16 | Akzo Nobel N.V. | Process for grinding cellulose ether |
| PL1984429T3 (pl) | 2006-01-30 | 2018-05-30 | Hercules Llc | Sposób wytwarzania eterów celulozy ulegających rozproszeniu w zimnej wodzie |
| US8519120B2 (en) | 2006-08-08 | 2013-08-27 | Shin-Etsu Chemical Co., Ltd. | Methods for producing a low-substituted hydroxypropylcellulose powder |
| JP5258223B2 (ja) * | 2006-08-08 | 2013-08-07 | 信越化学工業株式会社 | 腸溶性固体分散体の固形製剤及びその製造方法 |
| EP3594248B1 (en) | 2006-10-27 | 2021-08-04 | Capsugel Belgium NV | Hydroxypropyl methyl cellulose hard capsules and process of manufacture |
| DE102006057188A1 (de) * | 2006-12-05 | 2008-06-12 | Dow Wolff Cellulosics Gmbh | Celluloseether für Feststoffformulierungen |
| KR101774208B1 (ko) | 2010-07-28 | 2017-09-04 | 다우 글로벌 테크놀로지스 엘엘씨 | 폴리삭카라이드 유도체의 건식 분쇄 방법 |
-
2012
- 2012-03-29 MX MX2013011688A patent/MX344527B/es active IP Right Grant
- 2012-03-29 KR KR1020137026352A patent/KR101902751B1/ko active Active
- 2012-03-29 CN CN201280025503.3A patent/CN103561728B/zh active Active
- 2012-03-29 WO PCT/US2012/031112 patent/WO2012138533A1/en not_active Ceased
- 2012-03-29 BR BR112013022418A patent/BR112013022418A2/pt not_active Application Discontinuation
- 2012-03-29 EP EP12714151.3A patent/EP2694041B1/en active Active
- 2012-03-29 CN CN201610320448.0A patent/CN105949328A/zh active Pending
- 2012-03-29 JP JP2014503691A patent/JP6034365B2/ja active Active
- 2012-03-29 US US14/009,442 patent/US9334416B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| MX344527B (es) | 2016-12-19 |
| CN103561728B (zh) | 2016-08-10 |
| CN105949328A (zh) | 2016-09-21 |
| CN103561728A (zh) | 2014-02-05 |
| EP2694041A1 (en) | 2014-02-12 |
| EP2694041B1 (en) | 2019-12-11 |
| KR101902751B1 (ko) | 2018-10-02 |
| US9334416B2 (en) | 2016-05-10 |
| KR20140015446A (ko) | 2014-02-06 |
| BR112013022418A2 (pt) | 2016-12-06 |
| JP6034365B2 (ja) | 2016-11-30 |
| US20140013999A1 (en) | 2014-01-16 |
| WO2012138533A1 (en) | 2012-10-11 |
| JP2014510185A (ja) | 2014-04-24 |
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