MX2011008790A - Reactor de lecho fluidizado para la produccion de silice de alta pureza. - Google Patents
Reactor de lecho fluidizado para la produccion de silice de alta pureza.Info
- Publication number
- MX2011008790A MX2011008790A MX2011008790A MX2011008790A MX2011008790A MX 2011008790 A MX2011008790 A MX 2011008790A MX 2011008790 A MX2011008790 A MX 2011008790A MX 2011008790 A MX2011008790 A MX 2011008790A MX 2011008790 A MX2011008790 A MX 2011008790A
- Authority
- MX
- Mexico
- Prior art keywords
- fluidized bed
- bed reactor
- production
- high purity
- purity silicon
- Prior art date
Links
- 229910052710 silicon Inorganic materials 0.000 title abstract 3
- 239000010703 silicon Substances 0.000 title abstract 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000007789 gas Substances 0.000 abstract 2
- 239000011241 protective layer Substances 0.000 abstract 2
- 238000005260 corrosion Methods 0.000 abstract 1
- 230000007797 corrosion Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/037—Purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/027—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1818—Feeding of the fluidising gas
- B01J8/1827—Feeding of the fluidising gas the fluidising gas being a reactant
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/027—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
- C01B33/029—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material by decomposition of monosilane
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/027—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
- C01B33/03—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material by decomposition of silicon halides or halosilanes or reduction thereof with hydrogen as the only reducing agent
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/027—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
- C01B33/035—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material by decomposition or reduction of gaseous or vaporised silicon compounds in the presence of heated filaments of silicon, carbon or a refractory metal, e.g. tantalum or tungsten, or in the presence of heated silicon rods on which the formed silicon is deposited, a silicon rod being obtained, e.g. Siemens process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00389—Controlling the temperature using electric heating or cooling elements
- B01J2208/00407—Controlling the temperature using electric heating or cooling elements outside the reactor bed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00389—Controlling the temperature using electric heating or cooling elements
- B01J2208/00415—Controlling the temperature using electric heating or cooling elements electric resistance heaters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00433—Controlling the temperature using electromagnetic heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00433—Controlling the temperature using electromagnetic heating
- B01J2208/0046—Infrared radiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
- B01J2219/0236—Metal based
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Silicon Compounds (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
Se describen los métodos y aparatos para la producción de silicio de alta pureza incluyendo un reactor de lecho fluidizado con una o más capas protectoras depositadas sobre una superficie interna del reactor de lecho fluidizado. La capa protectora puede ser resistente a la corrosión por los gases de fluidización y los gases que llevan silicio.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/393,852 US8168123B2 (en) | 2009-02-26 | 2009-02-26 | Fluidized bed reactor for production of high purity silicon |
| PCT/US2009/065345 WO2010098797A1 (en) | 2009-02-26 | 2009-11-20 | Fluidized bed reactor for production of high purity silicon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2011008790A true MX2011008790A (es) | 2011-12-14 |
Family
ID=42631134
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2011008790A MX2011008790A (es) | 2009-02-26 | 2009-11-20 | Reactor de lecho fluidizado para la produccion de silice de alta pureza. |
Country Status (12)
| Country | Link |
|---|---|
| US (3) | US8168123B2 (es) |
| EP (1) | EP2318313A4 (es) |
| JP (1) | JP2012519130A (es) |
| KR (1) | KR20110132338A (es) |
| CN (1) | CN102239115A (es) |
| AU (1) | AU2009341100A1 (es) |
| BR (1) | BRPI0924261A2 (es) |
| CA (1) | CA2753354A1 (es) |
| MX (1) | MX2011008790A (es) |
| RU (1) | RU2011139109A (es) |
| TW (1) | TW201034757A (es) |
| WO (1) | WO2010098797A1 (es) |
Families Citing this family (33)
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| CN103787336B (zh) | 2008-09-16 | 2016-09-14 | 储晞 | 生产高纯颗粒硅的方法 |
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| US8168123B2 (en) | 2009-02-26 | 2012-05-01 | Siliken Chemicals, S.L. | Fluidized bed reactor for production of high purity silicon |
| TW201113391A (en) * | 2009-03-19 | 2011-04-16 | Ae Polysilicon Corp | Silicide-coated metal surfaces and methods of utilizing same |
| TWI498165B (zh) * | 2009-04-20 | 2015-09-01 | Jiangsu Zhongneng Polysilicon Technology Dev Co Ltd | 具有經矽化物塗覆的金屬表面之反應器 |
| TWI454309B (zh) * | 2009-04-20 | 2014-10-01 | Jiangsu Zhongneng Polysilicon Technology Dev Co Ltd | 用於將反應排出氣體冷卻之方法及系統 |
| US8029756B1 (en) * | 2010-03-30 | 2011-10-04 | Peak Sun Sillcon Corporation | Closed-loop silicon production |
| CN101935038B (zh) * | 2010-08-13 | 2013-04-10 | 镇江环太硅科技有限公司 | 硅锭切割废料回收方法 |
| US20120148728A1 (en) * | 2010-12-09 | 2012-06-14 | Siliken Sa | Methods and apparatus for the production of high purity silicon |
| KR20140005199A (ko) * | 2011-01-19 | 2014-01-14 | 알이씨 실리콘 인코포레이티드 | 반응기 시스템 및 이를 사용한 다결정 실리콘 제조 방법 |
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| US8875728B2 (en) | 2012-07-12 | 2014-11-04 | Siliken Chemicals, S.L. | Cooled gas distribution plate, thermal bridge breaking system, and related methods |
| EP2883613B1 (en) * | 2012-08-13 | 2020-09-09 | Jiangsu Zhongneng Polysilicon Technology Development Co., Ltd. | Method for preparing high sphericity seed crystal and fluidized bed particle silicon |
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| DE112013005298T5 (de) * | 2012-11-06 | 2015-07-23 | Rec Silicon Inc | Verfahren und Vorrichtung zum Reduzieren der Kontamination von Partikeln in einem Fliessbettreaktor |
| US9587993B2 (en) | 2012-11-06 | 2017-03-07 | Rec Silicon Inc | Probe assembly for a fluid bed reactor |
| US9212421B2 (en) | 2013-07-10 | 2015-12-15 | Rec Silicon Inc | Method and apparatus to reduce contamination of particles in a fluidized bed reactor |
| CN104302810B (zh) * | 2012-12-21 | 2017-03-29 | 陕西有色天宏瑞科硅材料有限责任公司 | 流化床反应器设备用的高温级钢 |
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| DE102013206339A1 (de) * | 2013-04-10 | 2014-10-16 | Wacker Chemie Ag | Vorrichtung und Verfahren zum Ausbau von polykristallinen Siliciumstäben aus einem Reaktor |
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| US9662628B2 (en) | 2014-08-15 | 2017-05-30 | Rec Silicon Inc | Non-contaminating bonding material for segmented silicon carbide liner in a fluidized bed reactor |
| US20160045881A1 (en) * | 2014-08-15 | 2016-02-18 | Rec Silicon Inc | High-purity silicon to form silicon carbide for use in a fluidized bed reactor |
| US9446367B2 (en) | 2014-08-15 | 2016-09-20 | Rec Silicon Inc | Joint design for segmented silicon carbide liner in a fluidized bed reactor |
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| CN104383865B (zh) * | 2014-11-20 | 2016-09-21 | 江苏科技大学 | 一种磁流化床装置及使用该装置的控制方法和试验方法 |
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| EP3310942B1 (en) | 2015-06-16 | 2022-07-13 | Versum Materials US, LLC | Processes for depositing silicon-containing films |
| RU2022102529A (ru) * | 2015-10-09 | 2022-03-03 | МИЛУОКИ СИЛИКОН, ЭлЭлСи | Очищенный кремний, а также устройства и системы для его производства |
| WO2019079879A1 (en) | 2017-10-27 | 2019-05-02 | Kevin Allan Dooley Inc. | SYSTEM AND METHOD FOR PRODUCING HIGH-PURITY SILICON |
| JP6911219B1 (ja) * | 2019-11-22 | 2021-07-28 | 株式会社トクヤマ | トリクロロシランの製造方法 |
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| WO2003040036A1 (fr) | 2001-10-19 | 2003-05-15 | Tokuyama Corporation | Procede de production de silicium |
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| WO2004035472A1 (ja) * | 2002-09-12 | 2004-04-29 | Takayuki Shimamune | 高純度シリコンの製造方法及び装置 |
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| GB0327169D0 (en) * | 2003-11-21 | 2003-12-24 | Statoil Asa | Method |
| CN1898411A (zh) * | 2003-12-23 | 2007-01-17 | 约翰·C·舒马赫 | 用于半导体反应器的排气调节系统 |
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| US8168123B2 (en) | 2009-02-26 | 2012-05-01 | Siliken Chemicals, S.L. | Fluidized bed reactor for production of high purity silicon |
-
2009
- 2009-02-26 US US12/393,852 patent/US8168123B2/en not_active Expired - Fee Related
- 2009-11-20 MX MX2011008790A patent/MX2011008790A/es not_active Application Discontinuation
- 2009-11-20 RU RU2011139109/05A patent/RU2011139109A/ru unknown
- 2009-11-20 AU AU2009341100A patent/AU2009341100A1/en not_active Abandoned
- 2009-11-20 EP EP09840944.4A patent/EP2318313A4/en not_active Withdrawn
- 2009-11-20 BR BRPI0924261-9A patent/BRPI0924261A2/pt not_active IP Right Cessation
- 2009-11-20 CN CN2009801490221A patent/CN102239115A/zh active Pending
- 2009-11-20 CA CA2753354A patent/CA2753354A1/en not_active Abandoned
- 2009-11-20 WO PCT/US2009/065345 patent/WO2010098797A1/en not_active Ceased
- 2009-11-20 KR KR1020117019738A patent/KR20110132338A/ko not_active Ceased
- 2009-11-20 JP JP2011552017A patent/JP2012519130A/ja active Pending
- 2009-11-24 TW TW098139951A patent/TW201034757A/zh unknown
-
2010
- 2010-10-13 US US12/903,994 patent/US8158093B2/en not_active Expired - Fee Related
-
2012
- 2012-03-14 US US13/420,074 patent/US20120171102A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| EP2318313A4 (en) | 2013-05-01 |
| WO2010098797A1 (en) | 2010-09-02 |
| US8168123B2 (en) | 2012-05-01 |
| EP2318313A1 (en) | 2011-05-11 |
| TW201034757A (en) | 2010-10-01 |
| AU2009341100A1 (en) | 2011-09-08 |
| US20120171102A1 (en) | 2012-07-05 |
| CN102239115A (zh) | 2011-11-09 |
| US20110027160A1 (en) | 2011-02-03 |
| JP2012519130A (ja) | 2012-08-23 |
| RU2011139109A (ru) | 2013-11-20 |
| US8158093B2 (en) | 2012-04-17 |
| BRPI0924261A2 (pt) | 2015-08-25 |
| CA2753354A1 (en) | 2010-09-02 |
| KR20110132338A (ko) | 2011-12-07 |
| US20100215562A1 (en) | 2010-08-26 |
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