MX2010003148A - Procedimiento para la preparacion de diamidas de acido sulfonico. - Google Patents
Procedimiento para la preparacion de diamidas de acido sulfonico.Info
- Publication number
- MX2010003148A MX2010003148A MX2010003148A MX2010003148A MX2010003148A MX 2010003148 A MX2010003148 A MX 2010003148A MX 2010003148 A MX2010003148 A MX 2010003148A MX 2010003148 A MX2010003148 A MX 2010003148A MX 2010003148 A MX2010003148 A MX 2010003148A
- Authority
- MX
- Mexico
- Prior art keywords
- sup
- formula
- atoms
- iii
- sulfonic acid
- Prior art date
Links
- -1 sulfonic acid diamides Chemical class 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 4
- 229910052757 nitrogen Inorganic materials 0.000 abstract 3
- QAHVHSLSRLSVGS-UHFFFAOYSA-N sulfamoyl chloride Chemical compound NS(Cl)(=O)=O QAHVHSLSRLSVGS-UHFFFAOYSA-N 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 125000003118 aryl group Chemical group 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 125000004433 nitrogen atom Chemical group N* 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 125000005842 heteroatom Chemical group 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 1
- 150000003335 secondary amines Chemical class 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/34—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfuric acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C307/00—Amides of sulfuric acids, i.e. compounds having singly-bound oxygen atoms of sulfate groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C307/04—Diamides of sulfuric acids
- C07C307/06—Diamides of sulfuric acids having nitrogen atoms of the sulfamide groups bound to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C381/00—Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
- C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
- C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
- C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
- C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
- C07D239/52—Two oxygen atoms
- C07D239/54—Two oxygen atoms as doubly bound oxygen atoms or as unsubstituted hydroxy radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Procedimiento para la preparaci?n de diamidas de ?cido sulf?nico de la f?rmula I R1R2N-S(O)2-NH2 (I), en donde R1 y R2 representan, independientemente el uno del otro, un radical alquilo primario con 1 a 8 ?tomos de carbono, un radical alquilo secundario con 3 a 8 ?tomos de carbono o un radical cicloalquilo con 5 a 8 ?tomos de carbono, o forman, junto con el ?tomo de nitr?geno, un heterociclo de nitr?geno, saturado, de 5 a 8 miembros, que puede presentar como miembro de anillo, junto con el ?tomo de nitr?geno, otro hetero?tomo seleccionado de entre O y S, pudiendo el heterociclo de nitr?geno presentar 1, 2, 3 ? 4 grupos alquilo, cada cual con 1 a 4 ?tomos de carbono como sustituyentes, y que comprende i) hacer reaccionar con cloruro de sulfurilo una amina secundaria de la f?rmula II R1R2NH (II), en la que R1 y R2 tienen los significados antedichos, en un disolvente org?nico inerte y en presencia de una amina terciaria, para convertirla en un cloruro de sulfamo?lo de la f?rmula III R1R2N-S(O)2-CI (III), en la que R1 y R2 tienen los significado antedichos, y ii) hacer reaccionar con amoniaco el cloruro de sulfamo?lo de la f?rmula III obtenido en el pasa i), y en el que el paso ii) se aplica, en el disolvente inerte, en particular el disolvente arom?tico, el cloruro de sulfamo?lo de la f?rmula III en la forma de la soluci?n obtenida en el paso i).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP07118416 | 2007-10-12 | ||
| PCT/EP2008/063630 WO2009050120A1 (de) | 2007-10-12 | 2008-10-10 | Verfahren zur herstelung von sulfonsäurediamiden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2010003148A true MX2010003148A (es) | 2010-04-01 |
Family
ID=39186045
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2010003148A MX2010003148A (es) | 2007-10-12 | 2008-10-10 | Procedimiento para la preparacion de diamidas de acido sulfonico. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US9920002B2 (es) |
| EP (1) | EP2200978A1 (es) |
| JP (1) | JP5465672B2 (es) |
| CN (1) | CN101821233B (es) |
| AR (1) | AR068849A1 (es) |
| BR (1) | BRPI0818408B1 (es) |
| IL (1) | IL204595A (es) |
| MX (1) | MX2010003148A (es) |
| WO (1) | WO2009050120A1 (es) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007063028A2 (de) * | 2005-12-01 | 2007-06-07 | Basf Se | Verfahren zur herstellung von sulfonamiden |
| CN103130727B (zh) * | 2013-02-27 | 2015-07-08 | 江苏省农用激素工程技术研究中心有限公司 | 苯嘧磺草胺中间体的制备方法 |
| JP6141762B2 (ja) * | 2013-12-27 | 2017-06-07 | 富士フイルム株式会社 | 染料化合物及びその製造方法、着色硬化性組成物、カラーフィルタ及びその製造方法、画像表示装置、並びに固体撮像素子 |
| CN107827786A (zh) * | 2017-11-24 | 2018-03-23 | 常州沃腾化工科技有限公司 | N‑甲基‑n‑异丙基胺基磺酰胺的生产方法 |
| EP3587396A1 (en) | 2018-06-27 | 2020-01-01 | Basf Se | A method of isolating a n-(3-nitrobenzoyl)sulfamide |
| US11267707B2 (en) * | 2019-04-16 | 2022-03-08 | Honeywell International Inc | Purification of bis(fluorosulfonyl) imide |
| CN112679292B (zh) * | 2020-12-25 | 2022-05-20 | 复旦大学 | 一种磺酰仲胺类化合物的合成方法 |
| CN113185467B (zh) * | 2021-04-20 | 2022-03-08 | 江苏乾元生物科技有限公司 | 一种苯嘧磺草胺的制备方法 |
| CN115246791B (zh) * | 2021-04-26 | 2024-11-05 | 内蒙古世杰化工有限公司 | 一种合成6-三氟甲基尿嘧啶的方法及其中间体 |
| CN114478326B (zh) * | 2022-01-21 | 2023-10-03 | 安徽宁亿泰科技有限公司 | 一种苯嘧磺草胺关键中间体的合成方法 |
| CN121039108A (zh) | 2023-03-30 | 2025-11-28 | 安道麦阿甘有限公司 | 用于制备磺酰胺衍生物的方法 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1240853B (de) * | 1962-12-06 | 1967-05-24 | Smith Kline French Lab | Verfahren zur Herstellung von Sulfurylamiden |
| US3198785A (en) * | 1964-04-17 | 1965-08-03 | Sandoz Ag | Sulfamoyl azabicyclononanes and derivatives thereof |
| US3709677A (en) * | 1969-06-25 | 1973-01-09 | Sandoz Ag | N-substituted sulfamoyl compounds useful as herbicides |
| NL175521C (nl) * | 1973-04-26 | 1984-11-16 | Hoechst Ag | Werkwijze voor het bereiden van carbonzuurchloriden. |
| DE2933148A1 (de) * | 1979-08-16 | 1981-02-26 | Bayer Ag | Verfahren zur herstellung von aromatischen dicarbonsaeuredichloriden iv |
| DE3040295A1 (de) * | 1980-10-25 | 1982-06-03 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von aromatischen carbonsaeurechloriden |
| JPS61155350A (ja) | 1984-12-28 | 1986-07-15 | Ihara Nikkei Kagaku Kogyo Kk | 脂肪酸クロライド及び芳香族酸クロライドの製造方法 |
| BR8807217A (pt) | 1987-09-23 | 1989-10-17 | Hoffmann La Roche | Compostos heterocilicos |
| US5238908A (en) * | 1989-08-31 | 1993-08-24 | Rohm And Haas Company | Herbicidal glutaramic acids and derivatives |
| TW224421B (es) * | 1991-12-24 | 1994-06-01 | Shell Internat Researce Schappel N V | |
| WO1998032748A1 (en) * | 1997-01-23 | 1998-07-30 | F. Hoffmann-La Roche Ag | Sulfamide-metalloprotease inhibitors |
| US20020065270A1 (en) | 1999-12-28 | 2002-05-30 | Moriarty Kevin Joseph | N-heterocyclic inhibitors of TNF-alpha expression |
| IL150420A0 (en) | 1999-12-28 | 2002-12-01 | Pharmacopeia Inc | Pyrimidine and triazine kinase inhibitors |
| EP1274708A1 (en) | 2000-04-17 | 2003-01-15 | Basf Aktiengesellschaft | Herbicidal 3-heterocyclic substituted benzisothiazole and benzisoxazole compounds |
| US6251829B1 (en) * | 2000-04-18 | 2001-06-26 | Rohm And Haas Company | Herbicidal benzoyloxy carboxylates and carboxamides |
| DK1226127T3 (da) * | 2000-05-04 | 2009-10-19 | Basf Se | Substituerede phenylsulfamoylcarboxamider |
| JP2004535446A (ja) | 2001-06-26 | 2004-11-25 | ブリストル−マイヤーズ スクイブ カンパニー | ＴＮＦ−α発現のＮ−ヘテロ環阻害剤 |
| CA2448737C (en) | 2001-07-20 | 2010-06-01 | Boehringer Ingelheim (Canada) Ltd. | Viral polymerase inhibitors |
| JP4384028B2 (ja) * | 2002-05-16 | 2009-12-16 | ビーエーエスエフ ソシエタス・ヨーロピア | スルファミン酸ハロゲン化物の製造方法 |
| AU2003301443A1 (en) | 2002-10-18 | 2004-05-04 | E.I. Du Pont De Nemours And Company | Azolecarboxamide herbicides |
| BR0315932A (pt) * | 2002-10-30 | 2005-09-13 | Basf Ag | Processo para a preparação de iso (tio) cianatos de fenila, composto, e, processo para a preparação do mesmo |
| WO2004106324A1 (en) | 2003-05-27 | 2004-12-09 | E.I. Dupont De Nemours And Company | Azolecarboxamide herbicides |
| EP1516870A1 (en) | 2003-09-22 | 2005-03-23 | Fuji Photo Film Co., Ltd. | Process for producing aromatic compound derivative by reaction of aromatic compound substituted with sulfamoyloxy, sulfinamoyloxy, or carbamoyloxy group, with nucleophilic agent |
| JP4351888B2 (ja) * | 2003-09-22 | 2009-10-28 | 富士フイルム株式会社 | スルファモイルオキシ基またはスルフィナモイルオキシ基が置換された芳香族化合物と求核剤との反応による芳香族化合物誘導体の製造方法 |
| ES2465499T3 (es) * | 2004-07-22 | 2014-06-05 | Basf Se | Procedimiento para la preparación de 3-fenil(tio)uracilos y -ditiouracilos |
| JP2006083133A (ja) * | 2004-09-17 | 2006-03-30 | Sankyo Co Ltd | スルファミド誘導体医薬組成物 |
| ITMI20050275A1 (it) | 2005-02-22 | 2006-08-23 | Miteni Spa | Procedimento per la preparazione di derivati dell'acido benzoico attraverso un nuovo intermedio di sintesi |
| CA2609050C (en) * | 2005-05-24 | 2013-11-05 | Basf Aktiengesellschaft | Method for production of 1-alkyl-3-phenyluracils |
| WO2007063028A2 (de) * | 2005-12-01 | 2007-06-07 | Basf Se | Verfahren zur herstellung von sulfonamiden |
-
2008
- 2008-10-10 BR BRPI0818408-9A patent/BRPI0818408B1/pt active IP Right Grant
- 2008-10-10 EP EP08838788A patent/EP2200978A1/de not_active Withdrawn
- 2008-10-10 US US12/681,843 patent/US9920002B2/en active Active
- 2008-10-10 WO PCT/EP2008/063630 patent/WO2009050120A1/de not_active Ceased
- 2008-10-10 MX MX2010003148A patent/MX2010003148A/es active IP Right Grant
- 2008-10-10 CN CN200880111156.XA patent/CN101821233B/zh active Active
- 2008-10-10 JP JP2010528412A patent/JP5465672B2/ja active Active
- 2008-10-10 AR ARP080104453A patent/AR068849A1/es active IP Right Grant
-
2010
- 2010-03-18 IL IL204595A patent/IL204595A/en active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| US9920002B2 (en) | 2018-03-20 |
| IL204595A (en) | 2014-03-31 |
| IL204595A0 (en) | 2010-11-30 |
| EP2200978A1 (de) | 2010-06-30 |
| JP5465672B2 (ja) | 2014-04-09 |
| US20100222586A1 (en) | 2010-09-02 |
| BRPI0818408A2 (pt) | 2015-09-15 |
| BRPI0818408B1 (pt) | 2024-01-09 |
| CN101821233A (zh) | 2010-09-01 |
| JP2011500536A (ja) | 2011-01-06 |
| AR068849A1 (es) | 2009-12-09 |
| WO2009050120A1 (de) | 2009-04-23 |
| CN101821233B (zh) | 2016-06-29 |
| BRPI0818408A8 (pt) | 2016-11-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |