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BRPI0818408A8 - Processos para preparar diamidas sulfúricas e ingredientes herbricidas atvos. - Google Patents

Processos para preparar diamidas sulfúricas e ingredientes herbricidas atvos.

Info

Publication number
BRPI0818408A8
BRPI0818408A8 BRPI0818408A BRPI0818408A BRPI0818408A8 BR PI0818408 A8 BRPI0818408 A8 BR PI0818408A8 BR PI0818408 A BRPI0818408 A BR PI0818408A BR PI0818408 A BRPI0818408 A BR PI0818408A BR PI0818408 A8 BRPI0818408 A8 BR PI0818408A8
Authority
BR
Brazil
Prior art keywords
iii
formula
carbon atoms
ingredients
processes
Prior art date
Application number
BRPI0818408A
Other languages
English (en)
Inventor
Pleschke Axel
Schmidt Thomas
Gebhardt Joachim
Löhr Sandra
Keil Michael
Hendrik Wevers Jan
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BRPI0818408A2 publication Critical patent/BRPI0818408A2/pt
Publication of BRPI0818408A8 publication Critical patent/BRPI0818408A8/pt
Publication of BRPI0818408B1 publication Critical patent/BRPI0818408B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/34—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfuric acids
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C307/00—Amides of sulfuric acids, i.e. compounds having singly-bound oxygen atoms of sulfate groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C307/04—Diamides of sulfuric acids
    • C07C307/06—Diamides of sulfuric acids having nitrogen atoms of the sulfamide groups bound to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C381/00—Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
    • C07D239/52—Two oxygen atoms
    • C07D239/54—Two oxygen atoms as doubly bound oxygen atoms or as unsubstituted hydroxy radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PROCESSOS PARA PREPARAR DIAMIDAS SULFÚRICAS E INGREDIENTES HERBICIDAS ATIVOS. A presente invenção se refere a um método para produzir aminas de dcido sulfônico da formula geral (I) R1R2N-S(O)2-NH2(I), onde R1 e R2 são independentes um do outro e representa um radical alquila primário tendo de 1 a 8 átomos de carbono, um radical alguila secunddário tendo de 3 a 8 átomos de carbono, ou um radical cicloalquila tendo de 5 a 8 átomos de carbono, ou, junto com átomo de nitrogénio, formam um composto heterociclico de nitrogênio saturado de 5 a 8 membros gue pode compreender, além do atomo de nitrogênio, um heteroátomo adicional, selecionado dentre O e S, como um membro de anel, onde o composto heterociclico de nitrogênio é insubstituido, ou pode compreender 1, 2, 3 ou 4 grupos alquila cada um tendo 1 a 4 átomos de carbono como substituintes. O método compreende as seguintes etapas: i) conversão de uma amina secundária da formula (Il), R1R2NH (Il), onde R1 e R2 tém o significado indicado acima, tendo cloreto de sulfurila em um solvente inorte, particularmente aromático, na presença de uma amina tercidria, para formar um sulfamoila da fórmula (III) R1R2N-S(O2)-CI (III) onde R1 e R2 tém o significado indicado acima, e (iii) conversão do cloreto de sulfamoila da fórmula (III) obtido na etapa i) usando amônia, onde na etapa ii) o cloreto de sulfamoila da fórmula (III) é usado na forma de solução obtida na etapa i) no solvente inerte, particularmente aromático..
BRPI0818408-9A 2007-10-12 2008-10-10 Processos para preparar diamidas sulfúricas e ingredientes herbicidas ativos BRPI0818408B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP07118416 2007-10-12
EP07118416.2 2007-10-12
PCT/EP2008/063630 WO2009050120A1 (de) 2007-10-12 2008-10-10 Verfahren zur herstelung von sulfonsäurediamiden

Publications (3)

Publication Number Publication Date
BRPI0818408A2 BRPI0818408A2 (pt) 2015-09-15
BRPI0818408A8 true BRPI0818408A8 (pt) 2016-11-22
BRPI0818408B1 BRPI0818408B1 (pt) 2024-01-09

Family

ID=39186045

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0818408-9A BRPI0818408B1 (pt) 2007-10-12 2008-10-10 Processos para preparar diamidas sulfúricas e ingredientes herbicidas ativos

Country Status (9)

Country Link
US (1) US9920002B2 (pt)
EP (1) EP2200978A1 (pt)
JP (1) JP5465672B2 (pt)
CN (1) CN101821233B (pt)
AR (1) AR068849A1 (pt)
BR (1) BRPI0818408B1 (pt)
IL (1) IL204595A (pt)
MX (1) MX2010003148A (pt)
WO (1) WO2009050120A1 (pt)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2821516A1 (en) 2005-12-01 2007-06-07 Basf Se Process for producing fluorinated m-nitrobenzoyl chlorides
CN103130727B (zh) * 2013-02-27 2015-07-08 江苏省农用激素工程技术研究中心有限公司 苯嘧磺草胺中间体的制备方法
JP6141762B2 (ja) * 2013-12-27 2017-06-07 富士フイルム株式会社 染料化合物及びその製造方法、着色硬化性組成物、カラーフィルタ及びその製造方法、画像表示装置、並びに固体撮像素子
CN107827786A (zh) * 2017-11-24 2018-03-23 常州沃腾化工科技有限公司 N‑甲基‑n‑异丙基胺基磺酰胺的生产方法
EP3587396A1 (en) 2018-06-27 2020-01-01 Basf Se A method of isolating a n-(3-nitrobenzoyl)sulfamide
US11267707B2 (en) 2019-04-16 2022-03-08 Honeywell International Inc Purification of bis(fluorosulfonyl) imide
CN112679292B (zh) * 2020-12-25 2022-05-20 复旦大学 一种磺酰仲胺类化合物的合成方法
CN113185467B (zh) * 2021-04-20 2022-03-08 江苏乾元生物科技有限公司 一种苯嘧磺草胺的制备方法
CN115246791B (zh) * 2021-04-26 2024-11-05 内蒙古世杰化工有限公司 一种合成6-三氟甲基尿嘧啶的方法及其中间体
CN114478326B (zh) * 2022-01-21 2023-10-03 安徽宁亿泰科技有限公司 一种苯嘧磺草胺关键中间体的合成方法
AR132221A1 (es) 2023-03-30 2025-06-04 Adama Agan Ltd Proceso para la preparación de derivados de sulfamida

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NL175521C (nl) * 1973-04-26 1984-11-16 Hoechst Ag Werkwijze voor het bereiden van carbonzuurchloriden.
DE2933148A1 (de) * 1979-08-16 1981-02-26 Bayer Ag Verfahren zur herstellung von aromatischen dicarbonsaeuredichloriden iv
DE3040295A1 (de) * 1980-10-25 1982-06-03 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von aromatischen carbonsaeurechloriden
JPS61155350A (ja) 1984-12-28 1986-07-15 Ihara Nikkei Kagaku Kogyo Kk 脂肪酸クロライド及び芳香族酸クロライドの製造方法
JPH02501388A (ja) * 1987-09-23 1990-05-17 チバ　―　ガイギー　アクチエンゲゼルシャフト 複素環式化合物
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GEP20063931B (en) * 2000-05-04 2006-10-10 Basf Aktiengescellschaft Uracil substituted phenyl sulfamoyl carboxamides
JP2004535446A (ja) 2001-06-26 2004-11-25 ブリストル−マイヤーズ　スクイブ　カンパニー ＴＮＦ−α発現のＮ−ヘテロ環阻害剤
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KR101238470B1 (ko) * 2004-07-22 2013-03-04 바스프 에스이 3-페닐(티오)우라실 및 디티오우라실의 제조 방법
JP2006083133A (ja) * 2004-09-17 2006-03-30 Sankyo Co Ltd スルファミド誘導体医薬組成物
ITMI20050275A1 (it) 2005-02-22 2006-08-23 Miteni Spa Procedimento per la preparazione di derivati dell'acido benzoico attraverso un nuovo intermedio di sintesi
CN101180277B (zh) * 2005-05-24 2011-07-06 巴斯福股份公司 生产1-烷基-3-苯基尿嘧啶的方法
CA2821516A1 (en) * 2005-12-01 2007-06-07 Basf Se Process for producing fluorinated m-nitrobenzoyl chlorides

Also Published As

Publication number Publication date
IL204595A0 (en) 2010-11-30
IL204595A (en) 2014-03-31
BRPI0818408B1 (pt) 2024-01-09
EP2200978A1 (de) 2010-06-30
MX2010003148A (es) 2010-04-01
US20100222586A1 (en) 2010-09-02
BRPI0818408A2 (pt) 2015-09-15
JP2011500536A (ja) 2011-01-06
CN101821233A (zh) 2010-09-01
WO2009050120A1 (de) 2009-04-23
JP5465672B2 (ja) 2014-04-09
US9920002B2 (en) 2018-03-20
AR068849A1 (es) 2009-12-09
CN101821233B (zh) 2016-06-29

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Legal Events

Date Code Title Description
B15K Others concerning applications: alteration of classification

Free format text: AS CLASSIFICACOES ANTERIORES ERAM: C07C 303/34 , C07C 307/06 , C07D 239/54

Ipc: C07C 303/34 (2006.01), C07C 307/06 (2006.01), C07D

B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]
B12B Appeal against refusal [chapter 12.2 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 10/10/2008, OBSERVADAS AS CONDICOES LEGAIS. PATENTE CONCEDIDA CONFORME ADI 5.529/DF, QUE DETERMINA A ALTERACAO DO PRAZO DE CONCESSAO.