MX2009005158A - Proceso para separar fluoruro de hidrogeno a partir de corrientes de alimentacion organicas. - Google Patents
Proceso para separar fluoruro de hidrogeno a partir de corrientes de alimentacion organicas.Info
- Publication number
- MX2009005158A MX2009005158A MX2009005158A MX2009005158A MX2009005158A MX 2009005158 A MX2009005158 A MX 2009005158A MX 2009005158 A MX2009005158 A MX 2009005158A MX 2009005158 A MX2009005158 A MX 2009005158A MX 2009005158 A MX2009005158 A MX 2009005158A
- Authority
- MX
- Mexico
- Prior art keywords
- hydrogen fluoride
- chloro
- tetrafluoropropane
- trifluoropropene
- organic
- Prior art date
Links
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 title abstract 7
- 229910000040 hydrogen fluoride Inorganic materials 0.000 title abstract 7
- 238000000034 method Methods 0.000 title abstract 2
- SMCNZLDHTZESTK-UHFFFAOYSA-N 2-chloro-1,1,1,2-tetrafluoropropane Chemical compound CC(F)(Cl)C(F)(F)F SMCNZLDHTZESTK-UHFFFAOYSA-N 0.000 abstract 4
- OQISUJXQFPPARX-UHFFFAOYSA-N 2-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C(Cl)=C OQISUJXQFPPARX-UHFFFAOYSA-N 0.000 abstract 4
- 239000012044 organic layer Substances 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 239000010410 layer Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/07—Preparation of halogenated hydrocarbons by addition of hydrogen halides
- C07C17/087—Preparation of halogenated hydrocarbons by addition of hydrogen halides to unsaturated halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
- C07C19/10—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Se proporciona un proceso para purificar una corriente de alimentación orgánica que consiste en: (a) destilar una corriente de alimentación orgánica sin procesar que contenga fluoruro de hidrógeno, 2-cloro-1,1,1,2-tetrafluoropropano y cloro-3,3,3-trifluoropropeno para producir una primera corriente de destilado que contenga una composición tipo azeótropo de 2-cloro-1,1,1,2-tetrafluoropropano, 2-cloro-3,3,3-trifluoropropeno y fluoruro de hidrógeno, y una primera corriente de residuos rica en fluoruro de hidrógeno; (b) enfriar la primera corriente de destilado para producir una composición intermedia que contenga una capa orgánica rica en 2-cloro-1,1,1,2-tetrafluoroprop ano y 2-cloro-3,3,3-trifluoropropeno, y una capa ácida rica en fluoruro de hidrógeno; y, opcional pero preferentemente, (c) destilar la capa orgánica para producir una segunda corriente de destilado que contenga una composición tipo azeótorpo de 2-cloro-1,1,1,2-tetrafluoropropano, 2-cloro-3,3,3-trifluoropropeno y fluoruro de hidrógeno, y una segunda corriente de residuos que contenga una corriente de alimentación orgánica purificada considerablemente libre de fluoruro de hidrógeno.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US5351808P | 2008-05-15 | 2008-05-15 | |
| US12/464,666 US8168837B2 (en) | 2008-05-15 | 2009-05-12 | Process for separating hydrogen fluoride from organic feedstocks |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2009005158A true MX2009005158A (es) | 2009-12-18 |
Family
ID=40940406
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2009005158A MX2009005158A (es) | 2008-05-15 | 2009-05-14 | Proceso para separar fluoruro de hidrogeno a partir de corrientes de alimentacion organicas. |
Country Status (7)
| Country | Link |
|---|---|
| US (3) | US8168837B2 (es) |
| EP (1) | EP2119692B1 (es) |
| JP (1) | JP5491069B2 (es) |
| KR (1) | KR101629908B1 (es) |
| CN (1) | CN101684060B (es) |
| ES (1) | ES2428904T3 (es) |
| MX (1) | MX2009005158A (es) |
Families Citing this family (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9493384B2 (en) | 2007-07-06 | 2016-11-15 | Honeywell International Inc. | Process for producing 2,3,3,3-tetrafluoropropene |
| US8845921B2 (en) * | 2008-04-09 | 2014-09-30 | Honeywell International Inc. | Separation of close boiling compounds by addition of a third compound |
| US8975454B2 (en) | 2008-07-31 | 2015-03-10 | Honeywell International Inc. | Process for producing 2,3,3,3-tetrafluoropropene |
| US8252965B2 (en) * | 2008-08-22 | 2012-08-28 | Honeywell International Inc. | Method for separating halocarbons |
| US8008243B2 (en) * | 2008-10-31 | 2011-08-30 | Honeywell International Inc. | Azeotrope-like compositions of 1,1,2,3-tetrachloropropene and hydrogen fluoride |
| US9061958B2 (en) | 2009-03-24 | 2015-06-23 | Arkema Inc. | Separation of R-1233 from hydrogen fluoride |
| WO2010111067A1 (en) | 2009-03-24 | 2010-09-30 | Arkema Inc. | Separation of r-1233 from hydrogen fluoride |
| CN102596868A (zh) * | 2009-11-10 | 2012-07-18 | 大金工业株式会社 | 纯化2,3,3,3-四氟丙烯的方法 |
| CA3016991C (en) * | 2009-12-22 | 2020-10-27 | E. I. Du Pont De Nemours And Company | Compositions comprising 2,3,3,3-tetrafluoropropene, 1,1,2,3-tetrachloropropene, 2-chloro-3,3,3-trifluoropropene, or 2-chloro-1,1,1,2-tetrafluoropropane |
| US8927791B2 (en) * | 2010-04-29 | 2015-01-06 | Honeywell International Inc. | Method for producing tetrafluoropropenes |
| US8378158B2 (en) * | 2010-12-03 | 2013-02-19 | Honeywell International Inc. | Azeotrope-like compositions of (Z)-1-chloro-3,3,3-trifluoropropene and hydrogen fluoride |
| US9000240B2 (en) | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
| FR2977584B1 (fr) * | 2011-07-08 | 2014-12-05 | Arkema France | Procede de separation et recuperation du 2,3,3,3-tetrafluoropropene et de l'acide fluorhydrique |
| EP2755937B1 (en) * | 2011-09-15 | 2019-10-30 | Daikin Industries, Ltd. | Method for purifying chlorinated hydrocarbon |
| IN2014DN02372A (es) * | 2011-09-30 | 2015-05-15 | Honeywell Int Inc | |
| WO2013067356A1 (en) * | 2011-11-04 | 2013-05-10 | Haiyou Wang | Process for producing 2,3,3,3-tetrafluoropropene |
| JP6224622B2 (ja) * | 2012-01-09 | 2017-11-01 | ザ ケマーズ カンパニー エフシー リミテッド ライアビリティ カンパニー | 反応器パッシベーションのための方法 |
| IN2014DN06917A (es) * | 2012-02-10 | 2015-05-15 | Haiyou Wang | |
| JP6360439B2 (ja) * | 2012-02-29 | 2018-07-18 | ハネウェル・インターナショナル・インコーポレーテッドHoneywell International Inc. | 2,3,3,3−テトラフルオロプロペンの生産方法 |
| US9018428B2 (en) | 2012-09-06 | 2015-04-28 | Honeywell International Inc. | Reactor and agitator useful in a process for making 1-chloro-3,3,3-trifluoropropene |
| CN102974114B (zh) * | 2012-12-18 | 2014-10-29 | 上海试四化学品有限公司 | 一种二氯乙烷蒸馏装置以及蒸馏工艺 |
| US9334206B2 (en) * | 2013-03-15 | 2016-05-10 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
| FR3003565B1 (fr) | 2013-03-20 | 2018-06-29 | Arkema France | Composition comprenant hf et 2,3,3,3-tetrafluoropropene |
| JP2016523965A (ja) * | 2013-07-12 | 2016-08-12 | アーケマ・インコーポレイテッド | 膜を使用して有機フッ素化合物を分離する方法 |
| CN103613481B (zh) * | 2013-11-01 | 2015-08-12 | 西安近代化学研究所 | 氟化氢和2-氯-1,1,1-三氟丙烯混合物的分离方法 |
| EP3984986A1 (en) | 2015-05-21 | 2022-04-20 | The Chemours Company FC, LLC | Hydrofluorination of 1233xf to 244bb by sbf5 |
| JP6052340B2 (ja) * | 2015-05-29 | 2016-12-27 | ダイキン工業株式会社 | 含フッ素化合物含有組成物の製造方法 |
| CN108251895A (zh) * | 2016-12-29 | 2018-07-06 | 江苏鲁汶仪器有限公司 | 一种氟化氢气相腐蚀设备及方法 |
| US10351494B1 (en) * | 2018-01-08 | 2019-07-16 | Honeywell International Inc. | Systems and methods for reducing the formation of impurities during 244bb dehydrochlorination to 1234yf |
| CN112313199A (zh) | 2018-06-06 | 2021-02-02 | 霍尼韦尔国际公司 | 用于HCFC-244bb的脱氯化氢以制备HFO-1234yf的方法 |
| FR3100461B1 (fr) * | 2019-09-06 | 2021-09-03 | Arkema France | Procédé de purification d’hydrofluorocarbures |
| CN113735063B (zh) * | 2021-09-26 | 2023-04-18 | 金宏气体股份有限公司 | 一种9n电子级hf的提纯装置及提纯工艺 |
| US20230234901A1 (en) * | 2022-01-26 | 2023-07-27 | Honeywell International Inc. | Preparation of an improved composition from 1-chloro-3,3,3-trifluoropropene (hfo-1233zd) high boiling residue by-product |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5918481A (en) * | 1997-11-20 | 1999-07-06 | Alliedsignal Inc. | Process for separating hydrogen fluoride from fluorocarbons |
| EP1395535B1 (en) * | 2001-01-25 | 2008-08-13 | Honeywell International, Inc. | Process for the manufacture of fluorocarbons |
| US20090182179A1 (en) | 2008-01-15 | 2009-07-16 | Honeywell International Inc. | Hydrofluorination of 2-chloro-3,3,3-trifluoropropene to 2-chloro-1,1,1,2-tetrafluoropropane with catalysts of sbcl3, sbcl5, sbf5, ticl4, sncl4, cr2o3 and fluorinated cr2o3 |
| US8084653B2 (en) * | 2004-04-29 | 2011-12-27 | Honeywell International, Inc. | Method for producing fluorinated organic compounds |
| US7897823B2 (en) * | 2004-10-29 | 2011-03-01 | E. I. Du Pont De Nemours And Company | Process for production of azeotrope compositions comprising hydrofluoroolefin and hydrogen fluoride and uses of said azeotrope compositions in separation processes |
| US20080030615A1 (en) * | 2005-06-29 | 2008-02-07 | Maximino Vasquez | Techniques to switch between video display modes |
| US7476771B2 (en) * | 2005-11-01 | 2009-01-13 | E.I. Du Pont De Nemours + Company | Azeotrope compositions comprising 2,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof |
| EP3336074B1 (en) * | 2006-01-03 | 2025-07-09 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
| RU2466979C2 (ru) * | 2006-08-24 | 2012-11-20 | Е.И.Дюпон Де Немур Энд Компани | Способ отделения фторолефинов от фтороводорода путем азеотропной дистилляции |
| US8076521B2 (en) * | 2007-06-27 | 2011-12-13 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
| SG10202111316SA (en) * | 2008-05-07 | 2021-11-29 | Du Pont | Compositions comprising 2,3-dichloro-1,1,1-trifluoropropane, 2-chloro-1,1,1-trifluoropropene, 2 chloro-1,1,1,2-tetrafluoropropane or 2,3,3,3-tetrafluoropropene |
-
2009
- 2009-05-12 US US12/464,666 patent/US8168837B2/en active Active
- 2009-05-13 EP EP09160188.0A patent/EP2119692B1/en active Active
- 2009-05-13 ES ES09160188T patent/ES2428904T3/es active Active
- 2009-05-14 MX MX2009005158A patent/MX2009005158A/es active IP Right Grant
- 2009-05-14 CN CN200910149754.2A patent/CN101684060B/zh active Active
- 2009-05-15 JP JP2009118184A patent/JP5491069B2/ja active Active
- 2009-05-15 KR KR1020090042786A patent/KR101629908B1/ko active Active
-
2012
- 2012-03-19 US US13/423,726 patent/US8519201B2/en active Active
-
2013
- 2013-08-02 US US13/957,560 patent/US8716538B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN101684060A (zh) | 2010-03-31 |
| CN101684060B (zh) | 2014-04-02 |
| US8716538B2 (en) | 2014-05-06 |
| US8168837B2 (en) | 2012-05-01 |
| EP2119692B1 (en) | 2013-07-24 |
| US8519201B2 (en) | 2013-08-27 |
| JP5491069B2 (ja) | 2014-05-14 |
| US20130338408A1 (en) | 2013-12-19 |
| ES2428904T3 (es) | 2013-11-12 |
| KR20090119743A (ko) | 2009-11-19 |
| US20090287027A1 (en) | 2009-11-19 |
| KR101629908B1 (ko) | 2016-06-13 |
| JP2009298781A (ja) | 2009-12-24 |
| US20120190901A1 (en) | 2012-07-26 |
| EP2119692A1 (en) | 2009-11-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |