MX2007008981A - Procedimiento para preparar ciclohexanona y ciclohexanol. - Google Patents
Procedimiento para preparar ciclohexanona y ciclohexanol.Info
- Publication number
- MX2007008981A MX2007008981A MX2007008981A MX2007008981A MX2007008981A MX 2007008981 A MX2007008981 A MX 2007008981A MX 2007008981 A MX2007008981 A MX 2007008981A MX 2007008981 A MX2007008981 A MX 2007008981A MX 2007008981 A MX2007008981 A MX 2007008981A
- Authority
- MX
- Mexico
- Prior art keywords
- mixture
- cyclohexanol
- phase
- organic
- degree
- Prior art date
Links
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 title abstract 6
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000000203 mixture Substances 0.000 abstract 6
- 239000008346 aqueous phase Substances 0.000 abstract 4
- 239000012074 organic phase Substances 0.000 abstract 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- FGGJBCRKSVGDPO-UHFFFAOYSA-N hydroperoxycyclohexane Chemical compound OOC1CCCCC1 FGGJBCRKSVGDPO-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/385—Saturated compounds containing a keto group being part of a ring
- C07C49/403—Saturated compounds containing a keto group being part of a ring of a six-membered ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
- C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
- C07C45/53—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of hydroperoxides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La presente invencion se refiere a un procedimiento para preparar ciclohexanona y ciclohexanol, comprendiendo dicho procedimiento (a) neutralizar acidos y/o dioxido de carbono presentes en una disolucion organica que comprende ademas hidroperoxido de ciclohexilo mezclando la disolucion organica con una primera disolucion acuosa basica a una temperatura de desde 50 hasta 80 degree C para formar una primera mezcla que comprende una primera fase acuosa con un pH de desde 8.5 hasta 13 y una primera fase organica, (b) separar la primera fase acuosa de la primera mezcla dando como resultado una mezcla restante que comprende la primera fase organica, (c) descomponer el hidroperoxido de ciclohexilo presente en dicha mezcla restante mezclando dicha mezcla restante con una segunda disolucion acuosa basica a una temperatura de desde 60 hasta 110 degree C para formar una segunda mezcla que comprende una segunda fase acuosa y una segunda fase organica que comprende ciclohexanona y ciclohexanol, (d) separar la segunda fase acuosa de la segunda fase organica a una temperatura superior a 80 degree C.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP05075184 | 2005-01-25 | ||
| EP05075185 | 2005-01-25 | ||
| PCT/EP2006/001003 WO2006079562A1 (en) | 2005-01-25 | 2006-01-17 | Process for preparing cyclohexanone and cyclohexanol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2007008981A true MX2007008981A (es) | 2007-09-21 |
Family
ID=36092208
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2007008983A MX2007008983A (es) | 2005-01-25 | 2006-01-17 | Procedimiento para preparar ciclohexanona y ciclohexanol. |
| MX2007008981A MX2007008981A (es) | 2005-01-25 | 2006-01-17 | Procedimiento para preparar ciclohexanona y ciclohexanol. |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2007008983A MX2007008983A (es) | 2005-01-25 | 2006-01-17 | Procedimiento para preparar ciclohexanona y ciclohexanol. |
Country Status (15)
| Country | Link |
|---|---|
| US (2) | US7619122B2 (es) |
| EP (2) | EP1841720B1 (es) |
| JP (2) | JP2008528537A (es) |
| KR (2) | KR101310409B1 (es) |
| CN (2) | CN101107210B (es) |
| AT (1) | ATE426586T1 (es) |
| BR (2) | BRPI0607369A2 (es) |
| DE (1) | DE602006005898D1 (es) |
| EA (2) | EA014018B1 (es) |
| ES (1) | ES2684413T3 (es) |
| MX (2) | MX2007008983A (es) |
| MY (2) | MY145594A (es) |
| PL (1) | PL1841721T3 (es) |
| TW (2) | TWI365867B (es) |
| WO (2) | WO2006079562A1 (es) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101310409B1 (ko) * | 2005-01-25 | 2013-09-23 | 디에스엠 아이피 어셋츠 비.브이. | 사이클로헥산온 및 사이클로헥산올의 제조 방법 |
| US8304584B2 (en) | 2007-06-27 | 2012-11-06 | H R D Corporation | Method of making alkylene glycols |
| US7491856B2 (en) | 2007-06-27 | 2009-02-17 | H R D Corporation | Method of making alkylene glycols |
| US7592493B2 (en) * | 2007-06-27 | 2009-09-22 | H R D Corporation | High shear process for cyclohexanol production |
| TW200944497A (en) * | 2008-04-17 | 2009-11-01 | China Petrochemical Dev Corp | System and method for producing naphthenone |
| RU2458903C1 (ru) * | 2010-12-23 | 2012-08-20 | Открытое акционерное общество "Щекиноазот" | Способ получения циклогексанона и циклогексанола и установка для его осуществления |
| CN102627525B (zh) * | 2012-03-31 | 2013-12-25 | 肖藻生 | 一种环己烷氧化制备环己醇和环己酮的生产工艺 |
| CN104557497A (zh) * | 2013-10-09 | 2015-04-29 | 中国石油化工股份有限公司 | 一种提高环己基过氧化氢分解酮醇比的方法 |
| CN105646141A (zh) * | 2014-11-11 | 2016-06-08 | 中国科学院大连化学物理研究所 | 一种碱液循环用无过环己烷氧化液脱酸的方法 |
| WO2017099072A1 (ja) | 2015-12-07 | 2017-06-15 | 宇部興産株式会社 | ケトン及び／又はアルコールの製造方法及びそのシステム |
| CN107778133B (zh) * | 2016-08-25 | 2021-05-07 | 中国石油化工股份有限公司 | 一种制备环己醇和环己酮的方法 |
| CN107778131B (zh) * | 2016-08-25 | 2021-02-05 | 中国石油化工股份有限公司 | 一种基于多层双环流导流筒鼓泡反应器制备环己醇和环己酮的方法 |
| CN107778132B (zh) * | 2016-08-25 | 2021-02-05 | 中国石油化工股份有限公司 | 一种基于多层导流筒鼓泡反应器制备环己醇和环己酮的方法 |
| CN109180444B (zh) * | 2018-09-05 | 2021-07-16 | 上海交通大学 | 使用二氧化碳加速氢化芳香化合物合成环己酮的方法 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US768292A (en) | 1904-04-01 | 1904-08-23 | George Josiph Miller | Animal-trap. |
| NL288272A (es) | 1963-01-28 | |||
| DE2650892C3 (de) * | 1976-11-06 | 1980-05-29 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Aufarbeitung von Cyclohexanol und Cyclohexanon enthaltenden Reaktionsgemischen |
| NL7802125A (nl) * | 1978-02-25 | 1979-08-28 | Stamicarbon | Werkwijze voor het bereiden van cycloalkanolen en cycloalkanonen. |
| NL8201695A (nl) | 1982-04-23 | 1983-11-16 | Stamicarbon | Werkwijze voor de bereiding van cyclohexanol en cyclohexanon. |
| US4874901A (en) | 1988-05-06 | 1989-10-17 | Boc, Inc. | Process for the production of polyfluorinated ethers |
| JPH0819019B2 (ja) | 1991-07-16 | 1996-02-28 | 三菱化学株式会社 | シクロヘキサンの酸化反応混合物の処理法 |
| JPH05250069A (ja) | 1992-03-09 | 1993-09-28 | Funai Electric Co Ltd | トラックボール付入力装置 |
| JP2500977B2 (ja) * | 1992-03-24 | 1996-05-29 | 三菱化学株式会社 | シクロヘキサノンの製造方法 |
| BE1007904A3 (nl) * | 1993-12-23 | 1995-11-14 | Dsm Nv | Werkwijze voor de bereiding van een alkanol en/of een alkanon. |
| BE1009662A3 (nl) * | 1995-10-13 | 1997-06-03 | Dsm Nv | Werkwijze voor het ontleden van cycloalkylhydroperoxide. |
| JP2002128714A (ja) * | 2000-10-17 | 2002-05-09 | Sumitomo Chem Co Ltd | シクロヘキサンの酸化方法 |
| US6700022B2 (en) * | 2002-06-05 | 2004-03-02 | E. I. Du Pont De Nemours And Company | High yield cyclohexyl hydroperoxide decompostition process |
| KR101310409B1 (ko) * | 2005-01-25 | 2013-09-23 | 디에스엠 아이피 어셋츠 비.브이. | 사이클로헥산온 및 사이클로헥산올의 제조 방법 |
-
2006
- 2006-01-17 KR KR1020077019271A patent/KR101310409B1/ko not_active Expired - Lifetime
- 2006-01-17 BR BRPI0607369-7A patent/BRPI0607369A2/pt not_active IP Right Cessation
- 2006-01-17 EA EA200701581A patent/EA014018B1/ru not_active IP Right Cessation
- 2006-01-17 AT AT06700970T patent/ATE426586T1/de not_active IP Right Cessation
- 2006-01-17 WO PCT/EP2006/001003 patent/WO2006079562A1/en not_active Ceased
- 2006-01-17 EP EP06700970A patent/EP1841720B1/en not_active Revoked
- 2006-01-17 EA EA200701580A patent/EA011023B1/ru not_active IP Right Cessation
- 2006-01-17 DE DE602006005898T patent/DE602006005898D1/de not_active Expired - Lifetime
- 2006-01-17 ES ES06706658.9T patent/ES2684413T3/es not_active Expired - Lifetime
- 2006-01-17 PL PL06706658T patent/PL1841721T3/pl unknown
- 2006-01-17 MX MX2007008983A patent/MX2007008983A/es active IP Right Grant
- 2006-01-17 MX MX2007008981A patent/MX2007008981A/es active IP Right Grant
- 2006-01-17 JP JP2007552605A patent/JP2008528537A/ja not_active Ceased
- 2006-01-17 EP EP06706658.9A patent/EP1841721B1/en not_active Expired - Lifetime
- 2006-01-17 WO PCT/EP2006/000521 patent/WO2006079485A1/en not_active Ceased
- 2006-01-17 CN CN2006800031179A patent/CN101107210B/zh not_active Expired - Fee Related
- 2006-01-17 KR KR1020077019268A patent/KR20070110299A/ko not_active Ceased
- 2006-01-17 US US11/795,563 patent/US7619122B2/en not_active Expired - Fee Related
- 2006-01-17 BR BRPI0607224-0A patent/BRPI0607224A2/pt not_active IP Right Cessation
- 2006-01-17 US US11/795,868 patent/US7642384B2/en not_active Expired - Fee Related
- 2006-01-17 CN CN2006800031164A patent/CN101107209B/zh not_active Expired - Fee Related
- 2006-01-17 JP JP2007552558A patent/JP2008528528A/ja active Pending
- 2006-01-23 MY MYPI20060279A patent/MY145594A/en unknown
- 2006-01-23 MY MYPI20060278A patent/MY144617A/en unknown
- 2006-01-24 TW TW095102609A patent/TWI365867B/zh not_active IP Right Cessation
- 2006-01-24 TW TW095102611A patent/TWI365868B/zh not_active IP Right Cessation
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |