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WO2009047867A1 - 硬質皮膜被覆部材、及びその製造方法 - Google Patents

硬質皮膜被覆部材、及びその製造方法 Download PDF

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Publication number
WO2009047867A1
WO2009047867A1 PCT/JP2007/069993 JP2007069993W WO2009047867A1 WO 2009047867 A1 WO2009047867 A1 WO 2009047867A1 JP 2007069993 W JP2007069993 W JP 2007069993W WO 2009047867 A1 WO2009047867 A1 WO 2009047867A1
Authority
WO
WIPO (PCT)
Prior art keywords
coating film
hard coating
plane
group
peak intensity
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2007/069993
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English (en)
French (fr)
Inventor
Kazuyuki Kubota
Hitoshi Ohnuma
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Moldino Tool Engineering Ltd
Original Assignee
Hitachi Tool Engineering Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=40549023&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=WO2009047867(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Hitachi Tool Engineering Ltd filed Critical Hitachi Tool Engineering Ltd
Priority to US12/682,535 priority Critical patent/US8304098B2/en
Priority to JP2009536907A priority patent/JP5246165B2/ja
Priority to KR1020107010319A priority patent/KR101200785B1/ko
Priority to PCT/JP2007/069993 priority patent/WO2009047867A1/ja
Priority to EP07829729.8A priority patent/EP2208560B2/en
Priority to CN2007801010615A priority patent/CN101855035B/zh
Publication of WO2009047867A1 publication Critical patent/WO2009047867A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24Vacuum evaporation
    • C23C14/32Vacuum evaporation by explosion; by evaporation and subsequent ionisation of the vapours, e.g. ion-plating
    • C23C14/325Electric arc evaporation
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/06Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
    • C23C14/0641Nitrides
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/06Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
    • C23C14/0664Carbonitrides
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/06Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
    • C23C14/0676Oxynitrides
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C30/00Coating with metallic material characterised only by the composition of the metallic material, i.e. not characterised by the coating process
    • C23C30/005Coating with metallic material characterised only by the composition of the metallic material, i.e. not characterised by the coating process on hard metal substrates
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/24Structurally defined web or sheet [e.g., overall dimension, etc.]
    • Y10T428/24479Structurally defined web or sheet [e.g., overall dimension, etc.] including variation in thickness
    • Y10T428/24612Composite web or sheet
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/26Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/26Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
    • Y10T428/263Coating layer not in excess of 5 mils thick or equivalent
    • Y10T428/264Up to 3 mils
    • Y10T428/2651 mil or less

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Cutting Tools, Boring Holders, And Turrets (AREA)
  • Physical Vapour Deposition (AREA)
  • Ceramic Products (AREA)

Abstract

 本発明の硬質皮膜被覆部材は、圧縮応力を有する厚さ5μm以上の硬質皮膜が被覆された部材であって、前記硬質皮膜が組成式:(Me1-aXa)α(N1-x-yCxOy)[ただし、Meは4a、5a、6a族からなる群から選ばれた少なくとも一種の元素であり、XはAl、Si、B、Sからなる群から選ばれた少なくとも一種の元素であり、a,x,yはそれぞれX、C、Oの含有量(原子比)を表し、αは(Me1-aXa)と(N1-x-yCxOy)との比を表し、0.1≦a≦0.65,0≦x≦0.1,0≦y≦0.1及び0.85≦α≦1.25を満たす。]で表される面心立方構造を有し、前記硬質皮膜のX線回折における(111)面のピーク強度Ir、(200)面のピーク強度Is及び(220)面のピーク強度Itが、2≦Is/Ir及び0.2≦It/Ir≦1を満たし、(200)面の半価幅W(°)が、W≦0.7であることを特徴とする。
PCT/JP2007/069993 2007-10-12 2007-10-12 硬質皮膜被覆部材、及びその製造方法 Ceased WO2009047867A1 (ja)

Priority Applications (6)

Application Number Priority Date Filing Date Title
US12/682,535 US8304098B2 (en) 2007-10-12 2007-10-12 Hard-coated member, and its production method
JP2009536907A JP5246165B2 (ja) 2007-10-12 2007-10-12 硬質皮膜被覆部材の製造方法
KR1020107010319A KR101200785B1 (ko) 2007-10-12 2007-10-12 경질 피막 피복 부재, 및 그 제조 방법
PCT/JP2007/069993 WO2009047867A1 (ja) 2007-10-12 2007-10-12 硬質皮膜被覆部材、及びその製造方法
EP07829729.8A EP2208560B2 (en) 2007-10-12 2007-10-12 Process for the production of the member covered with hard coating
CN2007801010615A CN101855035B (zh) 2007-10-12 2007-10-12 被覆有硬质被膜的部件及其制造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/JP2007/069993 WO2009047867A1 (ja) 2007-10-12 2007-10-12 硬質皮膜被覆部材、及びその製造方法

Publications (1)

Publication Number Publication Date
WO2009047867A1 true WO2009047867A1 (ja) 2009-04-16

Family

ID=40549023

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2007/069993 Ceased WO2009047867A1 (ja) 2007-10-12 2007-10-12 硬質皮膜被覆部材、及びその製造方法

Country Status (6)

Country Link
US (1) US8304098B2 (ja)
EP (1) EP2208560B2 (ja)
JP (1) JP5246165B2 (ja)
KR (1) KR101200785B1 (ja)
CN (1) CN101855035B (ja)
WO (1) WO2009047867A1 (ja)

Cited By (18)

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JP2012011393A (ja) * 2010-06-29 2012-01-19 Kobe Steel Ltd せん断用金型及びその製造方法
US20120247141A1 (en) * 2010-01-14 2012-10-04 Carrier Corporation Reciprocating Refrigeration Compressor Oil Sealing
JP2014505369A (ja) * 2011-02-01 2014-02-27 エーエスエムエル ネザーランズ ビー.ブイ. 基板テーブル、リソグラフィ装置、およびデバイス製造方法
JP2014145114A (ja) * 2013-01-29 2014-08-14 Kobe Steel Ltd 軟質金属に対する耐凝着性に優れた硬質皮膜
WO2014129273A1 (ja) * 2013-02-21 2014-08-28 住友電工ハードメタル株式会社 表面被覆切削工具およびその製造方法
JP2014526393A (ja) * 2011-09-19 2014-10-06 ラミナ テクノロジーズ ソシエテ アノニム 被膜付き切削工具
JP2015053358A (ja) * 2013-09-06 2015-03-19 三菱マテリアル株式会社 サーミスタ用金属窒化物材料及びその製造方法並びにサーミスタセンサ
JP2016003369A (ja) * 2014-06-17 2016-01-12 住友電工ハードメタル株式会社 硬質被膜、切削工具および硬質被膜の製造方法
JP2016003368A (ja) * 2014-06-17 2016-01-12 住友電工ハードメタル株式会社 硬質被膜、切削工具および硬質被膜の製造方法
EP2463398A4 (en) * 2009-08-04 2017-04-05 Tungaloy Corporation Coated member
WO2017094440A1 (ja) * 2015-12-02 2017-06-08 三菱日立ツール株式会社 硬質皮膜、硬質皮膜被覆部材及びその製造方法、及び硬質皮膜の製造に用いるターゲット及びその製造方法
WO2018230212A1 (ja) * 2017-06-12 2018-12-20 日本特殊陶業株式会社 表面被覆切削工具
JP2019018286A (ja) * 2017-07-18 2019-02-07 三菱マテリアル株式会社 硬質被覆層がすぐれた耐摩耗性と耐チッピング性を発揮する表面被覆切削工具
WO2021193875A1 (ja) * 2020-03-27 2021-09-30 京セラ株式会社 被覆工具および切削工具
JPWO2021193876A1 (ja) * 2020-03-27 2021-09-30
JPWO2022138400A1 (ja) * 2020-12-25 2022-06-30
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