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WO2004032260A3 - Aktives nickelmischhydroxid-kathodenmaterial für alkalische akkumulatoren und verfahren zu seiner herstellung - Google Patents

Aktives nickelmischhydroxid-kathodenmaterial für alkalische akkumulatoren und verfahren zu seiner herstellung Download PDF

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Publication number
WO2004032260A3
WO2004032260A3 PCT/DE2003/003219 DE0303219W WO2004032260A3 WO 2004032260 A3 WO2004032260 A3 WO 2004032260A3 DE 0303219 W DE0303219 W DE 0303219W WO 2004032260 A3 WO2004032260 A3 WO 2004032260A3
Authority
WO
WIPO (PCT)
Prior art keywords
nickel hydroxide
material based
active material
cathode active
mixed nickel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/DE2003/003219
Other languages
English (en)
French (fr)
Other versions
WO2004032260A2 (de
Inventor
Peter Baeuerlein
Bernd Schultheis
Wolfgang Reichel
Heinz Scherzberg
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Clarios Technology and Recycling GmbH
Original Assignee
VARTA Automotive Systems GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by VARTA Automotive Systems GmbH filed Critical VARTA Automotive Systems GmbH
Priority to JP2004540514A priority Critical patent/JP2006515950A/ja
Priority to AU2003280296A priority patent/AU2003280296A1/en
Priority to EP03770891A priority patent/EP1543573A2/de
Publication of WO2004032260A2 publication Critical patent/WO2004032260A2/de
Publication of WO2004032260A3 publication Critical patent/WO2004032260A3/de
Priority to US11/088,251 priority patent/US20050221179A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/24Electrodes for alkaline accumulators
    • H01M4/32Nickel oxide or hydroxide electrodes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/04Oxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • C01P2004/53Particles with a specific particle size distribution bimodal size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/11Powder tap density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/24Alkaline accumulators
    • H01M10/30Nickel accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/34Gastight accumulators
    • H01M10/345Gastight metal hydride accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/021Physical characteristics, e.g. porosity, surface area
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

Ein aktives Nickelmischhydroxid-Kathodenmaterial, das für die Verwendung in alkalischen Akkumulatoren vorgesehen ist, besitzt eine spezielle bimodale Korngrössenverteilung, auf die die guten Eigenschaften des Nickelmischhydroxid-Kathodenmaterials zurückgeführt werden. Die Herstellung des Nickelmischhydroxid-Materials erfolgt besonders vorteilhaft in einem kontinuierlichen Fällungsprozess in einem Schlaufenreaktor, der über eine integrierte Klärzone verfügt.
PCT/DE2003/003219 2002-09-28 2003-09-26 Aktives nickelmischhydroxid-kathodenmaterial für alkalische akkumulatoren und verfahren zu seiner herstellung Ceased WO2004032260A2 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP2004540514A JP2006515950A (ja) 2002-09-28 2003-09-26 アルカリ蓄電池用の活性ニッケル混合水酸化物−カソード材料及びその製造方法
AU2003280296A AU2003280296A1 (en) 2002-09-28 2003-09-26 Cathode active material based on mixed nickel hydroxide for alkaline batteries and a process for the production thereof
EP03770891A EP1543573A2 (de) 2002-09-28 2003-09-26 Aktives nickelmischhydroxid-kathodenmaterial für alkalische akkumulatoren und verfahren zu seiner herstellung
US11/088,251 US20050221179A1 (en) 2002-09-28 2005-03-23 Active mixed nickel hydroxide cathode material for alkaline storage batteries and process for its production

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10245467.1 2002-09-28
DE10245467A DE10245467A1 (de) 2002-09-28 2002-09-28 Aktives Nickelmischhydroxid-Kathodenmaterial für alkalische Akkumulatoren und Verfahren zu seiner Herstellung

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US11/088,251 Continuation US20050221179A1 (en) 2002-09-28 2005-03-23 Active mixed nickel hydroxide cathode material for alkaline storage batteries and process for its production

Publications (2)

Publication Number Publication Date
WO2004032260A2 WO2004032260A2 (de) 2004-04-15
WO2004032260A3 true WO2004032260A3 (de) 2005-02-03

Family

ID=31984243

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DE2003/003219 Ceased WO2004032260A2 (de) 2002-09-28 2003-09-26 Aktives nickelmischhydroxid-kathodenmaterial für alkalische akkumulatoren und verfahren zu seiner herstellung

Country Status (7)

Country Link
EP (1) EP1543573A2 (de)
JP (1) JP2006515950A (de)
KR (1) KR20050073456A (de)
CN (1) CN100438152C (de)
AU (1) AU2003280296A1 (de)
DE (1) DE10245467A1 (de)
WO (1) WO2004032260A2 (de)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006265086A (ja) * 2005-02-24 2006-10-05 Toyota Motor Corp 水酸化ニッケル粒子の製造方法及び製造装置
DE102006015538A1 (de) * 2006-03-31 2007-10-11 H. C. Starck Gmbh & Co. Kg Vorrichtung und Verfahren zur Herstellung von Verbindungen durch Fällung
DE102006049107A1 (de) * 2006-10-13 2008-04-17 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in elektrochemischen Anwendungen
DE102007039471A1 (de) 2007-08-21 2009-02-26 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Lithium-Sekundärbatterien
DE102007049108A1 (de) * 2007-10-12 2009-04-16 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Batterien
JP5614334B2 (ja) * 2010-03-02 2014-10-29 住友金属鉱山株式会社 ニッケルコバルト複合水酸化物およびその製造方法、ならびに該複合水酸化物を用いて得られる非水系電解質二次電池用正極活物質
US10059602B2 (en) 2013-05-08 2018-08-28 Basf Se Process for producing suspensions
WO2017033895A1 (ja) * 2015-08-24 2017-03-02 住友金属鉱山株式会社 マンガンニッケル複合水酸化物及びその製造方法、リチウムマンガンニッケル複合酸化物及びその製造方法、並びに非水系電解質二次電池
DE102015115691B4 (de) * 2015-09-17 2020-10-01 Zentrum für Sonnenenergie- und Wasserstoff-Forschung Baden-Württemberg Gemeinnützige Stiftung Lithium-Nickel-Mangan-basierte Übergangsmetalloxidpartikel, deren Herstellung sowie deren Verwendung als Elektrodenmaterial
WO2017055977A1 (en) * 2015-09-30 2017-04-06 Umicore Precursors for lithium transition metal oxide cathode materials for rechargeable batteries
JP6911853B2 (ja) * 2016-06-14 2021-07-28 住友金属鉱山株式会社 化学反応装置、および、化学反応装置を用いた粒子の製造方法
ES2971158T3 (es) * 2019-10-01 2024-06-03 Basf Se Proceso de precipitación de un carbonato mixto o de un (oxi)hidróxido mixto
KR102555562B1 (ko) * 2020-06-15 2023-07-17 주식회사 엘 앤 에프 다성분계 금속 수산화물의 제조장치
JP2022039700A (ja) * 2020-08-28 2022-03-10 株式会社 イージーエス 金属水酸化物の製造方法、および、金属水酸化物の製造装置
CN114171727A (zh) * 2021-10-27 2022-03-11 深圳市豪鹏科技股份有限公司 一种正极材料、正极浆料、正极片及镍氢电池
DE102023114974A1 (de) * 2023-06-07 2024-12-12 K-Utec Ag Salt Technologies Vorrichtung zur Erzeugung von Lithiumkarbonat-Kristallen
WO2025016808A1 (en) * 2023-07-14 2025-01-23 Basf Se Process for making precursors of cathode active materials, and precursors

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5498403A (en) * 1994-05-20 1996-03-12 Hyundai Motor Company Method for preparing high density nickel hydroxide used for alkali rechargeable batteries
JPH1025117A (ja) * 1996-07-09 1998-01-27 Japan Metals & Chem Co Ltd 水酸化ニッケルの製造方法
DE19823129A1 (de) * 1997-08-04 1999-02-11 Samsung Display Devices Co Ltd Verfahren zur Herstellung einer hochdichten Formiermasse aus Nickelhydroxid

Family Cites Families (9)

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DE68917045T2 (de) * 1988-07-19 1995-03-16 Yuasa Battery Co Ltd Nickelelektrode für eine alkalische Batterie.
JP2805098B2 (ja) * 1990-02-27 1998-09-30 関西触媒化学株式会社 水酸化ニッケルの製造方法
US5700596A (en) * 1991-07-08 1997-12-23 Matsushita Electric Industrial Co., Ltd. Nickel hydroxide active material powder and nickel positive electrode and alkali storage battery using them
DE4342620C1 (de) * 1993-12-14 1995-07-06 Starck H C Gmbh Co Kg Verfahren zur Herstellung von Metallhydroxiden
JPH11307092A (ja) * 1998-04-17 1999-11-05 Sakai Chem Ind Co Ltd アルカリ蓄電池正極活物質用水酸化ニッケル粉末及びその製造方法
CA2374245A1 (en) * 1999-06-21 2000-12-28 Kabushiki Kaisha Toshiba Active material for anode of secondary cell and method for production thereof and non-aqueous electrolyte secondary cell, and recycled electronic functional material and method for recycling electronic functional material
JP2002093417A (ja) * 2000-09-11 2002-03-29 Mitsubishi Cable Ind Ltd Li−Co系複合酸化物、ならびにそれを用いた正極板およびリチウムイオン二次電池
JP2002184405A (ja) * 2000-12-12 2002-06-28 Matsushita Electric Ind Co Ltd アルカリ蓄電池用非焼結式ニッケル正極およびその製造方法ならびにそれを用いたアルカリ蓄電池
JP3955175B2 (ja) * 2000-12-13 2007-08-08 松下電器産業株式会社 アルカリ蓄電池用非焼結式ニッケル正極およびそれを用いたアルカリ蓄電池

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5498403A (en) * 1994-05-20 1996-03-12 Hyundai Motor Company Method for preparing high density nickel hydroxide used for alkali rechargeable batteries
JPH1025117A (ja) * 1996-07-09 1998-01-27 Japan Metals & Chem Co Ltd 水酸化ニッケルの製造方法
DE19823129A1 (de) * 1997-08-04 1999-02-11 Samsung Display Devices Co Ltd Verfahren zur Herstellung einer hochdichten Formiermasse aus Nickelhydroxid

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
PATENT ABSTRACTS OF JAPAN vol. 1998, no. 05 30 April 1998 (1998-04-30) *

Also Published As

Publication number Publication date
CN100438152C (zh) 2008-11-26
AU2003280296A1 (en) 2004-04-23
KR20050073456A (ko) 2005-07-13
AU2003280296A8 (en) 2004-04-23
DE10245467A1 (de) 2004-04-08
JP2006515950A (ja) 2006-06-08
CN1685541A (zh) 2005-10-19
EP1543573A2 (de) 2005-06-22
WO2004032260A2 (de) 2004-04-15

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