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WO1992008147A3 - Accelerateur rotatif d'echantillons pour resonance magnetique nucleaire a haute temperature - Google Patents

Accelerateur rotatif d'echantillons pour resonance magnetique nucleaire a haute temperature Download PDF

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Publication number
WO1992008147A3
WO1992008147A3 PCT/US1991/007609 US9107609W WO9208147A3 WO 1992008147 A3 WO1992008147 A3 WO 1992008147A3 US 9107609 W US9107609 W US 9107609W WO 9208147 A3 WO9208147 A3 WO 9208147A3
Authority
WO
WIPO (PCT)
Prior art keywords
strength
capsule
radial
ceramic
typically
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US1991/007609
Other languages
English (en)
Other versions
WO1992008147A2 (fr
Inventor
F David Doty
Jonathan B Spitzmesser
David Gordon Wilson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Doty Scientific Inc
Original Assignee
Doty Scientific Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Doty Scientific Inc filed Critical Doty Scientific Inc
Publication of WO1992008147A2 publication Critical patent/WO1992008147A2/fr
Publication of WO1992008147A3 publication Critical patent/WO1992008147A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
    • G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
    • G01R33/307—Sample handling arrangements, e.g. sample cells, spinning mechanisms specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer

Landscapes

  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Turbine Rotor Nozzle Sealing (AREA)
  • Ceramic Products (AREA)

Abstract

Un cylindre en céramique à paroi mince et à résistance élevée, en partie fermé à une extrémité et comprenant des aubes de turbines à entrée radiale s'adaptant dans l'extrémité en partie fermée, fournit l'entraînement rotatif, la protection de surface et la résistance à l'éclatement nécessaires pour contenir et mettre en rotation, à l'intérieur d'une bobine réceptrice/émettrice de RMN et à des vitesses de rotation élevées, une capsule en céramique molle jetable remplie d'un échantillon destiné à des expériences de RMN. Une configuration de turbine à entrée radiale améliorée permet d'obtenir une meilleure efficacité pour des micro-turbines. Un palier d'air cylindrique pour tourillon placé aux deux extrémités fournit un support et une stabilité radiales. Un palier d'air de poussée axiale est placé à l'extrémité opposée aux aubes de turbine entre le fond de protection de la capsule molle et une bague de poussée. La céramique à résistance élevée est généralement composée de zircone partiellement stabilisée ou de nitrure de silicium comprimé à chaud. La capsule jetable est généralement composée de nitrure de bore hexagonal.
PCT/US1991/007609 1990-11-01 1991-10-16 Accelerateur rotatif d'echantillons pour resonance magnetique nucleaire a haute temperature Ceased WO1992008147A2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US607,521 1984-05-07
US07/607,521 US5202633A (en) 1990-11-01 1990-11-01 High temperature nmr sample spinner

Publications (2)

Publication Number Publication Date
WO1992008147A2 WO1992008147A2 (fr) 1992-05-14
WO1992008147A3 true WO1992008147A3 (fr) 1992-06-11

Family

ID=24432630

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1991/007609 Ceased WO1992008147A2 (fr) 1990-11-01 1991-10-16 Accelerateur rotatif d'echantillons pour resonance magnetique nucleaire a haute temperature

Country Status (4)

Country Link
US (2) US5202633A (fr)
EP (1) EP0555408A1 (fr)
AU (1) AU8913691A (fr)
WO (1) WO1992008147A2 (fr)

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US5202633A (en) * 1990-11-01 1993-04-13 Doty Scientific, Inc. High temperature nmr sample spinner
WO1992015023A1 (fr) * 1991-02-25 1992-09-03 Doty Scientific, Inc. Systeme de rotation supersonique d'echantillon
US5289130A (en) * 1992-07-31 1994-02-22 Doty Scientific Inc. NMR sample rotor cooling technique
US5932940A (en) 1996-07-16 1999-08-03 Massachusetts Institute Of Technology Microturbomachinery
US5811201A (en) * 1996-08-16 1998-09-22 Southern California Edison Company Power generation system utilizing turbine and fuel cell
US6320384B1 (en) * 1996-12-23 2001-11-20 David F. Doty Thermal buffering of cross-coils in high-power NMR decoupling
US5886525A (en) * 1997-03-17 1999-03-23 The United States Of America As Represented By The Secretary Of The Navy Apparatus and method for performing NMR spectroscopy on solid sample by rotation
US6054857A (en) * 1997-03-18 2000-04-25 Doty Scientific, Inc. NMR MAS sealing sample cells and methods
US5867864A (en) * 1997-05-02 1999-02-09 The Hoover Company Hand held turbine powered extractor nozzle
US6510585B2 (en) 2000-01-14 2003-01-28 Royal Appliance Mfg. Co. Turbo tool
JP2003177172A (ja) * 2001-10-03 2003-06-27 Jeol Ltd 固体ｎｍｒ測定用高速スピナー
WO2003106828A2 (fr) * 2002-06-18 2003-12-24 Ingersoll-Rand Energy Systems Corporation Systeme de moteur a microturbine
EE00582U1 (et) * 2004-04-20 2006-01-16 Keemilise ja Bioloogilise Füüsika Instituut Kõrge lahutusega madaltemperatuurne tahke keha tuumamagnetresonantsi mõõtepea
US7170292B2 (en) * 2004-10-20 2007-01-30 Doty Scientific, Inc. NMR MAS inflow bernoulli bearing
WO2006085261A2 (fr) * 2005-02-10 2006-08-17 Doty Scientific, Inc. Sonde cryomas rmn pour aimants large trou a champ eleve
US7196521B2 (en) * 2005-03-29 2007-03-27 Doty Scientific, Inc. NMR MAS electret spin rate detection
US7541807B2 (en) * 2007-07-19 2009-06-02 Varian, Inc. Rotor drive apparatus and methods utilizing center-fed radial-outflow gas
US9448291B2 (en) * 2011-10-04 2016-09-20 Pressure Biosciences, Inc. High pressure sample containment system for electromagnetic measurements
US9063060B2 (en) 2011-10-10 2015-06-23 Jeol Resonance Inc. Solid-state NMR spectrometer, sample holder therefor, and method of solid-state NMR spectroscopy
US9151813B2 (en) 2012-08-08 2015-10-06 Battelle Memorial Institute High-pressure, high-temperature magic angle spinning nuclear magnetic resonance devices and processes for making and using same
JP5953633B2 (ja) 2012-10-09 2016-07-20 日本電子株式会社 Ｎｍｒ測定用スピナ
US9062904B2 (en) 2012-10-23 2015-06-23 Doty Scientific, Inc. Stabilizing control of a saturated cold gas stream
KR102106903B1 (ko) * 2014-03-12 2020-05-06 허친슨 전기 발생 장치를 구비한 유압 진동 방지 장치 및 이러한 진동 방지 장치를 위한 전기 발생 장치
US10281416B2 (en) * 2014-08-04 2019-05-07 Waters Technologies Corporation Devices for use in solid-state NMR analysis
FR3033049B1 (fr) * 2015-02-19 2019-07-12 Commissariat A L'energie Atomique Et Aux Energies Alternatives Procede et dispositif de controle de la temperature d'un flux de fluide destine a etre utilise par une sonde d'analyse par rmn, systeme d'analyse rmn correspondant
DE202015105448U1 (de) * 2015-10-14 2017-01-17 Bruker Biospin Gmbh Turbinenkappe, zugehöriger NMR-MAS-Rotor und zugehöriger NMR-MAS-Stator, insbesondere mit einem 0,7 mm Rotor-Röhrchen
DE102017220709B4 (de) * 2017-11-20 2019-05-29 Bruker Biospin Ag MAS-NMR-Rotorsystem mit verbesserter Raumnutzung
DE102019202001B3 (de) * 2019-02-14 2020-06-25 Bruker Biospin Gmbh MAS-Probenkopf mit thermisch isolierter Probenkammer
US11137458B2 (en) 2019-05-29 2021-10-05 Battelle Memorial Institute High-temperature NMR MAS probe with optimized temperature gradient across sample rotor
WO2025046415A1 (fr) 2023-09-01 2025-03-06 Doty Scientific Inc. Sonde rmn pour fonctionnement mas-dnp efficace à des températures ultra-basses

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GB1271262A (en) * 1969-05-23 1972-04-19 Cmw Lab Ltd Turbines
US3681683A (en) * 1970-09-14 1972-08-01 Varian Associates Gyromagnetic resonance spectrometer utilizing an improved sample spinning and ejecting structure
US4088944A (en) * 1976-10-04 1978-05-09 Varian Associates, Inc. NMR Spectrometer employing self centering turbine
US4254373A (en) * 1977-06-03 1981-03-03 Lippmaa Endel T Sensor for generating nuclear magnetic resonance signals
EP0073667A2 (fr) * 1981-08-31 1983-03-09 Monsanto Company Dispositif porte-échantillon tournant pour spectromètre à résonance magnétique nucléaire
US4456882A (en) * 1982-01-04 1984-06-26 University Of South Carolina High speed cylindrical nuclear magnetic resonance (NMR) sample spinner
US4739270A (en) * 1986-06-03 1988-04-19 Varian Associates, Inc. High speed spinner for NMR spectrometer
US4806868A (en) * 1987-11-13 1989-02-21 Varian Associates, Inc. NMR spinner speed control
US4859949A (en) * 1988-01-26 1989-08-22 Siemens Aktiengesellschaft Magnetic resonance spectroscopy apparatus
FR2628214A1 (fr) * 1988-03-01 1989-09-08 Sadis Bruker Spectrospin Sa Sonde pour mesures spectrometriques de resonances magnetiques aux tres hautes temperatures
US4899111A (en) * 1988-08-03 1990-02-06 The Regents Of The University Of California Probe for high resolution NMR with sample reorientation

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US5202633A (en) * 1990-11-01 1993-04-13 Doty Scientific, Inc. High temperature nmr sample spinner

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1271262A (en) * 1969-05-23 1972-04-19 Cmw Lab Ltd Turbines
US3681683A (en) * 1970-09-14 1972-08-01 Varian Associates Gyromagnetic resonance spectrometer utilizing an improved sample spinning and ejecting structure
US4088944A (en) * 1976-10-04 1978-05-09 Varian Associates, Inc. NMR Spectrometer employing self centering turbine
US4254373A (en) * 1977-06-03 1981-03-03 Lippmaa Endel T Sensor for generating nuclear magnetic resonance signals
EP0073667A2 (fr) * 1981-08-31 1983-03-09 Monsanto Company Dispositif porte-échantillon tournant pour spectromètre à résonance magnétique nucléaire
US4456882A (en) * 1982-01-04 1984-06-26 University Of South Carolina High speed cylindrical nuclear magnetic resonance (NMR) sample spinner
US4739270A (en) * 1986-06-03 1988-04-19 Varian Associates, Inc. High speed spinner for NMR spectrometer
US4806868A (en) * 1987-11-13 1989-02-21 Varian Associates, Inc. NMR spinner speed control
US4859949A (en) * 1988-01-26 1989-08-22 Siemens Aktiengesellschaft Magnetic resonance spectroscopy apparatus
FR2628214A1 (fr) * 1988-03-01 1989-09-08 Sadis Bruker Spectrospin Sa Sonde pour mesures spectrometriques de resonances magnetiques aux tres hautes temperatures
US4899111A (en) * 1988-08-03 1990-02-06 The Regents Of The University Of California Probe for high resolution NMR with sample reorientation

Also Published As

Publication number Publication date
WO1992008147A2 (fr) 1992-05-14
AU8913691A (en) 1992-05-26
US5202633A (en) 1993-04-13
US5333994A (en) 1994-08-02
EP0555408A1 (fr) 1993-08-18

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