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WO1992001222A3 - Process for injecting a sample into the separation column of a gas-phase chromatograph and injection device for carrying out said process - Google Patents

Process for injecting a sample into the separation column of a gas-phase chromatograph and injection device for carrying out said process Download PDF

Info

Publication number
WO1992001222A3
WO1992001222A3 PCT/FR1991/000530 FR9100530W WO9201222A3 WO 1992001222 A3 WO1992001222 A3 WO 1992001222A3 FR 9100530 W FR9100530 W FR 9100530W WO 9201222 A3 WO9201222 A3 WO 9201222A3
Authority
WO
WIPO (PCT)
Prior art keywords
sample
carrier gas
injecting
separation column
gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/FR1991/000530
Other languages
French (fr)
Other versions
WO1992001222A2 (en
Inventor
Michel Beche
Philippe Roussel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhone Poulenc Industries SA
Original Assignee
Rhone Poulenc Industries SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhone Poulenc Industries SA filed Critical Rhone Poulenc Industries SA
Publication of WO1992001222A2 publication Critical patent/WO1992001222A2/en
Publication of WO1992001222A3 publication Critical patent/WO1992001222A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/16—Injection
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
    • G01N35/10—Devices for transferring samples or any liquids to, in, or from, the analysis apparatus, e.g. suction devices, injection devices
    • G01N35/1095—Devices for transferring samples or any liquids to, in, or from, the analysis apparatus, e.g. suction devices, injection devices for supplying the samples to flow-through analysers

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)

Abstract

Process and device for injecting a sample into the separation column of a gas-phase chromatograph. According to the process (a) the means (7) for feeding the sample to the column (12) are connected by means of the following (listed in order of the downstream direction): an injection means (2), an expansion chamber (3), a connection means (4) provided with an inlet (13) for the carrier gas; (b) the carrier gas is fed through the inlet (13) of the connecting means (4); (c) the sample is injected using an injection means (2); (d) after a set time, the carrier gas supply according to (b) is cut off; (e) the carrier gas is fed during a set time using the injection means (2); (f) the carrier gas supply according to (e) is cut off; (g) the carrier gas is fed through the inlet (13) of the connection means (4), the injection means (2) being connected to escape means (17). The process and the device are designed for on-line industrial analysis.
PCT/FR1991/000530 1990-07-09 1991-07-02 Process for injecting a sample into the separation column of a gas-phase chromatograph and injection device for carrying out said process Ceased WO1992001222A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9008913A FR2664385B1 (en) 1990-07-09 1990-07-09 METHOD FOR INJECTING THE SAMPLE INTO THE SEPARATION COLUMN OF A CHROMATOGRAPHER IN THE GASEOUS PHASE AND INJECTION DEVICE FOR CARRYING OUT SAID METHOD.
FR90/08913 1990-07-09

Publications (2)

Publication Number Publication Date
WO1992001222A2 WO1992001222A2 (en) 1992-01-23
WO1992001222A3 true WO1992001222A3 (en) 1992-02-20

Family

ID=9398660

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR1991/000530 Ceased WO1992001222A2 (en) 1990-07-09 1991-07-02 Process for injecting a sample into the separation column of a gas-phase chromatograph and injection device for carrying out said process

Country Status (2)

Country Link
FR (1) FR2664385B1 (en)
WO (1) WO1992001222A2 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8888731B2 (en) 2007-08-17 2014-11-18 The Invention Science Fund I, Llc Systems, devices, and methods including infection-fighting and monitoring shunts
US9005263B2 (en) 2007-08-17 2015-04-14 The Invention Science Fund I, Llc System, devices, and methods including actively-controllable sterilizing excitation delivery implants

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006042952B3 (en) * 2006-09-13 2008-01-10 Siemens Ag Arrangement for dosing of gaseous sample into carrier gas stream, has probe gas path and carrier gas path, which are both attached at carrier gas source, where controllable dosing equipment is arranged for locking probe gas stopper
US8029740B2 (en) 2008-07-11 2011-10-04 The Invention Science Fund I, Llc Event-triggered self-sterilization of article surfaces
US20120041287A1 (en) 2008-12-04 2012-02-16 Searete Llc, A Limited Liability Corporation Of The State Of Delaware Systems, devices, and methods including implantable devices with anti-microbial properties
US9101678B2 (en) 2011-11-03 2015-08-11 Elwha Llc Heat-sanitization of surfaces

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3759107A (en) * 1972-10-05 1973-09-18 Searle & Co Ballistic injection for gas chromatography
US4300393A (en) * 1979-12-14 1981-11-17 Stearns Stanley D Sample introduction apparatus for gas chromatographic analysis using packed or capillary bore open tubular columns and method of testing
JPS59120956A (en) * 1982-12-28 1984-07-12 Shimadzu Corp Gas chromatograph
EP0232581A1 (en) * 1985-10-30 1987-08-19 The BOC Group, Inc. Capillary switch-valve
US4801430A (en) * 1986-09-25 1989-01-31 Trustees Of Tufts College Interface for separating an analyte of interest from a liquid solvent
WO1989003990A1 (en) * 1987-10-22 1989-05-05 Siemens Aktiengesellschaft Device and procedure for metering samples in gas chromatography

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59120955A (en) * 1982-12-28 1984-07-12 Shimadzu Corp Gas chromatograph

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3759107A (en) * 1972-10-05 1973-09-18 Searle & Co Ballistic injection for gas chromatography
US4300393A (en) * 1979-12-14 1981-11-17 Stearns Stanley D Sample introduction apparatus for gas chromatographic analysis using packed or capillary bore open tubular columns and method of testing
JPS59120956A (en) * 1982-12-28 1984-07-12 Shimadzu Corp Gas chromatograph
EP0232581A1 (en) * 1985-10-30 1987-08-19 The BOC Group, Inc. Capillary switch-valve
US4801430A (en) * 1986-09-25 1989-01-31 Trustees Of Tufts College Interface for separating an analyte of interest from a liquid solvent
WO1989003990A1 (en) * 1987-10-22 1989-05-05 Siemens Aktiengesellschaft Device and procedure for metering samples in gas chromatography

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Patent Abstracts of Japan, volume 8, no. 248 (P-313)[1685] 14 novembre 1984, & JP, A, 59-120956 (SHIMAZU SEISAKUSHO K.K.) 12 juillet 1984, voir l'abrégé en entier *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8888731B2 (en) 2007-08-17 2014-11-18 The Invention Science Fund I, Llc Systems, devices, and methods including infection-fighting and monitoring shunts
US9005263B2 (en) 2007-08-17 2015-04-14 The Invention Science Fund I, Llc System, devices, and methods including actively-controllable sterilizing excitation delivery implants

Also Published As

Publication number Publication date
FR2664385B1 (en) 1994-04-01
FR2664385A1 (en) 1992-01-10
WO1992001222A2 (en) 1992-01-23

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