US20020187222A1 - Shelf-stable filled pasta and methods of making - Google Patents
Shelf-stable filled pasta and methods of making Download PDFInfo
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- US20020187222A1 US20020187222A1 US10/211,302 US21130202A US2002187222A1 US 20020187222 A1 US20020187222 A1 US 20020187222A1 US 21130202 A US21130202 A US 21130202A US 2002187222 A1 US2002187222 A1 US 2002187222A1
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- Prior art keywords
- pasta
- piece
- filling
- acid
- filled
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- 235000015927 pasta Nutrition 0.000 title claims abstract description 101
- 238000000034 method Methods 0.000 title claims abstract description 26
- 238000011049 filling Methods 0.000 claims abstract description 42
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 41
- 239000002253 acid Substances 0.000 claims abstract description 23
- 230000000694 effects Effects 0.000 claims abstract description 23
- 230000005855 radiation Effects 0.000 claims abstract description 10
- 238000007789 sealing Methods 0.000 claims abstract description 8
- 238000004519 manufacturing process Methods 0.000 claims abstract description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims description 6
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 6
- 230000000994 depressogenic effect Effects 0.000 claims description 5
- 238000007710 freezing Methods 0.000 claims description 5
- 230000008014 freezing Effects 0.000 claims description 5
- 238000005057 refrigeration Methods 0.000 claims description 5
- 239000007789 gas Substances 0.000 claims description 4
- 238000007654 immersion Methods 0.000 claims description 4
- 235000019699 ravioli Nutrition 0.000 claims description 4
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 3
- PHOQVHQSTUBQQK-SQOUGZDYSA-N D-glucono-1,5-lactone Chemical compound OC[C@H]1OC(=O)[C@H](O)[C@@H](O)[C@@H]1O PHOQVHQSTUBQQK-SQOUGZDYSA-N 0.000 claims description 3
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 3
- 229920000615 alginic acid Polymers 0.000 claims description 3
- 235000010443 alginic acid Nutrition 0.000 claims description 3
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 3
- 235000015165 citric acid Nutrition 0.000 claims description 3
- 238000011010 flushing procedure Methods 0.000 claims description 3
- 239000001530 fumaric acid Substances 0.000 claims description 3
- 235000011087 fumaric acid Nutrition 0.000 claims description 3
- 235000012209 glucono delta-lactone Nutrition 0.000 claims description 3
- 239000000182 glucono-delta-lactone Substances 0.000 claims description 3
- 229960003681 gluconolactone Drugs 0.000 claims description 3
- 239000004310 lactic acid Substances 0.000 claims description 3
- 235000014655 lactic acid Nutrition 0.000 claims description 3
- 239000001630 malic acid Substances 0.000 claims description 3
- 235000011090 malic acid Nutrition 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- 235000000346 sugar Nutrition 0.000 claims description 3
- 150000008163 sugars Chemical class 0.000 claims description 3
- 239000011975 tartaric acid Substances 0.000 claims description 3
- 235000002906 tartaric acid Nutrition 0.000 claims description 3
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 239000003906 humectant Substances 0.000 claims description 2
- 238000010030 laminating Methods 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 238000001035 drying Methods 0.000 description 13
- 150000007513 acids Chemical class 0.000 description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- 239000004615 ingredient Substances 0.000 description 6
- 235000013305 food Nutrition 0.000 description 5
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 235000013312 flour Nutrition 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 3
- 235000021472 generally recognized as safe Nutrition 0.000 description 3
- 230000000813 microbial effect Effects 0.000 description 3
- 230000020477 pH reduction Effects 0.000 description 3
- 238000004806 packaging method and process Methods 0.000 description 3
- 238000009928 pasteurization Methods 0.000 description 3
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 2
- 244000098345 Triticum durum Species 0.000 description 2
- 235000019647 acidic taste Nutrition 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 235000015432 dried pasta Nutrition 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- -1 polyethylene Polymers 0.000 description 2
- 235000015067 sauces Nutrition 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000004278 EU approved seasoning Substances 0.000 description 1
- 206010073306 Exposure to radiation Diseases 0.000 description 1
- 240000008620 Fagopyrum esculentum Species 0.000 description 1
- 235000009419 Fagopyrum esculentum Nutrition 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 235000007264 Triticum durum Nutrition 0.000 description 1
- 235000019631 acid taste sensations Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 150000007514 bases Chemical class 0.000 description 1
- 235000014658 canned/preserved pasta Nutrition 0.000 description 1
- 238000009924 canning Methods 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 235000013351 cheese Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000002242 deionisation method Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 235000007983 food acid Nutrition 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 229920001684 low density polyethylene Polymers 0.000 description 1
- 239000004702 low-density polyethylene Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 230000002906 microbiologic effect Effects 0.000 description 1
- 238000011169 microbiological contamination Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000009448 modified atmosphere packaging Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 238000001223 reverse osmosis Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 235000014102 seafood Nutrition 0.000 description 1
- 239000000565 sealant Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 108700012359 toxins Proteins 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B2/00—Preservation of foods or foodstuffs, in general
- A23B2/30—Preservation of foods or foodstuffs, in general by heating materials in packages which are not progressively transported through the apparatus
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B2/00—Preservation of foods or foodstuffs, in general
- A23B2/05—Preservation of foods or foodstuffs, in general by heating using irradiation or electric treatment
- A23B2/08—Preservation of foods or foodstuffs, in general by heating using irradiation or electric treatment using microwaves or dielectric heating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/109—Types of pasta, e.g. macaroni or noodles
- A23L7/11—Filled, stuffed or multilayered pasta
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/109—Types of pasta, e.g. macaroni or noodles
- A23L7/111—Semi-moist pasta, i.e. containing about 20% of moist; Moist packaged or frozen pasta; Pasta fried or pre-fried in a non-aqueous frying medium, e.g. oil; Packaged pasta to be cooked directly in the package
Definitions
- This invention relates to shelf-stable filled pasta and methods of manufacturing same. More particularly, the invention relates to partially or fully cooked filled pasta of intermediate moisture in which the pasta shell is rendered shelf-stable by incorporation of or treatment with edible acids and the filling is rendered shelf-stable by means of a water activity depressants and microwave or radio frequency treatment.
- shelf-stable is intended to mean stable at ambient (room temperature) conditions in the absence of refrigeration and/or freezing.
- the inventive method of making shelf-stable filled pasta comprises providing an acid-treated or acid-containing tillable pasta piece having an equilibrium pH of about 4.6 or less; inserting filling into the tillable pasta piece to form a filled pasta piece; exposing the filling in the filled pasta piece to microwave or radio frequency radiation to reduce the water activity (A w ) in the filling to about 0.85 or less; sealing the filled pasta piece in a package; and pasteurizing the filled pasta piece at least once at any point in the process after the filling has been inserted into the fillable pasta piece.
- the fillable pasta piece is formed by first laminating uncooked pasta dough; the filled pasta piece is pasteurized with steam before being exposed to microwave or radio frequency radiation; the sealing entails flushing the package with a gas that contains nitrogen and substantially lacks oxygen; an additional pasteurizing step may occur after the sealing step; the filled pasta piece is a tortellini or a ravioli; and/or the acid-treated, fillable pasta piece is treated with or contains an edible acid, especially those selected from the group consisting of citric acid, lactic acid, fumaric acid, tartaric acid, malic acid and glucono delta lactone.
- the inventive shelf-stable filled pasta comprises a pasta produced by the foregoing method.
- Preferred embodiments of the inventive shelf-stable filled pasta comprise a pasta produced by methods having some or all of the foregoing preferred features.
- the shelf-stable pasta is made by first providing pasta ingredients.
- Any suitable material from wheat can be used to make the pasta, such as semolina, farina and flours derived from hard or soft wheat, durum wheat and the like.
- Other flours can also be used, such as those derived from rice, buckwheat and similar grain sources.
- Other ingredients such as flavorants, colorants and texture improving substances such as egg albumen, alginates, gums and cellulose derivatives may be added to the flour.
- the water used in the pasta is preferably purified by deionization or reverse osmosis water treatment systems, followed by UV light exposure.
- the optimum amount of water depends on the type of flour used and can be determined by one skilled in the art.
- Edible food acids that are generally recognized as safe (GRAS) are then added to either the water or the ingredients.
- the acids are added to the water before mixture with the ingredients.
- the formed pasta dough could be immersed in the acids.
- the pH of the acids ranges from about 1.5 to about 3.5 depending on their concentrations.
- the ingredients are mixed with the acidified water to obtain dough ranging in moisture between 29 percent and 36 percent and having an equilibrium pH of about 3.8 to 4.6, preferably about 4.6.
- the dough is sheeted, i.e., laminated three times by passing it through sheeting rolls to obtain the desired dough thickness.
- the dough may be shaped by extrusion.
- Fillable pasta such as Tortellini or ravioli pieces, are then formed and filled with the filling.
- the filling is prepared by mixing the filling base (meat, cheese, vegetable seafood or other fillings) with flavoring ingredients and seasonings, and water activity depressants such as salts, sugars, gums, alcohol, alginates and humectants such as glycerol or propylene glycol. Preservatives may also be added to inhibit the growth of yeast and mold. (Yeast and molds grow at much lower water activity levels than microbes.)
- the filled pasta pieces are then pasteurized, preferably with superheated steam, to set the pasta shell surface in order to maintain structural integrity during subsequent processing.
- Steam treatment typically occurs in a food grade steamer at atmospheric pressure for about 0.5 to about 6.0 minutes.
- the filling within the pasta pieces is then exposed to microwave or radio frequency waves to reduce the water activity of the preferably non-acidified filling to 0.85 or lower, more preferably to about 0.50 to 0.85, most preferably to about 0.80 to 0.85.
- Water activity is the measure of the unbound free water available to support biological and chemical reactions. Low values of water activity are known to reduce the growth of microorganisms.
- the radiation treatment is very short, preferably 5 to 150 seconds, more preferably 15 to 70 seconds, it flushes some moisture out of the filling without changing the state of the enveloping dough from the rubber viscoelastic state that characterizes freshly made pasta.
- microwave treatment of only 15 to 70 seconds with a 50 kw batch microwave generator has the effect of moistening the exterior of the pasta shell because moisture that escapes from the inner filling is deposited there. (Preferably, the moisture content of the final pasta shell is around 22 percent.) 50 kw batch microwave generators of the type available from Microdry Inc. and radio frequency generators of the type used by Radio Frequency Company Inc. are preferred.
- the filled pasta pieces are preferably sealed in modified atmosphere packaging by pulling vacuum and flushing with nitrogen (N 2 ) or a gas mixture of carbon dioxide (CO 2 ) and nitrogen(N 2 ).
- N 2 nitrogen
- CO 2 carbon dioxide
- Packaging under partial vacuum is preferred because removing excess air improves shelf stability by minimizing oxidative flavor changes.
- the package can be any food grade, high temperature stable packaging system having good gas and moisture barrier properties. Suitable packages include pouches made of a multi-layered film having a liner of low density polyethylene, a layer of standard polyethylene and a polypropylene sealant.
- the sealed pasta pieces may be pasteurized by, for example, boil-in-bag processing, steaming or microwave pasteurization.
- the temperature at the coldest spot should be in the range of from about 80° C. to 110° C. for about 5 to 60 minutes, and preferably from about 95° C. to 100° C. for about 10 to 20 minutes.
- Pasteurization of the filled pasta pieces may be completed before packaging, especially insofar as the purpose of the heat treatment of the packaged filled pasta is to render the package itself non-microbial.
- an uncooked or partially cooked moist pasta dough is extruded and treated with steam.
- the dough is then immersed in an aqueous solution containing edible acids (GRAS) to reduce the pH to levels that inhibit microbial growth.
- GRAS edible acids
- the solution may also contain water activity depressants.
- the immersion time will vary with the thickness of the pasta and the concentration of the acid or water depressant. Sufficient immersion times generally range from about 1 minute to about 4 minutes.
- the pasta is partially surface dried to improve handling properties during subsequent processing.
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Noodles (AREA)
Abstract
A shelf-stable filled pasta and a method of making same, the method comprising providing an acid-treated or acid-containing tillable pasta piece having a pH of about 4.6 or less; inserting filling into the tillable pasta piece; exposing the filling in the filled pasta piece to microwave or radio frequency radiation to reduce the water activity in the filling to about 0.85 or less; sealing the filled pasta piece in a package; and pasteurizing the filled pasta piece at any point in the process after the filling has been inserted into the fillable pasta piece. The shelf-stable filled pasta is a pasta made by the foregoing method.
Description
- 1. Field of the Invention
- This invention relates to shelf-stable filled pasta and methods of manufacturing same. More particularly, the invention relates to partially or fully cooked filled pasta of intermediate moisture in which the pasta shell is rendered shelf-stable by incorporation of or treatment with edible acids and the filling is rendered shelf-stable by means of a water activity depressants and microwave or radio frequency treatment.
- 2. Description of Related Art
- Many partially and fully cooked packaged pastas are disclosed in the prior art. Prior methods for rendering them storable include canning, complete or partial drying, freezing or refrigeration, and acidification. These methods, however, produce filled pasta with sensory attributes that are significantly different from freshly made filled pasta.
- Fully cooked canned pasta, which generally has more than 38 percent moisture, tends to be soggy and mushy because the moisture difference between the core and surface portion of the pasta is lost. When pasta is first made, the core is less moist than the surface of the pasta. This moisture difference is responsible for the desired “al dente” texture. Within hours, however, the moisture difference disappears and the pasta becomes soggy and mushy.
- Some workers in the field have resorted to drying the pasta to increase shelf stability. The drying process, however, normally requires careful control of temperature and humidity, takes a considerable amount of space, and must be done very slowly (6-18 hours). If hastened, a hard “skin” forms over the surface of the individual pasta pieces, and this skin cracks during subsequent drying. The result is pasta that is fragile and, when prepared for consumption in boiling water, falls apart. Drying can also result in microbiological contamination because the moist warm atmosphere of the dryers encourages microbiological growth. Furthermore, while the bacteria themselves may be rendered harmless by the heat during the final stages of drying, heat stable toxins are often produced that cannot be easily rendered harmless. Finally, dried pasta must be re-hydrated by immersing it in boiling water or steam. This takes a relatively long time and exacerbates the flavor loss already occasioned by the extended drying in filled dried pasta, often the filling does not rehydrate fully and uniformly during cooking.
- Others have attempted to reduce the water activity in pasta by adding water activity depressants such as sugars, salts, glycerol, propylene glycol and the like. Adding large amounts of water activity depressants, however, can harm the flavor and texture of the pasta, especially the shell portion of the filled pasta and especially if water depressants are the only means used to obtain pasta that need not be refrigerated or frozen.
- Others have attempted to increase shelf stability by adding edible acids to the filling and shell portion pasta to obtain a pH of around 4.6. These bacteria-killing acids, however, result in an unpleasant acid taste, especially when the filling is acidified. As U.S. Pat. No. 5,922,381 to Nestec states, “in the case of filled pasta products such as ravioli and tortellini, most fillings accentuate the acidic note and the products become almost inedible at pH lower than 4.6.” To counter the acidic note, others have added basic compounds to sauces in separate packages to neutralize the acids just before eating. In the case of filled pastas, however, the sauce fails to reach the filling, neutralizing only the acid near the exterior of the pasta shell.
- It can be appreciated from examining the prior art that there exists a continuing need for a new and improved fully or partially cooked shelf-stable filled pasta that needs no refrigeration or freezing to prolong shelf stability, and methods of making the same. In this regard, the present invention substantially fulfills this need. As used hereafter, “shelf-stable” is intended to mean stable at ambient (room temperature) conditions in the absence of refrigeration and/or freezing.
- The inventive method of making shelf-stable filled pasta comprises providing an acid-treated or acid-containing tillable pasta piece having an equilibrium pH of about 4.6 or less; inserting filling into the tillable pasta piece to form a filled pasta piece; exposing the filling in the filled pasta piece to microwave or radio frequency radiation to reduce the water activity (A w) in the filling to about 0.85 or less; sealing the filled pasta piece in a package; and pasteurizing the filled pasta piece at least once at any point in the process after the filling has been inserted into the fillable pasta piece.
- Preferred embodiments of the inventive method include some or all of the following features: the fillable pasta piece is formed by first laminating uncooked pasta dough; the filled pasta piece is pasteurized with steam before being exposed to microwave or radio frequency radiation; the sealing entails flushing the package with a gas that contains nitrogen and substantially lacks oxygen; an additional pasteurizing step may occur after the sealing step; the filled pasta piece is a tortellini or a ravioli; and/or the acid-treated, fillable pasta piece is treated with or contains an edible acid, especially those selected from the group consisting of citric acid, lactic acid, fumaric acid, tartaric acid, malic acid and glucono delta lactone.
- The inventive shelf-stable filled pasta comprises a pasta produced by the foregoing method. Preferred embodiments of the inventive shelf-stable filled pasta comprise a pasta produced by methods having some or all of the foregoing preferred features.
- Typically, in filled pasta both the dough and filling need to be acidified if their water activities are higher than 0.85. Acidification of both the dough and the filling, however, produces unacceptable sensory attributes due to a strong acidic taste. Most of the acidic taste is contributed by the acid in the filling. To eliminate the acidification of the filling while retaining shelf stability, I have found that it is necessary to reduce the filling's water activity to 0.85 or lower.
- In a preferred embodiment, the shelf-stable pasta is made by first providing pasta ingredients. Any suitable material from wheat can be used to make the pasta, such as semolina, farina and flours derived from hard or soft wheat, durum wheat and the like. Other flours can also be used, such as those derived from rice, buckwheat and similar grain sources. Other ingredients such as flavorants, colorants and texture improving substances such as egg albumen, alginates, gums and cellulose derivatives may be added to the flour.
- To reduce microbial load, the water used in the pasta is preferably purified by deionization or reverse osmosis water treatment systems, followed by UV light exposure. The optimum amount of water depends on the type of flour used and can be determined by one skilled in the art.
- Edible food acids that are generally recognized as safe (GRAS) are then added to either the water or the ingredients. Preferably, the acids are added to the water before mixture with the ingredients. (Alternatively, the formed pasta dough could be immersed in the acids.) The pH of the acids ranges from about 1.5 to about 3.5 depending on their concentrations.
- Next, the ingredients are mixed with the acidified water to obtain dough ranging in moisture between 29 percent and 36 percent and having an equilibrium pH of about 3.8 to 4.6, preferably about 4.6. The dough is sheeted, i.e., laminated three times by passing it through sheeting rolls to obtain the desired dough thickness. Alternatively, the dough may be shaped by extrusion. Fillable pasta, such as Tortellini or ravioli pieces, are then formed and filled with the filling.
- The filling is prepared by mixing the filling base (meat, cheese, vegetable seafood or other fillings) with flavoring ingredients and seasonings, and water activity depressants such as salts, sugars, gums, alcohol, alginates and humectants such as glycerol or propylene glycol. Preservatives may also be added to inhibit the growth of yeast and mold. (Yeast and molds grow at much lower water activity levels than microbes.)
- The filled pasta pieces are then pasteurized, preferably with superheated steam, to set the pasta shell surface in order to maintain structural integrity during subsequent processing. Steam treatment typically occurs in a food grade steamer at atmospheric pressure for about 0.5 to about 6.0 minutes.
- The filling within the pasta pieces is then exposed to microwave or radio frequency waves to reduce the water activity of the preferably non-acidified filling to 0.85 or lower, more preferably to about 0.50 to 0.85, most preferably to about 0.80 to 0.85. Water activity is the measure of the unbound free water available to support biological and chemical reactions. Low values of water activity are known to reduce the growth of microorganisms. One measure of water activity is A w=P/Po, where P is the vapor pressure of water in the food item and Po is the vapor pressure of pure water at the same temperature. Lowering Aw restricts the growth of bacteria and is accomplished by lowering P, the vapor pressure of water in the food item. P may be depressed by adding solutes to the food item. Most bacteria of concern require Aw values of 0.90 or greater to grow.
- Exposing the pasta to radiation drives water out of the filling, thereby increasing the filling's solute to water ratio. It is significant that this step entails an initial inside-to-outside movement of water, whereas conventional drying first removes water from the outside of the pasta shell and then, eventually, from the filling inside the shell. Conventional drying hardens the pasta shell, preventing rapid moisture removal from the filling. Thus, with conventional drying, prolonged drying time is needed to remove the desired amount of water from the filling, and this longer drying time causes excessive drying of the shell while the filling moisture remains high. If the radiation treatment is very short, preferably 5 to 150 seconds, more preferably 15 to 70 seconds, it flushes some moisture out of the filling without changing the state of the enveloping dough from the rubber viscoelastic state that characterizes freshly made pasta. Indeed, microwave treatment of only 15 to 70 seconds with a 50 kw batch microwave generator has the effect of moistening the exterior of the pasta shell because moisture that escapes from the inner filling is deposited there. (Preferably, the moisture content of the final pasta shell is around 22 percent.) 50 kw batch microwave generators of the type available from Microdry Inc. and radio frequency generators of the type used by Radio Frequency Company Inc. are preferred.
- After exposure to radiation, the filled pasta pieces are preferably sealed in modified atmosphere packaging by pulling vacuum and flushing with nitrogen (N 2) or a gas mixture of carbon dioxide (CO2) and nitrogen(N2). Packaging under partial vacuum is preferred because removing excess air improves shelf stability by minimizing oxidative flavor changes. The package can be any food grade, high temperature stable packaging system having good gas and moisture barrier properties. Suitable packages include pouches made of a multi-layered film having a liner of low density polyethylene, a layer of standard polyethylene and a polypropylene sealant.
- Finally, the sealed pasta pieces may be pasteurized by, for example, boil-in-bag processing, steaming or microwave pasteurization. In any event, it is essential that the filling in the center of the pasta reach the minimum pasteurization temperature. The temperature at the coldest spot should be in the range of from about 80° C. to 110° C. for about 5 to 60 minutes, and preferably from about 95° C. to 100° C. for about 10 to 20 minutes. Pasteurization of the filled pasta pieces may be completed before packaging, especially insofar as the purpose of the heat treatment of the packaged filled pasta is to render the package itself non-microbial.
- The surface appearance and consistency of the radiation-treated filled pasta are very similar to that of freshly produced filled pasta. It does not require refrigeration or freezing, cooks in short time, and has an extended shelf life on the order of nine months.
- In other embodiments, an uncooked or partially cooked moist pasta dough is extruded and treated with steam. The dough is then immersed in an aqueous solution containing edible acids (GRAS) to reduce the pH to levels that inhibit microbial growth. The solution may also contain water activity depressants. The immersion time will vary with the thickness of the pasta and the concentration of the acid or water depressant. Sufficient immersion times generally range from about 1 minute to about 4 minutes. Following the immersion step, the pasta is partially surface dried to improve handling properties during subsequent processing.
- It should be understood that the foregoing summary and detailed description of the invention are not intended to be limiting, but are only exemplary of the inventive features that are defined in the claims.
Claims (19)
1. A method of manufacturing filled pasta capable of storage without refrigeration or freezing, comprising the steps of:
a) providing a fillable pasta piece having a pH of about 4.6 or less;
b) inserting a filling into said fillable pasta piece to form a filled pasta piece;
c) exposing the filling in said filled pasta piece to microwave or radio frequency radiation to reduce the water activity of the filling to about 0.85 or less;
d) sealing said filled pasta piece in a package; and
e) pasteurizing said filled pasta piece at any point after said inserting a filling step.
2. The method of claim 1 , wherein said filling includes a water activity depressant.
3. The method of claim 2 , wherein said water activity depressant is selected from the group consisting of sugars, salts, gums, alcohol, alginates and humectants.
4. The method of claim 1 , wherein the water activity is reduced to 0.80 to 0.85.
5. The method of claim 1 , wherein said exposure to microwave or radio frequency radiation lasts from 15 to 70 seconds.
6. The method of claim 1 , wherein the filled pasta piece has a shelf life of at least nine months.
7. The method of claim 1 , wherein said fillable pasta piece is formed by first laminating uncooked pasta dough.
8. The method of claim 1 , wherein said filled pasta piece is pasteurized with steam before being exposed to microwave or radio frequency radiation.
9. The method of claim 1 , further comprising an additional pasteurizing step after said sealing.
10. The method of claim 1 , wherein said sealing comprises flushing said package with a gas containing nitrogen and substantially lacking oxygen.
11. The method of claim 1 , wherein said pH of said fillable pasta piece is reached by addition of an edible acid.
12. The method of claim 11 , wherein said edible acid is selected from the group consisting of citric acid, lactic acid, fumaric acid, tartaric acid, malic acid and glucono delta lactone.
13. The method of claim 1 , wherein said pH of said fillable pasta piece is reached by immersion in a solution containing an edible acid.
14. The method of claim 13 , wherein said edible acid is selected from the group consisting of citric acid, lactic acid, fumaric acid, tartaric acid, malic acid and glucono delta lactone.
15. A shelf-stable filled pasta produced by a process comprising the steps of:
a) providing an acid-treated or acid-containing fillable pasta piece having a pH of about 4.6 or less;
b) inserting filling into said tillable pasta piece to form a filled pasta piece;
c) exposing the filling in said filled pasta piece to microwave or radio frequency radiation to reduce the water activity of the filling to about 0.85 or less;
d) sealing said filled pasta piece in a package; and
e) pasteurizing said filled pasta piece at any point after said inserting a filling step.
16. The shelf-stable filled pasta of claim 15 , wherein said filling includes a water activity depressant.
17. The shelf-stable filled pasta of claim 15 , wherein the water activity is reduced to 0.80 to 0.85.
18. The shelf-stable filled pasta of claim 15 , wherein the filled pasta piece has a shelf life of at least nine months.
19. The shelf-stable filled pasta of claim 15 , wherein said filled pasta piece is selected from the group consisting of tortellini and ravioli.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/211,302 US20020187222A1 (en) | 2001-01-24 | 2002-08-05 | Shelf-stable filled pasta and methods of making |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/767,905 US6428835B1 (en) | 2001-01-24 | 2001-01-24 | Shelf-stable filled pasta and methods of making |
| US10/211,302 US20020187222A1 (en) | 2001-01-24 | 2002-08-05 | Shelf-stable filled pasta and methods of making |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US09/767,905 Division US6428835B1 (en) | 2001-01-24 | 2001-01-24 | Shelf-stable filled pasta and methods of making |
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| Publication Number | Publication Date |
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| US20020187222A1 true US20020187222A1 (en) | 2002-12-12 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US09/767,905 Expired - Lifetime US6428835B1 (en) | 2001-01-24 | 2001-01-24 | Shelf-stable filled pasta and methods of making |
| US10/211,302 Abandoned US20020187222A1 (en) | 2001-01-24 | 2002-08-05 | Shelf-stable filled pasta and methods of making |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US09/767,905 Expired - Lifetime US6428835B1 (en) | 2001-01-24 | 2001-01-24 | Shelf-stable filled pasta and methods of making |
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| US (2) | US6428835B1 (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110104338A1 (en) * | 2009-10-30 | 2011-05-05 | Coleman Edward C | Food Product Pertaining To A Filling-And-Cracker Sandwich |
| CN107996952A (en) * | 2018-01-29 | 2018-05-08 | 重庆味之海食品有限公司 | Based on the room temperature of microwave and gas-containing cooking combined sterilizing cooking bag and preparation method thereof |
| IT201900009801A1 (en) * | 2019-06-21 | 2020-12-21 | Wealth & Res Trading Ltd | Apparatus and method for producing dry food pasta |
| WO2022066632A1 (en) * | 2020-09-25 | 2022-03-31 | General Mills, Inc. | Ph controlled composition |
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| CA2345513C (en) * | 2000-04-26 | 2010-03-30 | Borden Foods Corporation | Ph control of sauces used on acidified pasta or rice |
| US20040067285A1 (en) * | 2002-10-02 | 2004-04-08 | Kenneth Gimelli | Uniform cooking pasta |
| US20050106292A1 (en) * | 2003-11-13 | 2005-05-19 | Huber Gordon R. | High moisture, shelf-stable acidulated food products |
| US20090047390A1 (en) * | 2007-07-27 | 2009-02-19 | John Cassel | Chicken noodle bites |
| KR101033277B1 (en) | 2008-04-07 | 2011-05-09 | 한국원자력연구원 | How to make ramen that can be eaten even in space |
| US9420804B2 (en) * | 2008-10-06 | 2016-08-23 | Kraft Foods Group Brands Llc | Shelf stable sauce for acidified starch |
| WO2014025328A2 (en) * | 2012-08-08 | 2014-02-13 | Nuh'un Ankara Makarnasi San. Ve Tic. A.Ş. | A manufacturing method that can be used for the production of stuffed pasta |
| IT201800007432A1 (en) * | 2018-07-23 | 2020-01-23 | METHOD OF MAKING A FOOD KIT FOR THE PREPARATION OF FRESH FILLED PASTA, FOOD KIT OBTAINED AND METHOD OF USE | |
| CN114304489B (en) * | 2021-12-14 | 2023-08-01 | 西北农林科技大学 | A method for drying dried noodles with low-frequency electromagnetic field |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4898744A (en) * | 1987-12-22 | 1990-02-06 | General Foods Corporation | Method for preparing and preserving filled pasta products |
| US5059433A (en) * | 1990-10-26 | 1991-10-22 | Borden, Inc. | Method of preparing shelf stable, filled dough food products |
| TW298560B (en) * | 1993-05-26 | 1997-02-21 | Cpc International Inc | |
| US5972397A (en) * | 1997-06-16 | 1999-10-26 | The University Of British Columbia | Method for preparing dried, uncooked potato slices |
| US5922381A (en) * | 1997-09-02 | 1999-07-13 | Nestec S.A. | Preparation of filled pastas |
-
2001
- 2001-01-24 US US09/767,905 patent/US6428835B1/en not_active Expired - Lifetime
-
2002
- 2002-08-05 US US10/211,302 patent/US20020187222A1/en not_active Abandoned
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110104338A1 (en) * | 2009-10-30 | 2011-05-05 | Coleman Edward C | Food Product Pertaining To A Filling-And-Cracker Sandwich |
| CN107996952A (en) * | 2018-01-29 | 2018-05-08 | 重庆味之海食品有限公司 | Based on the room temperature of microwave and gas-containing cooking combined sterilizing cooking bag and preparation method thereof |
| IT201900009801A1 (en) * | 2019-06-21 | 2020-12-21 | Wealth & Res Trading Ltd | Apparatus and method for producing dry food pasta |
| WO2020254977A1 (en) * | 2019-06-21 | 2020-12-24 | Wealth & Research Trading Ltd. | Apparatus and method for producing dry pasta |
| CN114144073A (en) * | 2019-06-21 | 2022-03-04 | 财富&研究贸易有限公司 | Apparatus and method for producing dried noodles |
| US12446602B2 (en) | 2019-06-21 | 2025-10-21 | Wealth & Research Trading Ltd. | Apparatus and method for producing dry pasta |
| WO2022066632A1 (en) * | 2020-09-25 | 2022-03-31 | General Mills, Inc. | Ph controlled composition |
| US12310389B2 (en) | 2020-09-25 | 2025-05-27 | General Mills, Inc. | PH controlled composition |
Also Published As
| Publication number | Publication date |
|---|---|
| US6428835B1 (en) | 2002-08-06 |
| US20020098266A1 (en) | 2002-07-25 |
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