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UA95898C2 - Способ разложения циклогексилгидропероксида и способ получения циклогексанона - Google Patents

Способ разложения циклогексилгидропероксида и способ получения циклогексанона

Info

Publication number
UA95898C2
UA95898C2 UAA200708303A UAA200708303A UA95898C2 UA 95898 C2 UA95898 C2 UA 95898C2 UA A200708303 A UAA200708303 A UA A200708303A UA A200708303 A UAA200708303 A UA A200708303A UA 95898 C2 UA95898 C2 UA 95898C2
Authority
UA
Ukraine
Prior art keywords
cyclohexanone
preparation
decomposing
cyclohexylhydroperoxide
decomposing cyclohexylhdroperoxide
Prior art date
Application number
UAA200708303A
Other languages
English (en)
Ukrainian (uk)
Inventor
Имре Тот
Original Assignee
ДСМ АйПи АСЕТС Б.В.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ДСМ АйПи АСЕТС Б.В. filed Critical ДСМ АйПи АСЕТС Б.В.
Publication of UA95898C2 publication Critical patent/UA95898C2/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/48—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups
    • C07C29/50—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups with molecular oxygen only
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/53—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of hydroperoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385—Saturated compounds containing a keto group being part of a ring
    • C07C49/403—Saturated compounds containing a keto group being part of a ring of a six-membered ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Steroid Compounds (AREA)

Abstract

Данное изобретение относится к способу разложения циклогексилгидропероксида с образованием циклогексанона, который предусматривает смешивание исходного органического раствора, содержащего циклогексилгидропероксид, с водным щелочным раствором без применения катализатора на основе переходных металлов, что приводит к образованию смеси, которая включает (i) водную фазу и (ii) органическую фазу, содержащую циклогексанон и циклогексанол.
UAA200708303A 2004-12-22 2005-12-16 Способ разложения циклогексилгидропероксида и способ получения циклогексанона UA95898C2 (ru)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP04078490 2004-12-22

Publications (1)

Publication Number Publication Date
UA95898C2 true UA95898C2 (ru) 2011-09-26

Family

ID=34928767

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA200708303A UA95898C2 (ru) 2004-12-22 2005-12-16 Способ разложения циклогексилгидропероксида и способ получения циклогексанона

Country Status (16)

Country Link
US (1) US7956221B2 (ru)
EP (1) EP1828090B1 (ru)
JP (1) JP2008524298A (ru)
KR (1) KR20070094930A (ru)
CN (1) CN101087747B (ru)
AT (1) ATE486054T1 (ru)
BR (1) BRPI0519246A2 (ru)
DE (1) DE602005024436D1 (ru)
EA (1) EA011556B1 (ru)
ES (1) ES2353806T3 (ru)
MX (1) MX2007007748A (ru)
MY (1) MY144731A (ru)
PL (1) PL1828090T3 (ru)
TW (1) TW200628435A (ru)
UA (1) UA95898C2 (ru)
WO (1) WO2006066904A1 (ru)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104557497A (zh) * 2013-10-09 2015-04-29 中国石油化工股份有限公司 一种提高环己基过氧化氢分解酮醇比的方法
EP3214061A4 (en) * 2014-10-31 2018-07-18 UBE Industries, Ltd. Method for producing ketone and/or alcohol, and system thereof
SG11201706920VA (en) * 2015-02-27 2017-09-28 Gcp Applied Tech Inc Modifying cementitious compositions using ketone alcohol oil waste
CN107778133B (zh) * 2016-08-25 2021-05-07 中国石油化工股份有限公司 一种制备环己醇和环己酮的方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB716820A (en) * 1951-04-19 1954-10-13 Du Pont Preparation of oxidized cyclohexane
JPS49108047A (ru) * 1973-02-20 1974-10-14
US4163027A (en) 1976-11-06 1979-07-31 Basf Aktiengesellschaft Working-up of reaction mixtures containing cyclohexanol and cyclohexanone
DE2650892C3 (de) * 1976-11-06 1980-05-29 Basf Ag, 6700 Ludwigshafen Verfahren zur Aufarbeitung von Cyclohexanol und Cyclohexanon enthaltenden Reaktionsgemischen
NL7802125A (nl) * 1978-02-25 1979-08-28 Stamicarbon Werkwijze voor het bereiden van cycloalkanolen en cycloalkanonen.
NL8201695A (nl) 1982-04-23 1983-11-16 Stamicarbon Werkwijze voor de bereiding van cyclohexanol en cyclohexanon.
JP2500977B2 (ja) 1992-03-24 1996-05-29 三菱化学株式会社 シクロヘキサノンの製造方法
NL9201269A (nl) * 1992-07-15 1994-02-01 Dsm Nv Werkwijze voor de bereiding van cyclohexylhydroperoxide.
US5824819A (en) * 1996-12-18 1998-10-20 Twenty-First Century Research Corporation Methods of preparing an intermediate oxidation product from a hydrocarbon by utilizing an activated initiator
US5892122A (en) * 1997-08-25 1999-04-06 E. I. Du Pont De Nemours And Company Method for making cyclohexanol and cyclohexanone

Also Published As

Publication number Publication date
CN101087747A (zh) 2007-12-12
JP2008524298A (ja) 2008-07-10
MY144731A (en) 2011-10-31
EA200701338A1 (ru) 2007-12-28
EP1828090A1 (en) 2007-09-05
KR20070094930A (ko) 2007-09-27
CN101087747B (zh) 2011-06-08
ES2353806T3 (es) 2011-03-07
BRPI0519246A2 (pt) 2009-01-06
TW200628435A (en) 2006-08-16
EP1828090B1 (en) 2010-10-27
US20100137645A1 (en) 2010-06-03
DE602005024436D1 (de) 2010-12-09
PL1828090T3 (pl) 2011-04-29
US7956221B2 (en) 2011-06-07
MX2007007748A (es) 2007-08-22
WO2006066904A1 (en) 2006-06-29
ATE486054T1 (de) 2010-11-15
EA011556B1 (ru) 2009-04-28

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