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TWI823503B - Silicon chip edge roughness detection fixture and detection method - Google Patents

Silicon chip edge roughness detection fixture and detection method Download PDF

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Publication number
TWI823503B
TWI823503B TW111128933A TW111128933A TWI823503B TW I823503 B TWI823503 B TW I823503B TW 111128933 A TW111128933 A TW 111128933A TW 111128933 A TW111128933 A TW 111128933A TW I823503 B TWI823503 B TW I823503B
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silicon wafer
edge
sample
silicon
edge roughness
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TW111128933A
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TW202247314A (en
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張婉婉
李陽
衡鵬
徐鵬
韓聰
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大陸商西安奕斯偉材料科技股份有限公司
大陸商西安奕斯偉矽片技術有限公司
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01BMEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B21/00Measuring arrangements or details thereof, where the measuring technique is not covered by the other groups of this subclass, unspecified or not relevant
    • G01B21/30Measuring arrangements or details thereof, where the measuring technique is not covered by the other groups of this subclass, unspecified or not relevant for measuring roughness or irregularity of surfaces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01BMEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B21/00Measuring arrangements or details thereof, where the measuring technique is not covered by the other groups of this subclass, unspecified or not relevant
    • G01B21/20Measuring arrangements or details thereof, where the measuring technique is not covered by the other groups of this subclass, unspecified or not relevant for measuring contours or curvatures, e.g. determining profile
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01BMEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B5/00Measuring arrangements characterised by the use of mechanical techniques
    • G01B5/0002Arrangements for supporting, fixing or guiding the measuring instrument or the object to be measured
    • G01B5/0004Supports
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q60/00Particular types of SPM [Scanning Probe Microscopy] or microscopes; Essential components thereof
    • G01Q60/24AFM [Atomic Force Microscopy] or apparatus therefor, e.g. AFM probes

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  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Radiology & Medical Imaging (AREA)
  • Testing Or Measuring Of Semiconductors Or The Like (AREA)
  • A Measuring Device Byusing Mechanical Method (AREA)
  • Length Measuring Devices By Optical Means (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

本發明實施例提供了一種矽片邊緣粗糙度檢測治具及檢測方法,該矽片邊緣粗糙度檢測治具包括:用於承載矽片樣品的基座,該基座包括水平底面及與該水平底面之間呈預設夾角α的傾斜承載面,0<α≤90°;及,用於夾持固定該矽片樣品的夾持部件,該夾持部件設置於該傾斜承載面上。本發明實施例提供的矽片邊緣粗糙度檢測治具及檢測方法,能夠對矽片邊緣的粗糙度和表面形貌分析,且能夠減少測量的誤差,保證測試可信度。Embodiments of the present invention provide a silicon wafer edge roughness detection fixture and a detection method. The silicon wafer edge roughness detection fixture includes: a base for carrying a silicon wafer sample. The base includes a horizontal bottom surface and a horizontal bottom surface. An inclined bearing surface with a preset angle α between the bottom surfaces, 0<α≤90°; and a clamping component for clamping and fixing the silicon wafer sample, the clamping component is arranged on the inclined bearing surface. The silicon wafer edge roughness detection fixture and detection method provided by embodiments of the present invention can analyze the roughness and surface morphology of the silicon wafer edge, reduce measurement errors, and ensure test reliability.

Description

矽片邊緣粗糙度檢測治具及檢測方法Silicon chip edge roughness detection fixture and detection method

本發明屬於半導體加工技術領域,尤其關於一種矽片邊緣粗糙度檢測治具及檢測方法。 The invention belongs to the field of semiconductor processing technology, and in particular relates to a silicon chip edge roughness detection jig and detection method.

近年來,大直徑矽片需求量急劇增加,在半導體生產中矽片邊緣相關問題得到了廣泛關注。在矽片加工生產中,矽片的邊緣主要存在兩個問題:一種是,由於腐蝕產生的微小缺口和裂縫導致矽片斷裂;另一種是,由於矽片邊緣粉塵顆粒和異物附著。這兩種問題在晶片製作過程中常導致晶片的良品率降低,因此矽片邊緣有一個無缺陷的平滑表面至關重要。 In recent years, the demand for large-diameter silicon wafers has increased dramatically, and issues related to the edges of silicon wafers have received widespread attention in semiconductor production. In the processing and production of silicon wafers, there are two main problems at the edges of silicon wafers: one is that the silicon wafers break due to micro-nicks and cracks caused by corrosion; the other is that dust particles and foreign matter adhere to the edges of the silicon wafers. These two problems often lead to a reduction in wafer yield during the wafer manufacturing process, so it is crucial to have a smooth, defect-free surface at the edge of the silicon wafer.

在相關技術中,採用原子力顯微鏡(Atomic Force Microscope,AFM)對矽片表面粗糙度進行檢測,但是,這種方式只能對矽片表面的粗糙度進行檢測,無法對矽片邊緣的粗糙度和邊緣表面狀態進行檢測。 In related technologies, Atomic Force Microscope (AFM) is used to detect the surface roughness of silicon wafers. However, this method can only detect the roughness of the silicon wafer surface and cannot detect the roughness and edge roughness of the silicon wafer edges. Check the edge surface condition.

本發明實施例提供了一種矽片邊緣粗糙度檢測治具及檢測方法,能夠對矽片邊緣的粗糙度和表面形貌分析,且能夠減少測量的誤差,保證測試可信度。 Embodiments of the present invention provide a silicon wafer edge roughness detection fixture and detection method, which can analyze the roughness and surface morphology of the silicon wafer edge, reduce measurement errors, and ensure test reliability.

本發明實施例所提供的技術方案如下: 本發明一種矽片邊緣粗糙度檢測治具,包括:用於承載矽片樣品的基座,該基座包括水平底面及與該水平底面之間呈預設夾角α的傾斜承載面,0<α

Figure 111128933-A0305-02-0004-7
90°;及,用於夾持固定該矽片樣品的夾持部件,該夾持部件設置於該傾斜承載面上。 The technical solutions provided by the embodiments of the present invention are as follows: A silicon wafer edge roughness detection fixture of the present invention includes: a base for carrying a silicon wafer sample. The base includes a horizontal bottom surface and a predetermined distance between the horizontal bottom surface and the horizontal bottom surface. Assume an inclined bearing surface with an included angle α, 0<α
Figure 111128933-A0305-02-0004-7
90°; and, a clamping component used to clamp and fix the silicon wafer sample, the clamping component is arranged on the inclined bearing surface.

示例性的,該矽片樣品包括邊緣倒角、及相對的第一表面和第二表面,在垂直於第一表面的橫截面上,該邊緣倒角包括最外側頂點O,經過該最外側頂點O的切線垂直於該第一表面,且該第一表面與該邊緣倒角結構的交界點a與經過該最外側頂點O的切線的垂直距離為A1,該第二表面與該邊緣倒角結構的交界點b與經過該最外側頂點O的切線的垂直距離為A2,該邊緣倒角結構的最外側頂點O與該第一表面之間的垂直距離為B1,與該第二表面之間的垂直距離為B2;其中,該預設夾角α與該矽片樣品的邊緣倒角之間滿足以下關係:tanα=B1/A1或者tanα=B2/A2。 Exemplarily, the silicon wafer sample includes an edge chamfer, and opposite first and second surfaces. On a cross-section perpendicular to the first surface, the edge chamfer includes an outermost vertex O, passing through the outermost vertex The tangent line of O is perpendicular to the first surface, and the vertical distance between the intersection point a of the first surface and the edge chamfer structure and the tangent line passing through the outermost vertex O is A1, and the second surface and the edge chamfer structure The vertical distance between the intersection point b and the tangent line passing through the outermost vertex O is A2, the vertical distance between the outermost vertex O of the edge chamfer structure and the first surface is B1, and the vertical distance between the outermost vertex O and the second surface is B1. The vertical distance is B2; where the preset angle α and the edge chamfer of the silicon wafer sample satisfy the following relationship: tanα=B1/A1 or tanα=B2/A2.

示例性的,該夾持部件採用可彈性變形材料製成的一體結構。 Exemplarily, the clamping component adopts an integrated structure made of elastically deformable material.

示例性的,該夾持部件包括垂直於該傾斜承載面的第一部分、及與該第一部分連接且平行於該傾斜承載面的第二部分,該第一部分、該第二部分與該傾斜承載面配合形成夾持槽,且該夾持槽的槽口朝向該傾斜承載面中水平位置最高的一側。 Exemplarily, the clamping component includes a first part perpendicular to the inclined bearing surface and a second part connected to the first part and parallel to the inclined bearing surface. The first part, the second part and the inclined bearing surface are A clamping groove is formed by cooperation, and the notch of the clamping groove faces the side with the highest horizontal position in the inclined bearing surface.

示例性的,該第二部分的位於該夾持槽的夾持入口處設置為弧形引導面。 Exemplarily, the second part is provided with an arc-shaped guide surface at the clamping entrance of the clamping groove.

示例性的,該基座採用硬質不易變形材料製成。 For example, the base is made of hard material that is not easily deformed.

本發明實施例還提供了一種矽片邊緣粗糙度檢測方法,包括: 在待檢測矽片的邊緣上切割出矽片樣品,該矽片樣品至少包括該待檢測矽片邊緣的一部分、及該待檢測矽片樣品表面的一部分;將該矽片樣品夾持固定於本發明實施例提供的矽片邊緣粗糙度檢測治具上,其中該矽片樣品的邊緣及該矽片樣品的表面至少部分未被該夾持部件遮擋;將該矽片邊緣粗糙度檢測治具放置於原子力顯示鏡的樣品臺上,其中該矽片樣品的邊緣倒角處的待檢測區域與該樣品台保持水平;通過原子力顯微鏡的探針對該待檢測區域進行掃描,以獲取測試圖像;對該測試圖像進行處理,得到矽片邊緣粗糙度值和矽片邊緣形貌。 Embodiments of the present invention also provide a method for detecting edge roughness of silicon wafers, including: Cut a silicon wafer sample on the edge of the silicon wafer to be detected, and the silicon wafer sample includes at least a part of the edge of the silicon wafer to be detected and a part of the surface of the silicon wafer sample to be detected; clamp and fix the silicon wafer sample on the On the silicon wafer edge roughness detection jig provided by the embodiment of the invention, the edge of the silicon wafer sample and the surface of the silicon wafer sample are at least partially not blocked by the clamping component; the silicon wafer edge roughness detection jig is placed On the sample stage of the atomic force display mirror, the area to be detected at the edge chamfer of the silicon wafer sample is kept level with the sample stage; the area to be detected is scanned by the probe of the atomic force microscope to obtain a test image; The test image is processed to obtain the edge roughness value of the silicon wafer and the edge morphology of the silicon wafer.

示例性的,該在待檢測矽片的邊緣預定位置點切割出矽片樣品,具體包括:將該待檢測矽片的邊緣沿該待檢測矽片的圓周順次均勻地劃分出N個檢測點,每個檢測點上切割一個矽片樣品,N個矽片樣品上順次標有序號。 Exemplarily, cutting a silicon wafer sample at a predetermined position on the edge of the silicon wafer to be detected specifically includes: dividing the edge of the silicon wafer to be detected into N detection points evenly and sequentially along the circumference of the silicon wafer to be detected, A silicon wafer sample is cut at each detection point, and the N silicon wafer samples are marked with serial numbers in sequence.

示例性的,每個該矽片樣品的尺寸為1cm×1cm。 For example, the size of each silicon wafer sample is 1cm×1cm.

本發明實施例所帶來的有益效果如下:本發明實施例提供的矽片邊緣粗糙度檢測治具及檢測方法,設計了一種專門的矽片邊緣粗糙度檢測治具,可以在待檢測矽片的邊緣上切割出矽片樣品之後,將矽片樣品放置於該治具上,而使得矽片樣品的邊緣待檢測部位保持水平,從而可利用原子力顯微鏡對矽片邊緣的粗糙度和表面形貌進行分析,且能夠減少測量的誤差,保證測試可信度。 The beneficial effects brought by the embodiments of the present invention are as follows: the silicon wafer edge roughness detection jig and detection method provided by the embodiments of the present invention design a special silicon wafer edge roughness detection jig, which can detect the silicon wafer edge roughness. After cutting the silicon wafer sample from the edge, place the silicon wafer sample on the jig so that the edge of the silicon wafer sample to be detected remains horizontal, so that the roughness and surface morphology of the silicon wafer edge can be measured using an atomic force microscope. Analyze and reduce measurement errors to ensure test reliability.

100:基座 100: base

110:水平底面 110: Horizontal bottom

120:傾斜承載面 120: Inclined bearing surface

200:夾持部件 200: Clamping parts

210:第一部分 210:Part One

220:第二部分 220:Part 2

221:弧形引導面 221: Arc guide surface

230:夾持槽 230: Clamping slot

10:矽片樣品 10:Silicon wafer sample

10a:斜面 10a: Incline

11:邊緣倒角 11: Edge chamfering

12:第一表面 12: First surface

13:第二表面 13: Second surface

圖1表示本發明實施例中提供的矽片邊緣粗糙度檢測治具的結構示意圖;圖2表示矽片樣品的邊緣處橫截面形貌示意圖;圖3表示本發明實施例中提供的矽片邊緣粗糙度檢測治具上承載矽片樣品時的結構示意圖;圖4表示本發明實施例中提供的矽片邊緣粗糙度檢測方法中切割矽片樣品的一種實施方式的示意圖;圖5表示本發明實施例中提供的矽片邊緣粗糙度檢測方法中切割矽片樣品的另一種實施方式的示意圖;圖6表示本發明實施例中提供的矽片邊緣粗糙度檢測方法中切割矽片樣品的另一種實施方式的示意圖。 Figure 1 shows a schematic structural diagram of a silicon wafer edge roughness detection fixture provided in an embodiment of the present invention; Figure 2 shows a schematic diagram of the cross-sectional morphology at the edge of a silicon wafer sample; Figure 3 shows the edge of a silicon wafer provided in an embodiment of the present invention A schematic structural diagram of a silicon wafer sample carried on a roughness detection jig; Figure 4 shows a schematic diagram of one embodiment of cutting a silicon wafer sample in the silicon wafer edge roughness detection method provided in the embodiment of the present invention; Figure 5 shows the implementation of the present invention A schematic diagram of another implementation of cutting a silicon wafer sample in the silicon wafer edge roughness detection method provided in the example; Figure 6 shows another implementation of cutting a silicon wafer sample in the silicon wafer edge roughness detection method provided in the embodiment of the present invention. Schematic diagram of the method.

為利 貴審查委員了解本發明之技術特徵、內容與優點及其所能達到之功效,茲將本發明配合附圖及附件,並以實施例之表達形式詳細說明如下,而其中所使用之圖式,其主旨僅為示意及輔助說明書之用,未必為本發明實施後之真實比例與精準配置,故不應就所附之圖式的比例與配置關係解讀、侷限本發明於實際實施上的申請範圍,合先敘明。 In order to help the review committee understand the technical features, content and advantages of the present invention and the effects it can achieve, the present invention is described in detail below in the form of embodiments with the accompanying drawings and attachments, and the drawings used therein are , its purpose is only for illustration and auxiliary description, and may not represent the actual proportions and precise configurations after implementation of the present invention. Therefore, the proportions and configuration relationships of the attached drawings should not be interpreted or limited to the actual implementation of the present invention. The scope shall be stated first.

在本發明實施例的描述中,需要理解的是,術語“長度”、“寬度”、“上”、“下”、“前”、“後”、“左”、“右”、“豎直”、“水平”、“頂”、“底”“內”、“外”等指示的方位或位置關係為基於附圖所示的方位或位置關係,僅是為了便於描述本發明實施例和簡化描述,而不是指示或暗示所 指的裝置或元件必須具有特定的方位、以特定的方位構造和操作,因此不能理解為對本發明的限制。 In the description of the embodiments of the present invention, it should be understood that the terms "length", "width", "upper", "lower", "front", "back", "left", "right", "vertical" ", "horizontal", "top", "bottom", "inner", "outer", etc. indicate the orientation or positional relationship based on the orientation or positional relationship shown in the drawings, and are only for convenience and simplicity in describing the embodiments of the present invention. describe, rather than indicate or imply It is intended that devices or elements must have a specific orientation, be constructed and operate in a specific orientation and therefore are not to be construed as limitations of the invention.

此外,術語“第一”、“第二”僅用於描述目的,而不能理解為指示或暗示相對重要性或者隱含指明所指示的技術特徵的數量。由此,限定有“第一”、“第二”的特徵可以明示或者隱含地包括一個或者更多個所述特徵。在本發明實施例的描述中,“多個”的含義是兩個或兩個以上,除非另有明確具體的限定。 In addition, the terms “first” and “second” are used for descriptive purposes only and cannot be understood as indicating or implying relative importance or implicitly indicating the quantity of indicated technical features. Thus, features defined as “first” and “second” may explicitly or implicitly include one or more of the described features. In the description of the embodiments of the present invention, "plurality" means two or more than two, unless otherwise explicitly and specifically limited.

在本發明實施例中,除非另有明確的規定和限定,術語“安裝”、“相連”、“連接”、“固定”等術語應做廣義理解,例如,可以是固定連接,也可以是可拆卸連接,或成一體;可以是機械連接,也可以是電連接;可以是直接相連,也可以通過中間媒介間接相連,可以是兩個元件內部的連通或兩個元件的相互作用關係。對於本領域的具通常知識者而言,可以根據具體情況理解上述術語在本發明實施例中的具體含義。 In the embodiments of the present invention, unless otherwise expressly stipulated and limited, the terms "installation", "connection", "connection", "fixing" and other terms should be understood in a broad sense. For example, it can be a fixed connection or a removable connection. Disassembly and connection, or integration; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium; it can be an internal connection between two elements or an interaction between two elements. For those with ordinary knowledge in the art, the specific meanings of the above terms in the embodiments of the present invention can be understood according to specific circumstances.

在對本發明實施例進行詳細說明之前,有必要對於相關技術進行以下說明:在相關技術中,矽片的邊緣拋光是為了除去矽片邊緣殘留的腐蝕坑,使邊緣變得光滑,使矽片更加堅固,拋光後的邊緣能將顆粒吸附降到最低,以確保矽片邊緣表面的加工精度和較高的良品率。在矽片邊緣表面拋光的加工技術中,首先進行機械的帶式邊緣粗拋光,然後,再對其邊緣表面進行鹼性膠體二氧化矽化學機械拋光的精拋光加工。 Before describing the embodiments of the present invention in detail, it is necessary to make the following description of the related technology: In the related technology, the edge polishing of the silicon wafer is to remove the remaining corrosion pits on the edge of the silicon wafer, smooth the edge, and make the silicon wafer more beautiful. Strong, polished edges can minimize particle adsorption to ensure processing accuracy and high yield on the edge surface of silicon wafers. In the processing technology of silicon wafer edge surface polishing, mechanical belt-type edge rough polishing is first performed, and then the edge surface is finely polished by alkaline colloidal silica chemical mechanical polishing.

矽片的加工製作及半導體器件的製造過程中,存在著一些非常快速的加熱和冷卻過程,因此在矽片的邊緣區域就比較容易產生熱應力的集中,然 而這種熱應力一旦超出了矽晶體本身限度,晶體就會產生位元錯及差排等缺陷。因此,對於矽片邊緣粗糙度和表面的測量和評估尤為重要。 During the processing of silicon wafers and the manufacturing of semiconductor devices, there are some very rapid heating and cooling processes, so it is easier for thermal stress to concentrate in the edge areas of the silicon wafers. Once this thermal stress exceeds the limit of the silicon crystal itself, the crystal will produce defects such as dislocations and dislocations. Therefore, it is particularly important to measure and evaluate the edge roughness and surface of silicon wafers.

然而,在相關技術中,對於矽片表面粗糙度的測量,其中廣受認可的是原子力顯微鏡(Atomic Force Microscope,AFM),其主要用於對矽片表面粗糙度監控,但是尚沒有對矽片邊緣粗糙度和邊緣表面狀態的檢測。 However, among related technologies, for the measurement of surface roughness of silicon wafers, the most widely recognized one is the atomic force microscope (AFM), which is mainly used to monitor the surface roughness of silicon wafers. However, there is no method for measuring the surface roughness of silicon wafers. Detection of edge roughness and edge surface condition.

為了實現對矽片邊緣粗糙度及邊緣表面狀態的檢測,本發明實施例提供了一種矽片邊緣粗糙度檢測治具及檢測方法,能夠對矽片邊緣的粗糙度和表面形貌分析,且能夠減少測量的誤差,保證測試可信度。 In order to detect the edge roughness and edge surface state of the silicon wafer, embodiments of the present invention provide a silicon wafer edge roughness detection jig and a detection method, which can analyze the roughness and surface morphology of the silicon wafer edge, and can Reduce measurement errors and ensure test reliability.

圖1和圖3所示為本發明實施例提供的矽片邊緣粗糙度檢測治具的結構示意圖。 1 and 3 are schematic structural diagrams of a silicon wafer edge roughness detection jig provided by an embodiment of the present invention.

如圖1和圖3所示,該矽片邊緣粗糙度檢測治具包括:基座100及夾持部件200,該基座100用於承載矽片樣品10,該基座100包括水平底面110及與該水平底面110之間呈預設夾角α的傾斜承載面120,0<α

Figure 111128933-A0305-02-0008-8
90°,該夾持部件200用於夾持固定該矽片樣品10,該夾持部件200設置於該傾斜承載面120上。 As shown in Figures 1 and 3, the silicon wafer edge roughness detection fixture includes: a base 100 and a clamping component 200. The base 100 is used to carry the silicon wafer sample 10. The base 100 includes a horizontal bottom surface 110 and The inclined bearing surface 120 forms a preset angle α with the horizontal bottom surface 110, 0<α
Figure 111128933-A0305-02-0008-8
90°, the clamping component 200 is used to clamp and fix the silicon wafer sample 10, and the clamping component 200 is disposed on the inclined bearing surface 120.

由於矽片的邊緣通常會進行倒角設計,因此,若將矽片樣品10直接放置於原子力顯微鏡的樣品臺上,由於矽片邊緣倒角的存在,邊緣待檢測部位呈斜面10a,導致原子力顯微鏡的探針無法對該斜面進行準確掃描,進而無法獲取準確的測試圖像。因此,本發明實施例中設計了一種專門的矽片邊緣粗糙度檢測治具,其主要包括基座100和夾持部件200兩部分,當矽片樣品10承載於基座100的傾斜承載面120上,可以實現矽片樣品10邊緣處的斜面與水平基底保持水平的目的,從而可以使得原子力顯微鏡的探針對該斜面10a進行準確掃描,進而獲取準確的測試圖像。 Since the edge of the silicon wafer is usually chamfered, if the silicon wafer sample 10 is placed directly on the sample stage of the atomic force microscope, due to the chamfering of the edge of the silicon wafer, the part to be detected on the edge will be a bevel 10a, causing the atomic force microscope to The probe cannot accurately scan the bevel, and therefore cannot obtain accurate test images. Therefore, in the embodiment of the present invention, a special silicon wafer edge roughness detection fixture is designed, which mainly includes two parts: a base 100 and a clamping component 200. When the silicon wafer sample 10 is loaded on the inclined bearing surface 120 of the base 100 By doing so, the bevel at the edge of the silicon wafer sample 10 can be kept level with the horizontal base, so that the probe of the atomic force microscope can accurately scan the bevel 10a, thereby obtaining accurate test images.

如圖2所示,該矽片樣品10包括邊緣倒角11、及相對的第一表面12和第二表面13,在垂直於第一表面12的橫截面上,該邊緣倒角11包括最外側頂點O,經過該最外側頂點O的切線垂直於該第一表面12,且該第一表面12與該邊緣倒角11結構的交界點a與經過該最外側頂點O的切線的垂直距離為A1,該第二表面13與該邊緣倒角11結構的交界點b與經過該最外側頂點O的切線的垂直距離為A2,該邊緣倒角11結構的最外側頂點O與該第一表面12之間的垂直距離為B1,與該第二表面13之間的垂直距離為B2;其中,該預設夾角α等於β1或β2;也就是說,該預設夾角α與該矽片樣品10的邊緣倒角11之間應滿足以下關係:tanα=B1/A1或者tanα=B2/A2。 As shown in FIG. 2 , the silicon wafer sample 10 includes an edge chamfer 11 and opposite first and second surfaces 12 and 13 . In a cross section perpendicular to the first surface 12 , the edge chamfer 11 includes an outermost edge chamfer 11 . At vertex O, the tangent line passing through the outermost vertex O is perpendicular to the first surface 12, and the vertical distance between the intersection point a of the first surface 12 and the edge chamfer 11 structure and the tangent line passing through the outermost vertex O is A1 , the vertical distance between the intersection point b of the second surface 13 and the edge chamfer 11 structure and the tangent line passing through the outermost vertex O is A2, and the distance between the outermost vertex O of the edge chamfer 11 structure and the first surface 12 The vertical distance between is B1, and the vertical distance between the second surface 13 and the second surface 13 is B2; wherein, the preset angle α is equal to β1 or β2; that is, the preset angle α and the edge of the silicon wafer sample 10 The following relationship should be satisfied between chamfers 11: tanα=B1/A1 or tanα=B2/A2.

採用上述方案,如圖3所示,當將該矽片樣品10承載於該傾斜承載面120之上時,由於該傾斜承載面120的傾斜角度與矽片樣品10的邊緣倒角11上的斜面角度互補,使得最終矽片樣品10上的邊緣倒角11處的待檢測部位,即倒角處的斜面能夠保持水平。 Using the above solution, as shown in Figure 3, when the silicon wafer sample 10 is carried on the inclined bearing surface 120, due to the inclination angle of the inclined bearing surface 120 and the slope on the edge chamfer 11 of the silicon wafer sample 10 The angles are complementary, so that the portion to be detected at the edge chamfer 11 on the final silicon wafer sample 10, that is, the bevel at the chamfer can remain level.

需要說明的是,在一些實施例中,該基座100的傾斜承載面120可以是固定的傾斜角度,也可以是根據實際產品需求,將該基座100的傾斜承載面120設計為傾斜角度可調的結構。 It should be noted that in some embodiments, the inclined bearing surface 120 of the base 100 may have a fixed inclination angle, or the inclined bearing surface 120 of the base 100 may be designed to have an inclination angle according to actual product requirements. tone structure.

此外,在一些示例性的實施例中,該基座100可採用硬質不易變形材料製成,該夾持部件200採用可彈性變形材料製成的一體結構。 In addition, in some exemplary embodiments, the base 100 can be made of hard non-deformable material, and the clamping component 200 can be made of an integral structure made of elastically deformable material.

具體的,一種實施例中,如圖1和圖3所示,該夾持部件200包括垂直於該傾斜承載面120的第一部分210、及與該第一部分210連接且平行於該傾斜承載面120的第二部分220,該第一部分210、該第二部分220與該傾斜承載面120 配合形成夾持槽230,且該夾持槽230的槽口朝向該傾斜承載面120中水平位置最高的一側。 Specifically, in one embodiment, as shown in FIGS. 1 and 3 , the clamping component 200 includes a first part 210 perpendicular to the inclined bearing surface 120 , and a first part 210 connected to the first part 210 and parallel to the inclined bearing surface 120 the second part 220, the first part 210, the second part 220 and the inclined bearing surface 120 A clamping groove 230 is formed in cooperation, and the notch of the clamping groove 230 faces the side with the highest horizontal position in the inclined bearing surface 120 .

上述方案中,該夾持部件200採用可彈性變形材料製成,且其第一部分210與第二部分220大致連接成L型結構,而與傾斜承載面120之間配合形成夾持槽230,該夾持槽230的開口寬度,即第二部分220與傾斜承載面120之間的距離,可以略小於矽片樣品10第一表面12與第二表面13之間的厚度,這樣,該矽片樣品10可插入該夾持槽230內,通過該第二部分220的彈性變形來夾持固定矽片樣品10。 In the above solution, the clamping component 200 is made of elastically deformable material, and the first part 210 and the second part 220 are generally connected to form an L-shaped structure, and cooperate with the inclined bearing surface 120 to form a clamping groove 230. The opening width of the clamping groove 230, that is, the distance between the second part 220 and the inclined bearing surface 120, can be slightly smaller than the thickness between the first surface 12 and the second surface 13 of the silicon wafer sample 10. In this way, the silicon wafer sample 10 can be inserted into the clamping groove 230, and the silicon chip sample 10 is clamped and fixed through the elastic deformation of the second part 220.

一些實施例中,該第二部分220的位於該夾持槽230的夾持入口處設置為弧形引導面221,這樣便於矽片樣品10進入該夾持槽230內。 In some embodiments, the second part 220 is provided with an arc-shaped guide surface 221 at the clamping entrance of the clamping groove 230 , which facilitates the silicon wafer sample 10 to enter the clamping groove 230 .

需要說明的是,這裡該第一部分210與該傾斜承載面120垂直是指,該第一部分210與該傾斜承載面120大致垂直,例如該第一部分210與該傾斜承載面120之間的角度為90°±10°,這裡該第二部分220與該傾斜承載面120平行是指,該第二部分220與該傾斜承載面120大致平行,例如該第二部分220與該傾斜承載面120之間的角度為0±10°。 It should be noted that the fact that the first part 210 is perpendicular to the inclined bearing surface 120 here means that the first part 210 is substantially perpendicular to the inclined bearing surface 120. For example, the angle between the first part 210 and the inclined bearing surface 120 is 90°. °±10°, here the parallel between the second part 220 and the inclined bearing surface 120 means that the second part 220 and the inclined bearing surface 120 are substantially parallel, for example, the distance between the second part 220 and the inclined bearing surface 120 The angle is 0±10°.

上述方案中的夾持結構採用彈性可變形材質,且利用第一部分210和第二部分220呈L型結構來夾持該矽片樣品10,可以一方面不損傷矽片樣品10,另一方面保持矽片樣品10的表面與傾斜承載面120平行貼合。 The clamping structure in the above solution uses elastically deformable material, and uses the first part 210 and the second part 220 to form an L-shaped structure to clamp the silicon wafer sample 10, which can not damage the silicon wafer sample 10 on the one hand, and maintain the The surface of the silicon chip sample 10 is parallel to the inclined bearing surface 120 .

當然可以理解的是,對於該夾持部件200的具體結構不限於此,只要能夠實現對該矽片樣品10進行夾持,且不損壞該矽片樣品10的結構均可以應用於此。 Of course, it can be understood that the specific structure of the clamping component 200 is not limited to this. As long as the silicon wafer sample 10 can be clamped and the silicon wafer sample 10 is not damaged, any structure can be applied.

此外,本發明實施例還提供了一種矽片邊緣粗糙度檢測方法,包括:步驟S01、在待檢測矽片的邊緣上切割出矽片樣品10,該矽片樣品10至少包括該待檢測矽片邊緣的一部分、及該待檢測矽片樣品表面的一部分;步驟S02、將該矽片樣品10夾持固定於本發明實施例提供的矽片邊緣粗糙度檢測治具上,其中該矽片樣品10的邊緣及該矽片樣品10的表面至少部分未被該夾持部件200遮擋;步驟S03、將該矽片邊緣粗糙度檢測治具放置於原子力顯示鏡的樣品臺上,其中該矽片樣品10的邊緣倒角11處的待檢測區域與該樣品台保持水平;步驟S04、通過原子力顯微鏡的探針對該待檢測區域進行掃描,以獲取測試圖像;步驟S05、對該測試圖像進行處理,得到矽片邊緣粗糙度值和矽片邊緣形貌。 In addition, embodiments of the present invention also provide a method for detecting edge roughness of silicon wafers, including: step S01, cutting a silicon wafer sample 10 on the edge of the silicon wafer to be detected, and the silicon wafer sample 10 at least includes the silicon wafer to be detected A part of the edge and a part of the surface of the silicon wafer sample to be detected; step S02, clamp and fix the silicon wafer sample 10 on the silicon wafer edge roughness detection jig provided by the embodiment of the present invention, wherein the silicon wafer sample 10 The edge of the silicon wafer sample 10 and the surface of the silicon wafer sample 10 are at least partially not blocked by the clamping component 200; step S03, place the silicon wafer edge roughness detection jig on the sample stage of the atomic force display mirror, wherein the silicon wafer sample 10 The area to be detected at the edge chamfer 11 is kept level with the sample stage; Step S04, scan the area to be detected through the probe of the atomic force microscope to obtain a test image; Step S05, process the test image, The edge roughness value of the silicon wafer and the edge morphology of the silicon wafer were obtained.

上述方案,在矽片的邊緣上切割出矽片樣品10,該矽片樣品10上保留至少部分邊緣和至少部分表面,便於對矽片的邊緣粗糙度以及邊緣形貌進行分析;而再通過本發明實施例提供的專門的矽片邊緣檢測治具來對矽片樣品10進行原子力顯微鏡檢測,保持矽片樣品10的邊緣處待檢測部位的斜面保持水平,來實現對矽片邊緣粗糙度以及邊緣形貌準確檢測。 In the above scheme, a silicon wafer sample 10 is cut on the edge of the silicon wafer, and at least part of the edge and at least part of the surface are retained on the silicon wafer sample 10 to facilitate analysis of the edge roughness and edge morphology of the silicon wafer; and then through this The special silicon wafer edge detection fixture provided by the embodiment of the invention is used to perform atomic force microscopy inspection on the silicon wafer sample 10, and the slope of the part to be detected at the edge of the silicon wafer sample 10 is kept level, so as to realize the edge roughness and edge detection of the silicon wafer. Accurate detection of morphology.

在一些實施例中,上述步驟S01具體包括:將該待檢測矽片的邊緣沿該待檢測矽片的圓周順次均勻地劃分出N個檢測點,每個檢測點上切割一個矽片樣品10,N個矽片樣品10上順次標有序號。 In some embodiments, the above step S01 specifically includes: dividing the edge of the silicon wafer to be detected into N detection points evenly along the circumference of the silicon wafer to be detected, and cutting a silicon wafer sample 10 at each detection point, The N silicon wafer samples 10 are sequentially marked with serial numbers.

例如,圖4所示,將待檢測矽片的邊緣沿圓周順次均勻劃分了4個檢測點,在每個檢測點切割一個矽片樣品10,得到4個矽片樣品10,對四個矽片樣品10順次排序,第1號樣品、第2號樣品、第3號樣品和第4號樣品,再通過將4 個樣品依次放置治具上,通過原子力顯微鏡得到測試圖像,從而得到待檢測矽片的邊緣粗糙度以及邊緣形貌分析。 For example, as shown in Figure 4, the edge of the silicon wafer to be detected is evenly divided into 4 detection points along the circumference, and a silicon wafer sample 10 is cut at each detection point to obtain 4 silicon wafer samples 10. For the four silicon wafers, Sample 10 is sorted in sequence, sample No. 1, sample No. 2, sample No. 3 and sample No. 4, and then 4 Each sample is placed on the jig in turn, and the test image is obtained through an atomic force microscope to obtain the edge roughness and edge morphology analysis of the silicon wafer to be detected.

例如,圖5所示,圖5中的4個檢測點與圖4中的4個檢測點選取位置不同,圖5所示也是將待檢測矽片的邊緣沿圓周順次均勻劃分了4個檢測點,在每個檢測點切割一個矽片樣品10,得到4個矽片樣品10,對四個矽片樣品10順次排序,第1號樣品、第2號樣品、第3號樣品和第4號樣品,再通過將4個樣品依次放置治具上,通過原子力顯微鏡得到測試圖像,從而得到待檢測矽片的邊緣粗糙度以及邊緣形貌分析。 For example, as shown in Figure 5, the four detection points in Figure 5 are selected at different positions than the four detection points in Figure 4. Figure 5 also shows that the edge of the silicon wafer to be detected is evenly divided into four detection points along the circumference. , cut a silicon wafer sample 10 at each detection point to obtain 4 silicon wafer samples 10. Sort the four silicon wafer samples 10 in sequence, sample No. 1, sample No. 2, sample No. 3 and sample No. 4 , and then place the four samples on the jig in sequence, and obtain the test image through the atomic force microscope, thereby obtaining the edge roughness and edge morphology analysis of the silicon wafer to be detected.

例如,圖6所示,是將待檢測矽片的邊緣沿圓周順次均勻劃分了8個檢測點,在每個檢測點切割一個矽片樣品10,得到8個矽片樣品10,對四個矽片樣品10順次排序,第1號樣品、第2號樣品、第3號樣品、第4號樣品、第5號樣品、第6號樣品和第7號樣品及第8號樣品,再通過將8個樣品依次放置治具上,通過原子力顯微鏡得到測試圖像,從而得到待檢測矽片的邊緣粗糙度以及邊緣形貌分析。 For example, as shown in Figure 6, the edge of the silicon wafer to be detected is evenly divided into 8 detection points along the circumference, and a silicon wafer sample 10 is cut at each detection point to obtain 8 silicon wafer samples 10. For four silicon wafer samples, Samples 10 are sorted in sequence, sample No. 1, sample No. 2, sample No. 3, sample No. 4, sample No. 5, sample No. 6, sample No. 7 and sample No. 8, and then pass through the 8 Each sample is placed on the jig in turn, and the test image is obtained through an atomic force microscope to obtain the edge roughness and edge morphology analysis of the silicon wafer to be detected.

需要說明的是,以上僅是舉例,在實際應用中,可根據不同的測試需求,從待檢測矽片的邊緣切割出矽片樣品10。 It should be noted that the above are only examples. In actual applications, the silicon wafer sample 10 can be cut from the edge of the silicon wafer to be detected according to different testing requirements.

一些實施例中,每個該矽片樣品10的尺寸大約為1cm×1cm。當然並不以此為限。 In some embodiments, the dimensions of each silicon wafer sample 10 are approximately 1 cm x 1 cm. Of course it is not limited to this.

有以下幾點需要說明:(1)本發明實施例附圖只相關連與本發明實施例相關連的結構,其他結構可參考通常設計; (2)為了清晰起見,在用於描述本發明的實施例的附圖中,層或區域的厚度被放大或縮小,即這些附圖並非按照實際的比例繪製。可以理解,當諸如層、膜、區域或基板之類的元件被稱作位於另一元件“上”或“下”時,所述元件可以“直接”位於另一元件“上”或“下”或者可以存在中間元件;(3)在不衝突的情況下,本發明的實施例及實施例中的特徵可以相互組合以得到新的實施例。 The following points need to be explained: (1) The drawings of the embodiments of the present invention only relate to the structures related to the embodiments of the present invention, and other structures can refer to common designs; (2) For the sake of clarity, in the drawings used to describe embodiments of the present invention, the thicknesses of layers or regions are exaggerated or reduced, that is, these drawings are not drawn according to actual scale. It will be understood that when an element such as a layer, film, region or substrate is referred to as being "on" or "under" another element, it can be "directly on" or "under" the other element Or there may be intermediate elements; (3) Without conflict, the embodiments of the present invention and the features in the embodiments can be combined with each other to obtain new embodiments.

以上僅為本發明之較佳實施例,並非用來限定本發明之實施範圍,如果不脫離本發明之精神和範圍,對本發明進行修改或者等同替換,均應涵蓋在本發明申請專利範圍的保護範圍當中。 The above are only preferred embodiments of the present invention and are not intended to limit the implementation scope of the present invention. If the present invention is modified or equivalently substituted without departing from the spirit and scope of the present invention, the protection shall be covered by the patent scope of the present invention. within the range.

100:基座 100: base

110:水平底面 110: Horizontal bottom

120:傾斜承載面 120: Inclined bearing surface

200:夾持部件 200: Clamping parts

210:第一部分 210:Part One

220:第二部分 220:Part 2

221:弧形引導面 221: Arc guide surface

230:夾持槽 230: Clamping slot

Claims (9)

一種矽片邊緣粗糙度檢測治具,包括: 用於承載矽片樣品的基座,該基座包括水平底面及與該水平底面之間呈預設夾角α的傾斜承載面,0<α≤90°;及,用於夾持固定該矽片樣品的夾持部件,該夾持部件設置於該傾斜承載面上。 A silicon chip edge roughness detection fixture, including: A base for carrying silicon wafer samples. The base includes a horizontal bottom surface and an inclined bearing surface with a preset angle α between the horizontal bottom surface and the horizontal bottom surface, 0<α≤90°; and, used for clamping and fixing the silicon wafer. The clamping component of the sample is arranged on the inclined bearing surface. 如請求項1所述之矽片邊緣粗糙度檢測治具,其中,該矽片樣品包括邊緣倒角、及相對的第一表面和第二表面,在垂直於第一表面的橫截面上,該邊緣倒角包括最外側頂點O,經過該最外側頂點O的切線垂直於該第一表面,且該第一表面與該邊緣倒角結構的交界點a與經過該最外側頂點O的切線的垂直距離為A1,該第二表面與該邊緣倒角結構的交界點b與經過該最外側頂點O的切線的垂直距離為A2,該邊緣倒角結構的最外側頂點O與該第一表面之間的垂直距離為B1,與該第二表面之間的垂直距離為B2;其中,該預設夾角α與該矽片樣品的邊緣倒角之間滿足以下關係:tanα=B1/A1或者tanα=B2/A2。The silicon wafer edge roughness detection fixture according to claim 1, wherein the silicon wafer sample includes edge chamfers, and opposite first and second surfaces. On a cross-section perpendicular to the first surface, the The edge chamfering includes the outermost vertex O, the tangent passing through the outermost vertex O is perpendicular to the first surface, and the intersection point a of the first surface and the edge chamfering structure is perpendicular to the tangent passing through the outermost vertex O. The distance is A1, the vertical distance between the intersection point b of the second surface and the edge chamfer structure and the tangent line passing through the outermost vertex O is A2, and the distance between the outermost vertex O of the edge chamfer structure and the first surface is The vertical distance to the second surface is B1, and the vertical distance to the second surface is B2; where the preset angle α and the edge chamfer of the silicon wafer sample satisfy the following relationship: tanα=B1/A1 or tanα=B2 /A2. 如請求項1所述之矽片邊緣粗糙度檢測治具,其中,該夾持部件採用可彈性變形材料製成的一體結構。The silicon chip edge roughness detection fixture according to claim 1, wherein the clamping component adopts an integrated structure made of elastically deformable material. 如請求項3所述之矽片邊緣粗糙度檢測治具,其中,該夾持部件包括垂直於該傾斜承載面的第一部分、及與該第一部分連接且平行於該傾斜承載面的第二部分,該第一部分、該第二部分與該傾斜承載面配合形成夾持槽,且該夾持槽的槽口朝向該傾斜承載面中水平位置最高的一側。The silicon chip edge roughness detection fixture according to claim 3, wherein the clamping component includes a first part perpendicular to the inclined bearing surface, and a second part connected to the first part and parallel to the inclined bearing surface. , the first part and the second part cooperate with the inclined bearing surface to form a clamping groove, and the notch of the clamping groove faces the side with the highest horizontal position in the inclined bearing surface. 如請求項4所述之矽片邊緣粗糙度檢測治具,其中,該第二部分的位於該夾持槽的夾持入口處設置有弧形引導面。The silicon chip edge roughness detection jig according to claim 4, wherein the second part is provided with an arc-shaped guide surface at the clamping entrance of the clamping groove. 如請求項1所述之矽片邊緣粗糙度檢測治具,其中,該基座採用硬質不易變形材料製成。The silicon chip edge roughness detection fixture as described in claim 1, wherein the base is made of hard and non-deformable material. 一種矽片邊緣粗糙度檢測方法,包括: 在待檢測矽片的邊緣上切割出矽片樣品,該矽片樣品至少包括該待檢測矽片邊緣的一部分、及該待檢測矽片樣品表面的一部分; 將該矽片樣品夾持固定於如請求項1至6中任一項所述之矽片邊緣粗糙度檢測治具上,其中該矽片樣品的邊緣及該矽片樣品的表面至少部分未被該夾持部件遮擋; 將該矽片邊緣粗糙度檢測治具放置於原子力顯示鏡的樣品臺上,其中該矽片樣品的邊緣倒角處的待檢測區域與該樣品台保持水平; 通過原子力顯微鏡的探針對該待檢測區域進行掃描,以獲取測試圖像; 對該測試圖像進行處理,得到矽片邊緣粗糙度值和矽片邊緣形貌。 A method for detecting edge roughness of silicon wafers, including: Cutting a silicon wafer sample on the edge of the silicon wafer to be detected, the silicon wafer sample includes at least a part of the edge of the silicon wafer to be detected and a part of the surface of the silicon wafer sample to be detected; The silicon wafer sample is clamped and fixed on the silicon wafer edge roughness detection fixture as described in any one of claims 1 to 6, wherein at least part of the edge of the silicon wafer sample and the surface of the silicon wafer sample are not The clamping part is blocked; The silicon wafer edge roughness detection fixture is placed on the sample stage of the atomic force display mirror, wherein the area to be detected at the edge chamfer of the silicon wafer sample is kept level with the sample stage; Scan the area to be detected with the probe of an atomic force microscope to obtain a test image; The test image is processed to obtain the edge roughness value of the silicon wafer and the edge morphology of the silicon wafer. 如請求項7所述之矽片邊緣粗糙度檢測方法,其中,該在待檢測矽片的邊緣預定位置點切割出矽片樣品,具體包括: 將該待檢測矽片的邊緣沿該待檢測矽片的圓周順次均勻地劃分出N個檢測點,每個檢測點上切割一個矽片樣品,N個矽片樣品上順次標有序號。 The silicon wafer edge roughness detection method as described in claim 7, wherein the silicon wafer sample is cut at a predetermined position on the edge of the silicon wafer to be detected, specifically including: The edge of the silicon chip to be detected is evenly divided into N detection points along the circumference of the silicon chip to be detected. A silicon chip sample is cut at each detection point, and the N silicon chip samples are sequentially marked with serial numbers. 如請求項8所述之矽片邊緣粗糙度檢測方法,其中,每個該矽片樣品的尺寸為1cm × 1cm。The silicon wafer edge roughness detection method as described in claim 8, wherein the size of each silicon wafer sample is 1cm × 1cm.
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