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RU2019134405A - Акриламидные фотоинициаторы - Google Patents

Акриламидные фотоинициаторы Download PDF

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Publication number
RU2019134405A
RU2019134405A RU2019134405A RU2019134405A RU2019134405A RU 2019134405 A RU2019134405 A RU 2019134405A RU 2019134405 A RU2019134405 A RU 2019134405A RU 2019134405 A RU2019134405 A RU 2019134405A RU 2019134405 A RU2019134405 A RU 2019134405A
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RU
Russia
Prior art keywords
general formula
alkyl
optionally substituted
acrylamide
iic
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RU2019134405A
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English (en)
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RU2019134405A3 (ru
Inventor
Якоб ВАНГЕ
Петр СЕГНАЛ
Дэвид ДЖЕПСОН
Эндрю ТОУС
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Колопласт А/С
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Application filed by Колопласт А/С filed Critical Колопласт А/С
Publication of RU2019134405A publication Critical patent/RU2019134405A/ru
Publication of RU2019134405A3 publication Critical patent/RU2019134405A3/ru

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/06—Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/30—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by doubly-bound oxygen atoms
    • C07C233/33—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by doubly-bound oxygen atoms with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/45—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups
    • C07C233/46—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
    • C07C233/49—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a carbon atom of an acyclic unsaturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/45—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups
    • C07C233/46—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
    • C07C233/51—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to an acyclic carbon atom of a carbon skeleton containing six-membered aromatic rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Indole Compounds (AREA)

Claims (17)

  1. Способ синтеза фотоинициаторов общей формулы (I),
  2. Figure 00000001
  3. (I),
  4. в которой R1 выбран из H или необязательно замещенного C1-C6алкила, и R2=H, при этом указанный способ включает стадии:
  5. a. приведения во взаимодействие спирта общей формулы IIa,
  6. Figure 00000002
  7. IIa,
  8. в которой Za представляет собой линкерный фрагмент, выбранный из одинарной связи, C1-C12алкилена, C1-C12алкенилена, -O-, -S-, -NRa- или -[O-(C1-C12алкилен)]n-, где Ra представляет собой H или необязательно замещенный C1-C12алкил, и n представляет собой целое число от 1 до 20; и
  9. R3 и R4 независимо выбраны из H или необязательно замещенного C1-C6алкила; где R3, или R4, или их часть могут быть связаны с Za с образованием одной или нескольких кольцевых структур;
  10. с акрилонитрилом общей формулы IIb,
  11. Figure 00000003
  12. IIb,
  13. в которой R1 выбран из H или необязательно замещенного C1-C6алкила;
  14. в реакции Риттера с образованием акриламида общей формулы IIc,
  15. Figure 00000004
  16. IIc,
  17. с последующей стадией (b) введения акриламида общей формулы IIc в реакцию ацилирования Фриделя-Крафтса с получением таким образом фотоинициатора общей формулы (I).
RU2019134405A 2017-03-31 2018-03-22 Акриламидные фотоинициаторы RU2019134405A (ru)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DKPA201770237 2017-03-31
DKPA201770237 2017-03-31
PCT/DK2018/050053 WO2018177488A1 (en) 2017-03-31 2018-03-22 Acrylami de photoi ni ti ators

Publications (2)

Publication Number Publication Date
RU2019134405A true RU2019134405A (ru) 2021-04-30
RU2019134405A3 RU2019134405A3 (ru) 2021-07-20

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RU2019134405A RU2019134405A (ru) 2017-03-31 2018-03-22 Акриламидные фотоинициаторы

Country Status (6)

Country Link
US (2) US10851045B2 (ru)
EP (1) EP3601213B1 (ru)
CN (1) CN110352186B (ru)
BR (1) BR112019017667A2 (ru)
RU (1) RU2019134405A (ru)
WO (1) WO2018177488A1 (ru)

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BR112019017667A2 (pt) * 2017-03-31 2020-03-31 Coloplast A/S Fotoiniciador, e, método de síntese dos fotoiniciadores.
BR112020002377A2 (pt) * 2017-08-17 2020-09-01 Coloplast A/S revestimento polimérico, métodos para sintetizar um revestimento polimérico e para revestir um cateter urinário, uso do revestimento polimérico, cateter urinário intermitente, e, kit.
US11406525B2 (en) 2017-11-09 2022-08-09 11 Health And Technologies Limited Ostomy monitoring system and method
USD893514S1 (en) 2018-11-08 2020-08-18 11 Health And Technologies Limited Display screen or portion thereof with graphical user interface
JP7792918B2 (ja) 2020-05-14 2025-12-26 スリーエム イノベイティブ プロパティズ カンパニー 全フッ素化基、光開始剤基、及びアミド連結基を含む化合物
AU2021361238A1 (en) 2020-10-15 2023-05-25 Convatec Technologies Inc. Ostomy systems and methods

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Also Published As

Publication number Publication date
RU2019134405A3 (ru) 2021-07-20
CN110352186B (zh) 2022-10-04
US20210171438A1 (en) 2021-06-10
EP3601213A1 (en) 2020-02-05
WO2018177488A1 (en) 2018-10-04
CN110352186A (zh) 2019-10-18
US10851045B2 (en) 2020-12-01
EP3601213B1 (en) 2022-05-11
US20200109106A1 (en) 2020-04-09
BR112019017667A2 (pt) 2020-03-31
US11685708B2 (en) 2023-06-27

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Effective date: 20211112