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RU2015144080A - Cross-linked products obtained by ionic crosslinking of a solid brand oligomer and polymer using an ionic crosslinking agent and methods for their preparation - Google Patents

Cross-linked products obtained by ionic crosslinking of a solid brand oligomer and polymer using an ionic crosslinking agent and methods for their preparation Download PDF

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Publication number
RU2015144080A
RU2015144080A RU2015144080A RU2015144080A RU2015144080A RU 2015144080 A RU2015144080 A RU 2015144080A RU 2015144080 A RU2015144080 A RU 2015144080A RU 2015144080 A RU2015144080 A RU 2015144080A RU 2015144080 A RU2015144080 A RU 2015144080A
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RU
Russia
Prior art keywords
polymer
oligomer
asphalt
crosslinked product
composition according
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RU2015144080A
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Russian (ru)
Inventor
Костас С. АВРАМИДИС
Original Assignee
Басф Се
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Publication of RU2015144080A publication Critical patent/RU2015144080A/en

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L95/00—Compositions of bituminous materials, e.g. asphalt, tar, pitch
    • C08L95/005—Aqueous compositions, e.g. emulsions
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/12—Polymerisation in non-solvents
    • C08F2/16—Aqueous medium
    • C08F2/22—Emulsion polymerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
    • C08J3/246—Intercrosslinking of at least two polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
    • C08L53/02—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers of vinyl-aromatic monomers and conjugated dienes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L9/00—Compositions of homopolymers or copolymers of conjugated diene hydrocarbons
    • C08L9/06—Copolymers with styrene
    • C08L9/08—Latex
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L95/00—Compositions of bituminous materials, e.g. asphalt, tar, pitch
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2395/00—Bituminous materials, e.g. asphalt, tar or pitch
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
    • C08J2423/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
    • C08J2423/18—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms
    • C08J2423/20—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms having four to nine carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2425/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Derivatives of such polymers
    • C08J2425/02—Homopolymers or copolymers of hydrocarbons
    • C08J2425/04—Homopolymers or copolymers of styrene
    • C08J2425/08—Copolymers of styrene
    • C08J2425/10—Copolymers of styrene with conjugated dienes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L25/00—Compositions of, homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Compositions of derivatives of such polymers
    • C08L25/02—Homopolymers or copolymers of hydrocarbons
    • C08L25/04—Homopolymers or copolymers of styrene
    • C08L25/08—Copolymers of styrene
    • C08L25/10—Copolymers of styrene with conjugated dienes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2555/00—Characteristics of bituminous mixtures
    • C08L2555/20—Mixtures of bitumen and aggregate defined by their production temperatures, e.g. production of asphalt for road or pavement applications
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A30/00—Adapting or protecting infrastructure or their operation
    • Y02A30/30—Adapting or protecting infrastructure or their operation in transportation, e.g. on roads, waterways or railways

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Paints Or Removers (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)

Claims (22)

1. Асфальтовая композиция, содержащая:1. An asphalt composition comprising: сшитый продукт, полученный ионным сшиванием олигомера твердой марки и полимера с применением ионного сшивающего агента.a crosslinked product obtained by ionic crosslinking of a solid brand oligomer and polymer using an ionic crosslinking agent. 2. Композиция по п. 1, в которой полимер является производным 4-80 мас.% стирола, 4-80 мас.% бутадиена и 8-25 мас.% олигомера твердой марки.2. The composition according to p. 1, in which the polymer is a derivative of 4-80 wt.% Styrene, 4-80 wt.% Butadiene and 8-25 wt.% Oligomer solid brand. 3. Композиция по п. 2, в которой полимер является производным 25-59 мас.% стирола, 25-59 мас.% бутадиена и 8-25 мас.% олигомера твердой марки.3. The composition according to p. 2, in which the polymer is a derivative of 25-59 wt.% Styrene, 25-59 wt.% Butadiene and 8-25 wt.% Oligomer solid brand. 4. Композиция по п. 1, в которой полимер является производным гидрофобного мономера, и гидрофобный мономер состоит из бутадиена.4. The composition according to p. 1, in which the polymer is a derivative of a hydrophobic monomer, and the hydrophobic monomer consists of butadiene. 5. Композиция по п. 1, в которой полимер является производным газофазного мономера, выбираемого из этилена, пропилена, изобутилена, винилхлорида, винилиденхлорида или их смеси.5. The composition of claim 1, wherein the polymer is a derivative of a gas phase monomer selected from ethylene, propylene, isobutylene, vinyl chloride, vinylidene chloride, or a mixture thereof. 6. Композиция по п. 5, в которой полимер является производным этилена и 81 мас.% или менее винилацетата.6. The composition according to p. 5, in which the polymer is a derivative of ethylene and 81 wt.% Or less vinyl acetate. 7. Композиция по п. 6, в которой полимер является производным 16%-41 мас.% этилена, 41-67 мас.% винилацетата и 8-25 мас.% олигомера твердой марки.7. The composition according to p. 6, in which the polymer is a derivative of 16% -41 wt.% Ethylene, 41-67 wt.% Vinyl acetate and 8-25 wt.% Oligomer solid brand. 8. Композиция по любому одному из пп. 1-7, в которой сшитый продукт не содержит серу.8. The composition according to any one of paragraphs. 1-7, in which the crosslinked product does not contain sulfur. 9. Асфальтовая композиция по любому одному из пп. 1-7, в которой верхний температурный предел по SHRP (программе стратегических исследований в области автомобильных дорог) составляет 76°С или выше.9. Asphalt composition according to any one of paragraphs. 1-7, in which the upper temperature limit for SHRP (strategic research program in the field of roads) is 76 ° C or higher. 10. Асфальтовая композиция по п. 8, в которой верхний температурный предел по SHRP составляет 76°С или выше.10. The asphalt composition of claim 8, wherein the SHRP upper temperature limit is 76 ° C. or higher. 11. Способ получения асфальтовой композиции по любому из пп. 1-10, включающий:11. A method of obtaining an asphalt composition according to any one of paragraphs. 1-10, including: обеспечение сшитого продукта;providing a crosslinked product; смешение сшитого продукта с асфальтом при температуре, равной 160°С или менее.mixing the crosslinked product with asphalt at a temperature of 160 ° C or less. 12. Способ получения асфальтовой композиции, включающий:12. A method of obtaining an asphalt composition, comprising: сшивание олигомера твердой марки и полимера с применением ионного сшивающего агента с образованием сшитого продукта; иcrosslinking a solid brand oligomer and a polymer using an ionic crosslinking agent to form a crosslinked product; and смешение сшитого продукта с асфальтом при температуре, равной 160°С или менее, с получением асфальтовой композиции.mixing the crosslinked product with asphalt at a temperature of 160 ° C. or less to obtain an asphalt composition. 13. Способ по п. 12, дополнительно включающий в себя стадию взаимодействия олигомера твердой марки с полимером до стадии сшивания.13. The method of claim 12, further comprising the step of reacting the solid brand oligomer with the polymer prior to the crosslinking step. 14. Способ по п. 12, в котором стадия сшивания протекает при температуре окружающей среды.14. The method according to p. 12, in which the stage of crosslinking proceeds at ambient temperature. 15. Способ по пп. 12-14, в котором стадия смешения включает в себя смешение сшитого продукта с асфальтом при температуре, равной 120°С или менее, с получением асфальтовой композиции.15. The method according to PP. 12-14, in which the mixing stage includes mixing the crosslinked product with asphalt at a temperature of 120 ° C or less, to obtain an asphalt composition. 16. Способ по любому одному из пп. 12-14, в котором асфальтовую композицию получают без применения сшивающих агентов на основе серы.16. The method according to any one of paragraphs. 12-14, in which the asphalt composition is obtained without the use of sulfur-based crosslinking agents. 17. Способ по п. 15, в котором асфальтовую композицию получают без применения сшивающих агентов на основе серы.17. The method according to p. 15, in which the asphalt composition is obtained without the use of crosslinking agents based on sulfur.
RU2015144080A 2013-03-15 2014-03-11 Cross-linked products obtained by ionic crosslinking of a solid brand oligomer and polymer using an ionic crosslinking agent and methods for their preparation RU2015144080A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361793686P 2013-03-15 2013-03-15
US61/793686 2013-03-15
PCT/EP2014/054680 WO2014139999A1 (en) 2013-03-15 2014-03-11 Crosslinked products prepared by ionically crosslinking a solid grade oligomer and a polymer using an ionic crosslinking agent and methods of making the same

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RU2015144080A true RU2015144080A (en) 2017-04-24

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US (2) US10174201B2 (en)
EP (1) EP2970517B1 (en)
KR (1) KR20150129849A (en)
CN (1) CN105283469B (en)
AU (1) AU2014230892B2 (en)
BR (1) BR112015021904A2 (en)
CA (1) CA2899547A1 (en)
MX (1) MX2015010210A (en)
RU (1) RU2015144080A (en)
WO (1) WO2014139999A1 (en)

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US20190136061A1 (en) 2019-05-09
EP2970517B1 (en) 2020-01-01
CA2899547A1 (en) 2014-09-18
US10174201B2 (en) 2019-01-08
MX2015010210A (en) 2015-11-25
AU2014230892A1 (en) 2015-09-17
CN105283469A (en) 2016-01-27
BR112015021904A2 (en) 2017-07-18
CN105283469B (en) 2018-02-13
WO2014139999A1 (en) 2014-09-18
EP2970517A1 (en) 2016-01-20
KR20150129849A (en) 2015-11-20
AU2014230892B2 (en) 2017-05-11
US20160046810A1 (en) 2016-02-18

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