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RU2013122018A - METHOD FOR PRODUCING 1-AZIDO-2-ETHYL-1,2-DIHYDROS (С60-Ih) [5,6] FULLERENA - Google Patents

METHOD FOR PRODUCING 1-AZIDO-2-ETHYL-1,2-DIHYDROS (С60-Ih) [5,6] FULLERENA Download PDF

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RU2013122018A
RU2013122018A RU2013122018/04A RU2013122018A RU2013122018A RU 2013122018 A RU2013122018 A RU 2013122018A RU 2013122018/04 A RU2013122018/04 A RU 2013122018/04A RU 2013122018 A RU2013122018 A RU 2013122018A RU 2013122018 A RU2013122018 A RU 2013122018A
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azido
ethyl
fullerena
dihydros
producing
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RU2013122018/04A
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RU2540087C2 (en
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Усеин Меметович Джемилев
Айрат Рамилевич Туктаров
Арслан Рифхатович Ахметов
Ильдар Рафисович Яруллин
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Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук
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Abstract

Способ получения 1-азидо-2-этил-1,2-дигидро(С-I)[5,6]фуллерена формулы (1)характеризующийся тем, что фуллерен Свзаимодействует с диэтилалюминий азидом (EtAlN) взятыми в мольном соотношении С:EtAlN=1:(40-60), в растворе сухого толуола при -20°С, в атмосфере аргона с последующим нагреванием до 40°С в течение 2-4 ч.The method of obtaining 1-azido-2-ethyl-1,2-dihydro (CI) [5,6] fullerene of the formula (1) characterized in that fullerene interacts with diethylaluminium azide (EtAlN) taken in a molar ratio C: EtAlN = 1: (40-60), in a solution of dry toluene at -20 ° C, in an argon atmosphere, followed by heating to 40 ° C for 2-4 hours

Claims (1)

Способ получения 1-азидо-2-этил-1,2-дигидро(С60-Ih)[5,6]фуллерена формулы (1)The method of obtaining 1-azido-2-ethyl-1,2-dihydro (C 60 -I h ) [5,6] fullerene of the formula (1)
Figure 00000001
Figure 00000001
 характеризующийся тем, что фуллерен С60 взаимодействует с диэтилалюминий азидом (Et2AlN3) взятыми в мольном соотношении С60:Et2AlN3=1:(40-60), в растворе сухого толуола при -20°С, в атмосфере аргона с последующим нагреванием до 40°С в течение 2-4 ч. characterized in that the fullerene C 60 interacts with diethylaluminium azide (Et 2 AlN 3 ) taken in a molar ratio of C 60 : Et 2 AlN 3 = 1: (40-60), in a solution of dry toluene at -20 ° C, in an argon atmosphere followed by heating to 40 ° C for 2-4 hours
RU2013122018/04A 2013-05-13 2013-05-13 Method of obtaining 1-azido-2-ethyl-1,2-dihydro(c60-ih)[5,6]fullerene RU2540087C2 (en)

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RU2484010C2 (en) * 2011-06-16 2013-06-10 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран METHOD OF PRODUCING 1-IODO-2-AZIDO(C60-Ih)[5,6]FULLERENE

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