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RU2010150252A - METHOD FOR PRODUCING AZIRIDINO [2 ', 3': 1,2] FULLERENA [60] - Google Patents

METHOD FOR PRODUCING AZIRIDINO [2 ', 3': 1,2] FULLERENA [60] Download PDF

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RU2010150252A
RU2010150252A RU2010150252/04A RU2010150252A RU2010150252A RU 2010150252 A RU2010150252 A RU 2010150252A RU 2010150252/04 A RU2010150252/04 A RU 2010150252/04A RU 2010150252 A RU2010150252 A RU 2010150252A RU 2010150252 A RU2010150252 A RU 2010150252A
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Russia
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aziridino
producing
fullerene
fullerena
nan3
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RU2010150252/04A
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Russian (ru)
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RU2466990C2 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Айрат Рамилевич Туктаров (RU)
Айрат Рамилевич Туктаров
Арслан Рифхатович Ахметов (RU)
Арслан Рифхатович Ахметов
Ильдар Рафисович Яруллин (RU)
Ильдар Рафисович Яруллин
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Учреждение Российской академии наук ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА РАН (RU)
Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран
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Abstract

Способ получения азиридино[2',3':1,2]фуллерена[60] общей формулы (1) ! ! отличающийся тем, что фуллерен С60 взаимодействует с азотистоводородной кислотой (HN3), генерируемой in situ реакцией NaN3 с H2SO4, взятыми в мольном соотношении С60:NaN3:H2SO4=1:(100-120):(100-120), в хлорбензоле при температуре 60°С в течение 2-4 ч. The method of producing aziridino [2 ', 3': 1,2] fullerene [60] of the general formula (1)! ! characterized in that the fullerene C60 interacts with nitric acid (HN3) generated in situ by the reaction of NaN3 with H2SO4 taken in a molar ratio of C60: NaN3: H2SO4 = 1: (100-120): (100-120), in chlorobenzene at a temperature 60 ° C for 2-4 hours

Claims (1)

Способ получения азиридино[2',3':1,2]фуллерена[60] общей формулы (1)The method of producing aziridino [2 ', 3': 1,2] fullerene [60] of the general formula (1)
Figure 00000001
Figure 00000001
 отличающийся тем, что фуллерен С60 взаимодействует с азотистоводородной кислотой (HN3), генерируемой in situ реакцией NaN3 с H2SO4, взятыми в мольном соотношении С60:NaN3:H2SO4=1:(100-120):(100-120), в хлорбензоле при температуре 60°С в течение 2-4 ч. characterized in that the fullerene C 60 interacts with nitric acid (HN 3 ) generated in situ by the reaction of NaN 3 with H 2 SO 4 taken in a molar ratio of C 60 : NaN 3 : H 2 SO 4 = 1: (100-120) : (100-120), in chlorobenzene at a temperature of 60 ° C for 2-4 hours
RU2010150252/04A 2010-12-07 2010-12-07 Method of obtaining aziridino[2',3':1,2] fullerene[60] RU2466990C2 (en)

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RU2594561C2 (en) * 2014-12-10 2016-08-20 Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук Method of producing n-alkil aziridino[2',3':1,9] fullerene [60]
RU2596876C2 (en) * 2014-12-10 2016-09-10 Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук Method of producing aziridino[2',3':1,9]fullerenes[60], containing framework and polycyclic substitutes
RU2594562C2 (en) * 2014-12-11 2016-08-20 Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук Method for producing n-arylaziridinum[2 ', 3 ': 1.9]fullerene [60]

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WO1996026186A1 (en) * 1995-02-23 1996-08-29 Hoechst Aktiengesellschaft Azafullerenes, method for producing them and their use
RU2342382C2 (en) * 2007-02-05 2008-12-27 Институт нефтехимии и катализа РАН Method of obtaining 2,5-dialkyl-3,4- fullero[60]tetrahydrothiophenes

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Effective date: 20121208