[go: up one dir, main page]

RU2007104481A - METHOD FOR PRODUCING 2-ALKYL-5-PHENYL-3,4-FULLERO [60] TETRAHYDROTHIOPHENES - Google Patents

METHOD FOR PRODUCING 2-ALKYL-5-PHENYL-3,4-FULLERO [60] TETRAHYDROTHIOPHENES Download PDF

Info

Publication number
RU2007104481A
RU2007104481A RU2007104481/04A RU2007104481A RU2007104481A RU 2007104481 A RU2007104481 A RU 2007104481A RU 2007104481/04 A RU2007104481/04 A RU 2007104481/04A RU 2007104481 A RU2007104481 A RU 2007104481A RU 2007104481 A RU2007104481 A RU 2007104481A
Authority
RU
Russia
Prior art keywords
fullero
tetrahydrothiophenes
phenyl
alkyl
producing
Prior art date
Application number
RU2007104481/04A
Other languages
Russian (ru)
Other versions
RU2342376C2 (en
Inventor
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Айрат Рамилевич Туктаров (RU)
Айрат Рамилевич Туктаров
Арслан Рифхатович Ахметов (RU)
Арслан Рифхатович Ахметов
Галина Аркадьевна Джемилева (RU)
Галина Аркадьевна Джемилева
Марко Пудас (FI)
Марко Пудас
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Original Assignee
Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Институт нефтехимии и катализа РАН (RU), Институт нефтехимии и катализа РАН filed Critical Институт нефтехимии и катализа РАН (RU)
Priority to RU2007104481/04A priority Critical patent/RU2342376C2/en
Publication of RU2007104481A publication Critical patent/RU2007104481A/en
Application granted granted Critical
Publication of RU2342376C2 publication Critical patent/RU2342376C2/en

Links

Landscapes

  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Claims (1)

Способ получения 2-алкил-5-фенил-3,4-фуллеро[60]тетрагидротиофенов общей формулы (1)The method of obtaining 2-alkyl-5-phenyl-3,4-fullero [60] tetrahydrothiophenes of the General formula (1)
Figure 00000001
Figure 00000001
 путем взаимодействия фуллерена С60 с алкилбензилсульфидами формулы RCH2SPh (где R=H, Me, Et), в присутствии катализатора цирконацендихлорида Cp2ZrCl2, взятыми в мольном соотношении С60: алкилбензилсульфид: Cp2ZrCl2 = 0,01:(0,045-0,055):(0,0015-0,0025), в среде толуола, при температуре 140-160°С в течение 4-8 ч.by reacting fullerene C 60 with alkylbenzyl sulfides of the formula RCH 2 SPh (where R = H, Me, Et), in the presence of a catalyst of zirconacene dichloride Cp 2 ZrCl 2 , taken in a molar ratio of C 60 : alkylbenzyl sulfide: Cp 2 ZrCl 2 = 0.01 :( 0.045-0.055) :( 0.0015-0.0025), in toluene, at a temperature of 140-160 ° C for 4-8 hours.
RU2007104481/04A 2007-02-05 2007-02-05 Method of obtaining 2-alkyl-5-phenyl-3,4- fullero[60]tetrahydrothiophenes RU2342376C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2007104481/04A RU2342376C2 (en) 2007-02-05 2007-02-05 Method of obtaining 2-alkyl-5-phenyl-3,4- fullero[60]tetrahydrothiophenes

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2007104481/04A RU2342376C2 (en) 2007-02-05 2007-02-05 Method of obtaining 2-alkyl-5-phenyl-3,4- fullero[60]tetrahydrothiophenes

Publications (2)

Publication Number Publication Date
RU2007104481A true RU2007104481A (en) 2008-08-10
RU2342376C2 RU2342376C2 (en) 2008-12-27

Family

ID=39746090

Family Applications (1)

Application Number Title Priority Date Filing Date
RU2007104481/04A RU2342376C2 (en) 2007-02-05 2007-02-05 Method of obtaining 2-alkyl-5-phenyl-3,4- fullero[60]tetrahydrothiophenes

Country Status (1)

Country Link
RU (1) RU2342376C2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2455290C1 (en) * 2010-12-07 2012-07-10 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing triazolino[4',5':1,2]fullerene[60]

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5372798A (en) * 1994-03-08 1994-12-13 Exxon Research And Engineering Company Fullerene compositions and preparation
RU2188154C2 (en) * 2000-07-14 2002-08-27 Институт нефтехимии и катализа АН РБ и УНЦ РАН Method of synthesis of fullerene[60] sulfoxides
RU2191182C1 (en) * 2001-05-14 2002-10-20 Институт нефтехимии и катализа АН РБ и УНЦ РАН METHOD OF SYNTHESIS OF 2,3-FULLERENO[60]-2,3,4,7-TETRA-HYDRO-1H-λ6-THIEPINE-1,1-DIOXIDE

Also Published As

Publication number Publication date
RU2342376C2 (en) 2008-12-27

Similar Documents

Publication Publication Date Title
EP2662352A3 (en) Method for Producing Phenylacetamide Compound
EP2339660A3 (en) Monoamine compound, charge transporting material and organic electroluminescent device
WO2008090282A3 (en) Hydrotreatment catalyst method for production and use thereof
BR112014004313A8 (en) GLYCOSIDE COMPOUND, METHODS OF PRODUCTION OF A THIOETHER, ETHER AND GLYCOSIDE COMPOUND, AND, ETHER.
JP2014094926A5 (en)
RU2010131168A (en) SULFENAMIDE, VOLCANIZATION ACCELERATOR OF RUBBER CONTAINING SULFENAMID AND METHOD FOR PRODUCING VULCANIZATION ACCELERATOR
MX2009011186A (en) A process for the manufacture of natural oil hydroxylates.
EA017861B9 (en) Method for producing 4-oxoquinoline compound
RU2007104481A (en) METHOD FOR PRODUCING 2-ALKYL-5-PHENYL-3,4-FULLERO [60] TETRAHYDROTHIOPHENES
MY145433A (en) Process for hydrogenating methylolalkanals
EP1728788A3 (en) Fluorine-containing amide compound and method for preparing the same
RU2007104473A (en) METHOD FOR PRODUCING 2,5-DIALKYL-3,4-FULLERO [60] TETRAHYDROTHIOPHENES
RU2007104307A (en) METHOD FOR PRODUCING 2,5-DIPHENYL-3,4, -FULLERO [60] TETRAHYDROTHIOPHENE
RU2007104485A (en) METHOD FOR PRODUCING 3,4-FULLERO [60] TETRAHYDROTHYOPHENE
RU2007104470A (en) METHOD FOR PRODUCING 2,5-DIPHENYL-3,4-FULLERO [60] TETRAHYDROTHIOPHEN-1-OH
RU2007104482A (en) METHOD FOR PRODUCING 2,5-DIALKYL-3,4-FULLERO [60] TETRAHYDROTHIOPHEN-1-ONES
WO2008149612A1 (en) Asymmetric bf3 complex
RU2008103094A (en) METHOD FOR PRODUCING 1-ALCOXY (CYCLOALCOXY) -1,2-DIHYDRO [60] FULLERENES
RU2007104471A (en) METHOD FOR PRODUCING 3,4-FULLERO [60] TETRAHYDROTHIOPHEN-1-OH
RU2007122007A (en) METHOD FOR PRODUCING 2,3-FULLERO [60] -7-PHENYL-7-PHOSFABICYCLO [2.2.1] HEPTAN
RU2007121961A (en) METHOD FOR PRODUCING 2, 3-FULLERO-7-TIABICYCLO [2.2.1] HEPTAN
RU2007122003A (en) METHOD FOR PRODUCING 1-HYDROXY-1,2-DIHYDRO [60] FULLERENA
DE602007010363D1 (en) sugar donor
RU2005115105A (en) METHOD FOR PRODUCING ACETYLENE COMPOUND
RU2004102935A (en) METHOD FOR PRODUCING 2- AND 4-ALKYLAMINO-3-AMINO-5-NITROBENZOIC ACIDS

Legal Events

Date Code Title Description
MM4A The patent is invalid due to non-payment of fees

Effective date: 20090206